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公开(公告)号：US06863925B1
公开(公告)日：2005-03-08
申请号：US09670189
申请日：2000-09-26
CPC分类号： C23C10/02 , C23C10/14 , C23C16/08 , C23C28/021 , C23C28/028 , C23C28/321 , C23C28/325 , C23C28/345 , C23C28/3455 , Y02T50/67
摘要： An article is coasted by preparing a coating source having an aluminum halide, a fluoride or an iodide of a modifying element as a source of the modifying element, and a carrier gas. The modifying element is zirconium, hafnium, and yttrium, or combinations thereof. The coating source is contacted to the article, and the coating source and the article are heated to a coating temperature of at least about 1850° F. for a period of time sufficient to permit aluminum and the modifying element to coat onto the surface of the article. The preferred fluorides of modifying elements are zirconium tetrafluoride and hafnium tetrafluoride.
摘要翻译： 通过制备具有改性元素的卤化铝，氟化物或碘化物作为改性元素的来源的涂料源和载气来制备物品。 改性元素是锆，铪和钇，或其组合。 将涂料源与制品接触，并将涂料源和制品加热至至少约1850°F的涂布温度一段足以允许铝和改性元素涂覆在表面上的时间 文章。 改性元素的优选氟化物是四氟化锆和四氟化铪。
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公开(公告)号：US06682827B2
公开(公告)日：2004-01-27
申请号：US10029320
申请日：2001-12-20
IPC分类号： B32B1504
CPC分类号： C23C28/321 , B32B15/01 , B32B15/013 , C22C19/03 , C23C14/16 , C23C28/345 , C23C28/3455 , C23C30/00 , Y10T428/1259 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/1275 , Y10T428/12861 , Y10T428/12875 , Y10T428/12944
摘要： A protective overlay coating for articles used in hostile thermal environments, and particularly for use as a bond coat for a thermal barrier coating deposited on the coating. The coating is predominantly beta-phase NiAl into which a platinum-group metal is incorporated, yielding a coating system capable of exhibiting improved spallation resistance as compared to prior bond coat materials containing platinum, must notably the platinum aluminide diffusion coatings. A preferred composition for the beta-phase NiAl overlay coating further contains chromium and zirconium or hafnium.
摘要翻译： 用于敌对热环境中用于制品的保护性覆盖涂层，特别用作沉积在涂层上的热障涂层的粘合涂层。 涂层主要是其中掺入铂族金属的β相NiAl，与现有的包含铂的粘结涂层材料相比，产生能够表现出改善的抗剥落性的涂层体系，必须特别是铂铝化物扩散涂层。 用于β相NiAl覆盖涂层的优选组合物还含有铬和锆或铪。
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公开(公告)号：US06663983B1
公开(公告)日：2003-12-16
申请号：US10064562
申请日：2002-07-26
IPC分类号： B32B1504
CPC分类号： C23C28/3215 , C23C14/083 , C23C28/321 , C23C28/345 , C23C28/3455 , F01D5/288 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/25
摘要： A thermal barrier coating (TBC) (26) for a component (10) intended for use in a hostile environment, such as the superalloy turbine, combustor and augmentor components of a gas turbine engine. The TBC (26) is formed of at least partially stabilized zirconia, preferably yttria-stabilized zirconia (YSZ), and exhibits improved strength and fracture toughness as a result of containing a dispersion of chromia precipitates or particles (32). The TBC (26) preferably consists essentially of YSZ and the chromia particles (32), which are preferably dispersed throughout the microstructure of the TBC (26), including the YSZ grains (30) and grain boundaries. The chromia particles (32) constitute at least 1 to about 10 volume percent of the TBC (26).
摘要翻译： 用于在敌对环境中使用的组件（10）的隔热涂层（TBC）（26），例如燃气涡轮发动机的超级合金涡轮机，燃烧器和增压器部件。 TBC（26）由至少部分稳定的氧化锆，优选氧化钇稳定的氧化锆（YSZ）形成，并且由于含有氧化铬析出物或颗粒（32）的分散体而显示出改善的强度和断裂韧性。 TBC（26）优选基本上由YSZ和氧化铬颗粒（32）组成，其优选分散在包括YSZ晶粒（30）和晶界的TBC（26）的整个微结构中。 氧化铁颗粒（32）构成TBC（26）的至少1至约10体积％。
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公开(公告)号：US06586115B2
公开(公告)日：2003-07-01
申请号：US09833446
申请日：2001-04-12
IPC分类号： B32B1504
CPC分类号： F01D5/288 , C04B35/486 , C04B2235/3206 , C04B2235/3208 , C04B2235/3213 , C04B2235/3215 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3229 , C04B2235/3272 , C04B2235/3275 , C04B2235/3279 , C04B2235/787 , C04B2235/80 , C04B2235/85 , C23C28/00 , C23C30/00 , F05D2300/134 , F05D2300/5024 , Y10T29/49922 , Y10T428/12611 , Y10T428/12618 , Y10T428/249956
摘要： A thermal barrier coating (TBC) for a component intended for use in a hostile environment, such as the superalloy turbine, combustor and augmentor components of a gas turbine engine. The TBC is formed of zirconia that is partially stabilized with yttria (YSZ), preferably not more than 3 weight percent yttria, and to which one or more additional metal oxides are alloyed to increase crystallographic defects and lattice strains in the TBC grains and/or form precipitates of zirconia and/or compound(s) of zirconia and/or yttria and the additional metal oxide(s), the inclusion of which reduces the thermal conductivity of the YSZ to levels lower than conventional 6-8% YSZ. Improvements are particularly contemplated for TBC having a columnar grain structure, such as those deposited by EBPVD and other PVD techniques.
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5.发明授权公开(公告)号：US06533875B1
公开(公告)日：2003-03-18
申请号：US09693077
申请日：2000-10-20
IPC分类号： B05D722
CPC分类号： C23C28/321 , C23C10/18 , C23C10/26 , C23C10/30 , C23C10/48 , C23C10/52 , C23C10/56 , C23C28/3215 , C23C28/325 , C23C28/345 , C23C28/3455 , Y02T50/67
摘要： A surface of a nickel-base article such as an internal surface of a gas turbine airfoil is protected with a donor layer of aluminum and at least one other element. To form the protective layer, a donor alloy is contacted to the protected surface of the article, and simultaneously the article and the donor alloy are heated to a coating temperature that is greater than about 0.7 of the absolute solidus temperature of the donor alloy but is such that the donor alloy remains in the form of a condensed phase contacting the protected surface of the article. The donor alloy is thereafter interdiffused into the protected surface of the article.
摘要翻译： 诸如燃气轮机翼型件的内表面的镍基制品的表面由铝的供体层和至少一个其它元件保护。 为了形成保护层，供体合金与制品的被保护表面接触，并且同时将制品和供体合金加热至比供体合金的绝对固相线温度大约0.7的涂层温度，但是 使得供体合金保持为与受保护的表面接触的凝聚相的形式。 然后，供体合金相互扩散到制品的受保护表面。
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公开(公告)号：US20120282485A1
公开(公告)日：2012-11-08
申请号：US13545625
申请日：2012-07-10
申请人： Benard Patrick Bewlay , Pazhayannur Ramanathan Subramanian , Joseph David Rigney , Richard Didomizio , Voramon Supatarawanich Dheeradhada
发明人： Benard Patrick Bewlay , Pazhayannur Ramanathan Subramanian , Joseph David Rigney , Richard Didomizio , Voramon Supatarawanich Dheeradhada
CPC分类号： C22C27/02 , B32B15/01 , C22C27/06 , C22C30/00 , C23C10/26 , C23C10/28 , C23C14/0682 , C23C14/5806 , C23C30/00 , F01D5/286 , F05D2230/90 , F05D2260/95 , F05D2300/502 , Y02T50/67 , Y02T50/672 , Y10T428/12361 , Y10T428/12611 , Y10T428/12819
摘要： Coatings suitable for use as protective oxide-forming coatings on Nb-based substrates exposed to high temperatures and oxidative environments. The coatings contain chromium and/or molybdenum, preferably contains silicon, and optionally contains niobium, titanium, hafnium, iron, rhenium, tantalum, and/or tungsten, which in combination form multiple intermetallic phases, which in combination form one or more intermetallic phases that promote the formation of a slow-growing oxide scale. Depending on the particular coating composition, the intermetallic phases maybe: a silicon-modified Cr2Nb Laves phase and optionally a chromium solid solution phase, a CrNbSi intermetallic phase, and/or an M3Si intermetallic phase where M is niobium, titanium, and/or chromium; or M5Si3, MSi2 and/or M3Si2 where M is molybdenum, niobium, titanium, chromium, hafnium, iron, rhenium, tantalum, and/or tungsten.
摘要翻译： 适用于暴露于高温和氧化环境的Nb基基底上的保护性氧化物形成涂层的涂料。 涂层含有铬和/或钼，优选含有硅，并且任选地包含铌，钛，铪，铁，铼，钽和/或钨，其组合形成多个金属间相，其组合形成一个或多个金属间相 促进形成缓慢生长的氧化皮。 根据具体的涂层组成，金属间化合物相可以是硅改性的Cr 2 Nb Laves相和任选的铬固溶体相，CrNbSi金属间相和/或M3Si金属间相，其中M是铌，钛和/或铬 ; 或M5Si3，MSi2和/或M3Si2，其中M是钼，铌，钛，铬，铪，铁，铼，钽和/或钨。
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公开(公告)号：US08247085B2
公开(公告)日：2012-08-21
申请号：US12275785
申请日：2008-11-21
申请人： Bernard Patrick Bewlay , Pazhayannur Ramanathan Subramanian , Joseph David Rigney , Richard DiDomizio , Voramon Supatarawanich Dheeradhada
发明人： Bernard Patrick Bewlay , Pazhayannur Ramanathan Subramanian , Joseph David Rigney , Richard DiDomizio , Voramon Supatarawanich Dheeradhada
CPC分类号： C22C27/02 , B32B15/01 , C22C27/06 , C22C30/00 , C23C10/26 , C23C10/28 , C23C14/0682 , C23C14/5806 , C23C30/00 , F01D5/286 , F05D2230/90 , F05D2260/95 , F05D2300/502 , Y02T50/67 , Y02T50/672 , Y10T428/12361 , Y10T428/12611 , Y10T428/12819
摘要： Coatings suitable for use as protective oxide-forming coatings on Nb-based substrates exposed to high temperatures and oxidative environments. The coatings contain chromium and/or molybdenum, preferably contains silicon, and optionally contains niobium, titanium, hafnium, iron, rhenium, tantalum, and/or tungsten, which in combination form multiple intermetallic phases, which in combination form one or more intermetallic phases that promote the formation of a slow-growing oxide scale. Depending on the particular coating composition, the intermetallic phases may be: a silicon-modified Cr2Nb Laves phase and optionally a chromium solid solution phase, a CrNbSi intermetallic phase, and/or an M3Si intermetallic phase where M is niobium, titanium, and/or chromium; or M5Si3, MSi2 and/or M3Si2 where M is molybdenum, niobium, titanium, chromium, hafnium, iron, rhenium, tantalum, and/or tungsten.
摘要翻译： 适用于暴露于高温和氧化环境的Nb基基底上的保护性氧化物形成涂层的涂料。 涂层含有铬和/或钼，优选含有硅，并且任选地包含铌，钛，铪，铁，铼，钽和/或钨，其组合形成多个金属间相，其组合形成一个或多个金属间相 促进形成缓慢生长的氧化皮。 根据特定的涂料组合物，金属间相可以是：硅改性的Cr 2 Nb Laves相和任选的铬固溶相，CrNbSi金属间相和/或M3Si金属间相，其中M是铌，钛和/或 铬; 或M5Si3，MSi2和/或M3Si2，其中M是钼，铌，钛，铬，铪，铁，铼，钽和/或钨。
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公开(公告)号：US06869508B2
公开(公告)日：2005-03-22
申请号：US10063808
申请日：2002-05-15
申请人： Ramgopal Darolia , Reed Roeder Corderman , Joseph David Rigney , Richard Arthur Nardi, Jr. , Michael James Weimer
发明人： Ramgopal Darolia , Reed Roeder Corderman , Joseph David Rigney , Richard Arthur Nardi, Jr. , Michael James Weimer
CPC分类号： B82Y10/00 , C23C14/16 , C23C14/246 , C23C14/30
摘要： A PVD process and apparatus (120) for depositing a coating (132) from multiple sources (110, 111) of different materials. The process and apparatus (120) are particulaity intended to deposit a beta-nickel aluminide coating (132) containing one or more elements whose vapor pressures are lower than NiAl. The PVD process and apparatus (120) entail feeding at least two materials (110, 111) into a coating chamber (122) and evaporating the materials (110, 111) at different rates from separate molten pools (114, 115) thereof. Articles (130) to be coated are suspended within the coating chamber (122), and transported with a support apparatus (118) relative to the two molten pools (114, 115) so as to deposit a coating (132) with a controlled composition that is a mixture of the first and second materials (110, 111).
摘要翻译： 一种用于从不同材料的多个源（110,111）沉积涂层（132）的PVD工艺和设备（120）。 该方法和装置（120）特别用于沉积含有一种或多种蒸气压低于NiAl的元素的β-镍铝化物涂层（132）。 PVD工艺和设备（120）需要将至少两种材料（110,111）进料到涂覆室（122）中并且以与其分离的熔池（114,115）不同的速率蒸发材料（110,111）。 待涂覆的制品（130）悬浮在涂覆室（122）内，并相对于两个熔池（114,115）用支撑装置（118）运输，以便沉积具有受控组合物的涂层（132） 即第一和第二材料（110,111）的混合物。
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9.发明授权Article protected by a diffusion aluminide coating applied by painting techniques 失效用喷涂技术涂覆的扩散铝化物涂层进行保护公开(公告)号：US06676992B2
公开(公告)日：2004-01-13
申请号：US09934752
申请日：2001-08-22
申请人： Jeffrey Allan Pfaendtner , Michael James Weimer , William Evan McCormack , Joseph David Rigney , Mark Lloyd Miller , John Lewis Lackman
发明人： Jeffrey Allan Pfaendtner , Michael James Weimer , William Evan McCormack , Joseph David Rigney , Mark Lloyd Miller , John Lewis Lackman
IPC分类号： B05D302
摘要： A method for coating an article includes preparing a coating precursor paint including aluminum-containing pigment particles, a temporary organic binder comprising an acrylic, and a solvent for the temporary organic binder. The coating precursor paint is applied to a surface of the article and thereafter heated to a temperature of from about 1200° F. to about 2100° F. in a non-oxidizing environment.
摘要翻译： 一种涂布物品的方法包括制备包括含铝颜料颗粒的涂料前体涂料，包含丙烯酸的临时有机粘合剂和用于临时有机粘合剂的溶剂。 将涂层前体涂料施加到制品的表面，然后在非氧化环境中加热至约1200°F至约2100°F的温度。
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公开(公告)号：US06544665B2
公开(公告)日：2003-04-08
申请号：US09765228
申请日：2001-01-18
IPC分类号： B32B1504
CPC分类号： C23C14/083 , C23C28/321 , C23C28/3215 , C23C28/323 , C23C28/325 , C23C28/345 , C23C28/3455 , C23C30/00 , Y10T428/12549 , Y10T428/1259 , Y10T428/12618 , Y10T428/249953 , Y10T428/26 , Y10T428/268
摘要： A thermal barrier coating (TBC) for a component intended for use in a hostile environment, such as the superalloy turbine, combustor and augmentor components of a gas turbine engine. The TBC is formed to contain small amounts of alumina precipitates dispersed throughout the grain boundaries and pores of the TBC to getter oxide impurities that would otherwise allow or promote grain sintering and coarsening and pore coarsening, the consequence of which would be densification of the TBC and therefore increased thermal conductivity. If sufficiently fine, the precipitates also serve to pin the grains and pore boundaries of the TBC, the effect of which is to reduce the tendency for the microstructure of the TBC to sinter, coarsen and undergo pore redistribution, which also increase thermal conductivity of the TBC 26.
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