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1.发明授权Cordierite porous ceramic honeycomb articles with delayed microcrack evolution 有权具有延迟微裂纹演化的堇青石多孔陶瓷蜂窝体制品公开(公告)号：US08999224B2
公开(公告)日：2015-04-07
申请号：US12956378
申请日：2010-11-30
IPC分类号： C04B35/195 , C04B38/00 , B01J35/04 , C04B35/636 , C04B35/638 , B01D46/24 , B01J37/02 , C04B111/00 , C04B111/20 , C04B111/34
CPC分类号： C04B38/0006 , B01D46/2429 , B01D46/244 , B01D46/2444 , B01D46/247 , B01D2046/2433 , B01D2046/2437 , B01D2046/2496 , B01J35/04 , B01J37/0215 , B29C47/0028 , C04B35/195 , C04B35/50 , C04B35/505 , C04B35/6365 , C04B35/638 , C04B2111/00793 , C04B2111/0081 , C04B2111/2084 , C04B2111/343 , C04B2235/3206 , C04B2235/3213 , C04B2235/3217 , C04B2235/3222 , C04B2235/3225 , C04B2235/3227 , C04B2235/3418 , C04B2235/3445 , C04B2235/3472 , C04B2235/349 , C04B2235/425 , C04B2235/6021 , C04B2235/76 , C04B2235/786 , C04B2235/787 , C04B2235/85 , C04B2235/9607 , C04B2235/9615 , Y10T428/24149 , C04B38/0054 , C04B38/0074 , C04B38/0645 , C04B38/0675 , C04B38/068
摘要： A porous ceramic honeycomb article includes a primary cordierite phase and an intercrystalline glass phase. In an as-fired condition, the porous ceramic honeycomb article exhibits microcrack parameter Nb3≦0.06 and an as-fired E500° C./E25° C. ratio ≦0.99. The article exhibits a coated microcrack parameter Nb3≦0.14 and a coated E500° C./E25° C. ratio ≦1.06 after the porous ceramic honeycomb article has been washcoated and calcined at a temperature of 550° C. After the article is exposed to a thermal treatment at a temperature ≧800° C. following washcoating and calcining, at least a first portion of the porous ceramic honeycomb article has a first treated microcrack parameter Nb3≧0.18, and a first treated mean coefficient of thermal expansion of not more than 12×10−7/° C. over a temperature range of 25° C. to 800° C. Methods of forming the porous ceramic honeycomb article are also disclosed.
摘要翻译： 多孔陶瓷蜂窝制品包括初级堇青石相和晶间玻璃相。 在焙烧条件下，多孔陶瓷蜂窝体制品显示出微裂纹参数Nb3＆nlE; 0.06和烧制的E500℃/ E25℃比。 在多孔陶瓷蜂窝体制品经过涂覆并在550℃的温度下煅烧之后，该制品显示出涂覆的微裂纹参数Nb 3+ nlE; 0.14和涂覆的E500℃/ E25℃比率和1.06。 在温度≥800℃下进行热处理，在洗涂和煅烧之后，多孔陶瓷蜂窝体制品的至少第一部分具有第一处理微裂纹参数Nb3≥0.18，并且第一次处理的平均热膨胀系数不大于 在25℃至800℃的温度范围内为12×10-7 /℃。还公开了形成多孔陶瓷蜂窝体制品的方法。
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2.发明申请Cordierite Porous Ceramic Honeycomb Articles With Delayed Microcrack Evolution 有权堇青石多孔陶瓷蜂窝制品与延迟微裂纹演变公开(公告)号：US20120135186A1
公开(公告)日：2012-05-31
申请号：US12956378
申请日：2010-11-30
CPC分类号： C04B38/0006 , B01D46/2429 , B01D46/244 , B01D46/2444 , B01D46/247 , B01D2046/2433 , B01D2046/2437 , B01D2046/2496 , B01J35/04 , B01J37/0215 , B29C47/0028 , C04B35/195 , C04B35/50 , C04B35/505 , C04B35/6365 , C04B35/638 , C04B2111/00793 , C04B2111/0081 , C04B2111/2084 , C04B2111/343 , C04B2235/3206 , C04B2235/3213 , C04B2235/3217 , C04B2235/3222 , C04B2235/3225 , C04B2235/3227 , C04B2235/3418 , C04B2235/3445 , C04B2235/3472 , C04B2235/349 , C04B2235/425 , C04B2235/6021 , C04B2235/76 , C04B2235/786 , C04B2235/787 , C04B2235/85 , C04B2235/9607 , C04B2235/9615 , Y10T428/24149 , C04B38/0054 , C04B38/0074 , C04B38/0645 , C04B38/0675 , C04B38/068
摘要： A porous ceramic honeycomb article includes a primary cordierite phase and an intercrystalline glass phase. In an as-fired condition, the porous ceramic honeycomb article exhibits microcrack parameter Nb3 ≦0.06 and an as-fired E500° C./E25° C. ratio ≦0.99. The article exhibits a coated microcrack parameter Nb3 ≦0.14 and a coated E500° C./E25° C. ratio ≦1.06 after the porous ceramic honeycomb article has been washcoated and calcined at a temperature of 550° C. After the article is exposed to a thermal treatment at a temperature ≧800° C. following washcoating and calcining, at least a first portion of the porous ceramic honeycomb article has a first treated microcrack parameter Nb3 ≧0.18, and a first treated mean coefficient of thermal expansion of not more than 12×10−7/° C. over a temperature range of 25° C. to 800° C. Methods of forming the porous ceramic honeycomb article are also disclosed.
摘要翻译： 多孔陶瓷蜂窝制品包括初级堇青石相和晶间玻璃相。 在焙烧条件下，多孔陶瓷蜂窝体制品显示出微裂纹参数Nb3＆nlE; 0.06和烧制的E500℃/ E25℃比。 在多孔陶瓷蜂窝体制品已经被涂覆并在550℃的温度下煅烧之后，该制品显示出涂覆的微裂纹参数Nb 3+ nlE; 0.14和涂覆的E500℃/ E25℃比率和1.06。 在温度≥800℃下进行热处理，在洗涂和煅烧之后，多孔陶瓷蜂窝体制品的至少第一部分具有第一处理的微裂纹参数Nb3≥0.18，并且第一次处理的平均热膨胀系数不为 在25℃至800℃的温度范围内超过12×10-7 /℃。还公开了形成多孔陶瓷蜂窝体制品的方法。
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3.发明申请Low back pressure porous cordierite ceramic honeycomb article and methods for manufacturing same 审中-公开低背压多孔堇青石陶瓷蜂窝体及其制造方法公开(公告)号：US20080050557A1
公开(公告)日：2008-02-28
申请号：US11895167
申请日：2007-08-23
申请人： Douglas Munroe Beall , Thomas Richard Chapman , Martin Joseph Murtagh , Balaji Venkatesan Swarnamani
发明人： Douglas Munroe Beall , Thomas Richard Chapman , Martin Joseph Murtagh , Balaji Venkatesan Swarnamani
CPC分类号： C04B38/0006 , C04B35/195 , C04B35/6263 , C04B2111/00793 , C04B2235/6562 , Y10T428/24149 , C04B38/0054 , C04B38/0067 , C04B38/068
摘要： Disclosed are porous ceramic honeycomb articles, such as filters, which are composed predominately of a cordierite composition. The ceramic honeycomb articles possess a porous microstructure characterized by a unique combination of relatively high porosity (>45%), and moderately narrow pore size distribution wherein greater than 15% and less than 38% of the total porosity exhibits a pore diameter less than 10 μm, and low CTE wherein CTE≦6.0×10−7/° C. (from 23° C. to 800° C.). The articles exhibit high thermal durability and high filtration efficiency coupled with low pressure drop. Such ceramic articles are particularly well suited for use in filtration applications, such as in diesel exhaust filters. Also disclosed are methods for manufacturing the porous ceramic honeycomb article.
摘要翻译： 公开了主要由堇青石组合物组成的多孔陶瓷蜂窝制品，例如过滤器。 陶瓷蜂窝体制品具有多孔微结构，其特征在于相对高孔隙率（> 45％）和适度窄的孔径分布的独特组合，其中大于15％且小于总孔隙率的38％显示孔径小于10 妈妈和低CTE，其中CTE <= 6.0×10 -7 /℃（从23℃至800℃）。 该制品表现出高热耐久性和高过滤效率以及低压降。 这种陶瓷制品特别适用于过滤应用，如柴油机废气过滤器。 还公开了制造多孔陶瓷蜂窝体制品的方法。
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4.发明申请公开(公告)号：US20080047243A1
公开(公告)日：2008-02-28
申请号：US11510227
申请日：2006-08-25
IPC分类号： B01D46/00
CPC分类号： C04B35/195 , B01D46/2425 , B01D46/2429 , B01D46/244 , B01D46/2444 , B01D2046/2433 , B01D2046/2437 , B01D2046/2496 , C04B38/0009 , C04B2111/00793 , C04B38/00 , C04B38/0054 , C04B38/0074
摘要： Disclosed are ceramic honeycomb articles, which are composed predominately of a crystalline phase cordierite composition. The ceramic honeycomb articles possess a microstructure characterized by a unique combination of relatively high total porosity of less than 54%, and relatively narrow pore size distribution having a d10 pore diameter of not less than 8 μm, a d90 pore diameter of not greater than 35 μm, and a value of df=(d50−d10)/d50 of less than 0.50. The articles exhibit high thermal durability and high filtration efficiency coupled with low pressure drop across the filter. Such ceramic articles are particularly well suited for filtration applications, such as diesel exhaust filters or DPFs. Also disclosed are methods for manufacturing the ceramic articles of the present invention.
摘要翻译： 公开了主要由结晶相堇青石组合物组成的陶瓷蜂窝体制品。 陶瓷蜂窝体制品具有微结构，其特征在于具有小于54％的相对高的总孔隙率的独特组合，以及具有不小于8μm的孔径的孔径分布， 不大于35μm的细孔直径，并且其中d≥30
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5.发明申请Methods for Manufacturing Low Back Pressure Porous Cordierite Ceramic Honeycomb Articles 审中-公开制造低背压多孔堇青石陶瓷蜂窝制品的方法公开(公告)号：US20110121478A1
公开(公告)日：2011-05-26
申请号：US13017792
申请日：2011-01-31
申请人： Douglas Munroe Beall , Thomas Richard Chapman , Martin Joseph Murtagh , Balaji Venkatesan Swarnamani
发明人： Douglas Munroe Beall , Thomas Richard Chapman , Martin Joseph Murtagh , Balaji Venkatesan Swarnamani
IPC分类号： B28B1/50
CPC分类号： C04B38/0006 , C04B35/195 , C04B35/6263 , C04B2111/00793 , C04B2235/6562 , Y10T428/24149 , C04B38/0054 , C04B38/0067 , C04B38/068
摘要： Disclosed are porous ceramic honeycomb articles, such as filters, which are composed predominately of a cordierite composition. The ceramic honeycomb articles possess a porous microstructure characterized by a unique combination of relatively high porosity (>45%), and moderately narrow pore size distribution wherein greater than 15% and less than 38% of the total porosity exhibits a pore diameter less than 10 μm, and low CTE wherein CTE≦6.0×10−7/° C. (from 23° C. to 800° C.). The articles exhibit high thermal durability and high filtration efficiency coupled with low pressure drop. Such ceramic articles are particularly well suited for use in filtration applications, such as in diesel exhaust filters. Also disclosed are methods for manufacturing the porous ceramic honeycomb article.
摘要翻译： 公开了主要由堇青石组合物组成的多孔陶瓷蜂窝制品，例如过滤器。 陶瓷蜂窝体制品具有多孔微结构，其特征在于相对高孔隙率（> 45％）和适度窄的孔径分布的独特组合，其中大于15％且小于总孔隙率的38％显示孔径小于10 μm和低CTE，其中CTE＆NlE; 6.0×10-7 /℃（从23℃至800℃）。 该制品表现出高热耐久性和高过滤效率以及低压降。 这种陶瓷制品特别适用于过滤应用，如柴油机废气过滤器。 还公开了制造多孔陶瓷蜂窝体制品的方法。
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6.发明授权High porosity ceramic honeycomb article containing rare earth oxide and method of manufacturing same 有权含有稀土氧化物的高孔隙率陶瓷蜂窝体及其制造方法公开(公告)号：US08709577B2
公开(公告)日：2014-04-29
申请号：US11823580
申请日：2007-06-28
IPC分类号： C04B35/195
CPC分类号： C04B35/195 , C04B38/0006 , C04B2111/00793 , C04B2111/0081 , C04B2111/2084 , C04B2111/32 , C04B2111/343 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3445 , C04B2235/349 , C04B2235/52 , C04B2235/5436 , C04B2235/5445 , C04B38/0054 , C04B38/0074 , C04B38/0645 , C04B38/068
摘要： The present invention describes a high porosity (% P≧45%), refractory, ceramic article comprising a cordierite ceramic phase and at least about 0.1 wt. % of a rare earth oxide, such as yttrium oxide or lanthanum oxide. When compared to typical high-porosity cordierite articles, the articles of the present invention may exhibit relatively high strength, relatively low microcracking, relatively high strain tolerance (MOR/E), and/or relatively high thermal shock resistance (TSP).
摘要翻译： 本发明描述了包含堇青石陶瓷相的至少约0.1重量％的高孔隙率（％P≥45％）的难熔陶瓷制品。 ％的稀土氧化物，例如氧化钇或氧化镧。 当与典型的高孔隙率堇青石制品相比时，本发明的制品可以表现出相对较高的强度，较低的微裂纹，较高的应变公差（MOR / E）和/或较高的耐热冲击性（TSP）。
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7.发明申请High porosity ceramic honeycomb article containing rare earth oxide and method of manufacturing same 有权含有稀土氧化物的高孔隙率陶瓷蜂窝体及其制造方法公开(公告)号：US20120177875A1
公开(公告)日：2012-07-12
申请号：US11823580
申请日：2007-06-28
IPC分类号： B32B3/12 , C04B35/195 , C04B35/64
CPC分类号： C04B35/195 , C04B38/0006 , C04B2111/00793 , C04B2111/0081 , C04B2111/2084 , C04B2111/32 , C04B2111/343 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3445 , C04B2235/349 , C04B2235/52 , C04B2235/5436 , C04B2235/5445 , C04B38/0054 , C04B38/0074 , C04B38/0645 , C04B38/068
摘要： The present invention describes a high porosity (% P≧45%), refractory, ceramic article comprising a cordierite ceramic phase and at least about 0.1 wt.% of a rare earth oxide, such as yttrium oxide or lanthanum oxide. When compared to typical high-porosity cordierite articles, the articles of the present invention may exhibit relatively high strength, relatively low microcracking, relatively high strain tolerance (MOR/E), and/or relatively high thermal shock resistance (TSP).
摘要翻译： 本发明描述了包含堇青石陶瓷相和至少约0.1重量％的稀土氧化物如氧化钇或氧化镧的高孔隙率（％P≥45％）的难熔陶瓷制品。 当与典型的高孔隙率堇青石制品相比时，本发明的制品可以表现出相对较高的强度，较低的微裂纹，较高的应变公差（MOR / E）和/或较高的耐热冲击性（TSP）。
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8.发明授权公开(公告)号：US07648550B2
公开(公告)日：2010-01-19
申请号：US11510227
申请日：2006-08-25
CPC分类号： C04B35/195 , B01D46/2425 , B01D46/2429 , B01D46/244 , B01D46/2444 , B01D2046/2433 , B01D2046/2437 , B01D2046/2496 , C04B38/0009 , C04B2111/00793 , C04B38/00 , C04B38/0054 , C04B38/0074
摘要： Disclosed are ceramic honeycomb articles, which are composed predominately of a crystalline phase cordierite composition. The ceramic honeycomb articles possess a microstructure characterized by a unique combination of relatively high total porosity of less than 54%, and relatively narrow pore size distribution having a d10 pore diameter of not less than 8 μm, a d90 pore diameter of not greater than 35 μm, and a value of df=(d50−d10)/d50 of less than 0.50. The articles exhibit high thermal durability and high filtration efficiency coupled with low pressure drop across the filter. Such ceramic articles are particularly well suited for filtration applications, such as diesel exhaust filters or DPFs. Also disclosed are methods for manufacturing the ceramic articles of the present invention.
摘要翻译： 公开了主要由结晶相堇青石组合物组成的陶瓷蜂窝体制品。 陶瓷蜂窝体制品具有微结构，其特征在于具有小于54％的相对高的总孔隙率和d10孔径不小于8μm的相对窄的孔径分布，d90孔径不大于35的独特组合 妈妈，df =（d50-d10）/ d50的值小于0.50。 该制品表现出高热耐久性和高过滤效率以及过滤器两端的低压降。 这种陶瓷制品特别适用于过滤应用，例如柴油机排气过滤器或DPF。 还公开了用于制造本发明的陶瓷制品的方法。
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9.发明授权公开(公告)号：US07618699B2
公开(公告)日：2009-11-17
申请号：US11823673
申请日：2007-06-28
申请人： Douglas Munroe Beall , Isabelle Marie Melscoet-Chauvel , Gregory Albert Merkel , Tinghong Tao , David John Thompson
发明人： Douglas Munroe Beall , Isabelle Marie Melscoet-Chauvel , Gregory Albert Merkel , Tinghong Tao , David John Thompson
CPC分类号： C04B35/195 , C04B35/62665 , C04B38/0009 , C04B2111/00793 , C04B2111/0081 , C04B2111/2084 , C04B2111/343 , C04B2111/346 , C04B2235/3206 , C04B2235/3217 , C04B2235/3218 , C04B2235/3222 , C04B2235/3418 , C04B2235/3445 , C04B2235/3463 , C04B2235/3472 , C04B2235/349 , C04B2235/36 , C04B2235/5436 , C04B2235/656 , C04B2235/6567 , C04B2235/80 , C04B2235/96 , Y10T428/24149 , Y10T428/249953 , C04B38/0054 , C04B38/0074 , C04B38/067 , C04B38/068
摘要： Substantially non-microcracked, porous, cordierite ceramic honeycomb bodies are provided. Although exhibiting moderately high thermal expansion (CTE) between 7×10−7 to 16×10−7/° C. (25-800° C.), the honeycomb bodies exhibit relatively high thermal shock parameter (TSP), such as TSR≧525° C. by virtue of a high MOR/E ratio, and/or low Eratio=ERT/E1000° C. and well interconnected porosity, as witnessed by a relatively high pore connectivity factor (PCF). A method of manufacturing the honeycomb ceramic structure is also provided.
摘要翻译： 提供了基本上非微裂纹，多孔的堇青石陶瓷蜂窝体。 尽管在7×10-7至16×10-7 /℃（25-800℃）之间呈现适度高的热膨胀（CTE），但蜂窝体表现出相对较高的热冲击参数（TSP），如TSR> = 525° 通过较高的MOR / E比率和/或较低的Eratio = ERT / E1000℃，以及良好相互连接的孔隙度，如通过较高的孔连通因子（PCF）所见。 还提供了一种蜂窝陶瓷结构体的制造方法。
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公开(公告)号：US07947355B2
公开(公告)日：2011-05-24
申请号：US11897108
申请日：2007-08-29
CPC分类号： C04B35/195 , C04B35/185 , C04B35/481 , C04B35/565 , C04B38/0006 , C04B2111/00793 , C04B2111/2084 , C04B2111/343 , C04B2235/36 , C04B2235/365 , Y10T428/24149 , C04B35/48 , C04B38/0074
摘要： A thermally shock resistant ceramic body, such as a porous ceramic honeycomb structure for a wall flow diesel engine exhaust filter or a flow-through ceramic catalyst support, is formed of a composite ceramic material comprising a major first ceramic phase exhibiting good thermal shock resistance and a minor second phase material that substantially reduces the elastic modulus of the composite ceramic material at elevated temperatures.
摘要翻译： 一种耐热冲击陶瓷体，例如用于壁流式柴油发动机排气过滤器或流通式陶瓷催化剂载体的多孔陶瓷蜂窝结构体，由复合陶瓷材料形成，该复合陶瓷材料包括具有良好耐热冲击性的主要第一陶瓷相和 一种次要的第二相材料，其在升高的温度下大大降低了复合陶瓷材料的弹性模量。
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