IN LINE, CONTINUOUS PROPPANT COATING METHOD

    公开(公告)号:US20220025249A1

    公开(公告)日:2022-01-27

    申请号:US17296871

    申请日:2019-12-06

    IPC分类号: C09K8/80 C09K8/70

    摘要: A continuous process for forming a coated proppant, said process comprising the steps of: (a) washing particles, (b) drying the particles at a first predetermined temperature, (c) cooling the particles, (d) feeding the cooled particles with a second predetermined temperature lower than the first predetermined temperature to an inlet of a combined continuous mixer and conveyor unit, (e) feeding a coating composition into the combined continuous mixer and conveyor unit, (f) mixing and simultaneously conveying the particles and the coating composition for a predetermined time, (g) curing the coating composition by transfer of heat from the particles, (h) discharging the coated particles from an outlet of the combined continuous mixer and conveyor unit, wherein said process does not comprise a step of heating the particles after the drying.

    PROCESS FOR MAKING URETHANE-ISOCYANURATES
    5.
    发明申请
    PROCESS FOR MAKING URETHANE-ISOCYANURATES 审中-公开
    制备尿素异构体的方法

    公开(公告)号:US20160122582A1

    公开(公告)日:2016-05-05

    申请号:US14896444

    申请日:2014-07-09

    摘要: A method for exposing a substrate to water under superatmospheric pressure at a temperature of at least 70° C. includes (a) applying a reaction mixture to a substrate, which reaction mixture has an isocyanate index of at least 10 and includes an aromatic polyisocyanate component, a polyol component having a polyol with a hydroxyl equivalent weight of at least 500, and a catalyst component having an isocyanate trimerization catalyst, and at least partially curing the reaction mixture to form a polyisocyanurate or polyurethane-isocyanurate polymer having a glass transition temperature of at least 80° C., and (b) exposing the substrate and the polyisocyanurate or polyurethane-isocyanurate polymer to water under superatmospheric pressure at a temperature of at least 70° C.

    摘要翻译: 一种在超过大气压下在至少70℃的温度下将基材暴露于水的方法包括(a)将反应混合物施加到基材上,该反应混合物的异氰酸酯指数至少为10,并且包括芳族多异氰酸酯组分 具有羟基当量重量至少为500的多元醇的多元醇组分和具有异氰酸酯三聚催化剂的催化剂组分,并且至少部分固化该反应混合物以形成玻璃化转变温度为的聚异氰脲酸酯或聚氨酯 - 异氰脲酸酯聚合物 至少80℃,和(b)在超大气压下在至少70℃的温度下将基材和聚异氰脲酸酯或聚氨酯 - 异氰脲酸酯聚合物暴露于水中。

    Process for Making Urethane-Isocyanates
    7.
    发明申请
    Process for Making Urethane-Isocyanates 有权
    制备聚氨酯 - 异氰酸酯的方法

    公开(公告)号:US20160002496A1

    公开(公告)日:2016-01-07

    申请号:US14763517

    申请日:2014-03-21

    IPC分类号: C09D175/08

    摘要: Polyisocyanurate or polyurethane-isocyanurate polymers are made by curing an aromatic polyisocyanate or a mixture of at least one aromatic polyisocyanate and at least one polyol having a hydroxyl equivalent weight of up to 200 in which the isocyanate index is at least 2.00, in the presence of at least one isocyanate trimerization catalyst, to form a polyisocyanurate or polyurethane-isocyanurate polymer having a glass transition temperature of at least 100° C., and then exposing the polyisocyanurate or polyurethane-isocyanurate polymer formed step a) to water under superatmospheric pressure at a temperature of at least 70° C.

    摘要翻译: 聚异氰脲酸酯或聚氨酯 - 异氰脲酸酯聚合物是通过将芳族多异氰酸酯或至少一种芳族多异氰酸酯与至少一种羟基当量重量至多为200的多元醇(其中异氰酸酯指数为至少2.00)的混合物在 至少一种异氰酸酯三聚催化剂,以形成玻璃化转变温度为至少100℃的聚异氰脲酸酯或聚氨酯 - 异氰脲酸酯聚合物,然后在超大气压下将形成步骤a)的聚异氰脲酸酯或聚氨酯 - 异氰脲酸酯聚合物暴露于水中, 温度至少为70℃

    TIN FREE SILYL-TERMINATED POLYMERS
    8.
    发明申请

    公开(公告)号:US20150011722A1

    公开(公告)日:2015-01-08

    申请号:US14496269

    申请日:2014-09-25

    摘要: Embodiments of the invention provide for methods of producing a composition comprising a crosslinkable silane-terminated polymer having at least one crosslinkable silyl group in each molecule. The method comprises providing a polymer having at least one unsaturated group and at least one alcoholic hydroxyl group in each molecule, adding to the polymer a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule and a hydrosilylation catalyst to thereby carry out a hydrosilylation reaction to form a composition comprising hydrosilylated polyoxyalkylene polymers, reacting the hydrosilylated polyoxyalkylene polymers with at least one isocyanate in the presence of a first tin-free catalyst to form an isocyanate reacted hydrosilylated polymer, and optionally reacting the isocyanate reacted hydrosilylated polymer with a polyol having a nominal functionality of at least 2 to form a polyol reacted crosslinkable silane-terminated polymer.

    摘要翻译: 本发明的实施方案提供了制备包含在每个分子中具有至少一个可交联甲硅烷基的可交联的硅烷端基聚合物的组合物的方法。 该方法包括在每个分子中提供具有至少一个不饱和基团和至少一个醇羟基的聚合物,向该聚合物中加入每个分子中具有氢 - 硅键和交联性甲硅烷基的化合物和氢化硅烷化催化剂从而携带 进行氢化硅烷化反应以形成包含氢化硅烷化聚氧化烯聚合物的组合物,在第一无锡催化剂存在下使氢化硅烷化聚氧化烯聚合物与至少一种异氰酸酯反应,以形成异氰酸酯反应的氢化硅烷化聚合物,并任选地使异氰酸酯反应的硅烷化聚合物与 具有至少2的标称官能度的多元醇以形成多元醇反应的可交联的硅烷封端的聚合物。

    Coated Proppants
    9.
    发明申请

    公开(公告)号:US20220275270A1

    公开(公告)日:2022-09-01

    申请号:US17630808

    申请日:2020-04-30

    IPC分类号: C09K8/80 C09K8/88

    摘要: Coated proppant particles are prepared by coating the particles with at least one polyisocyanate, and at least one urethane catalyst, and starch is present during at least part of the curing step. The starch becomes incorporated into in at least a portion of the cured coating. The coating cures rapidly at moderate temperatures, and bonds to itself well under conditions of heat and pressure as are experienced by the particles in subterranean formations.