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    Polyisocyanate suspensions in isocyanate reactive compounds and their use
    4.
    发明授权
    Polyisocyanate suspensions in isocyanate reactive compounds and their use 失效
    异氰酸酯反应性化合物中的聚异氰酸酯悬浮体及其用途

    公开(公告)号：US5185422A

    公开(公告)日：1993-02-09

    申请号：US862854

    申请日：1992-04-03

    申请人： Werner Drouve ,  Peter Hohlein ,  Wolfhart Wieczorrek

    发明人： Werner Drouve ,  Peter Hohlein ,  Wolfhart Wieczorrek

    IPC分类号： B60R13/06 ,  C08G18/48 ,  C08G18/70 ,  C08G18/78 ,  C08G18/79 ,  C08G18/80 ,  C09D175/00 ,  C09D175/04 ,  C09J175/00 ,  C09J175/04 ,  C09K3/10

    CPC分类号： C08G18/4891 ,  C08G18/707 ,  C08G18/7825 ,  C08G18/798 ,  C08G18/8038 ,  C08G2190/00 ,  Y10S528/903

    摘要： Suspensions of solid polyisocyanates inactivated on the surface of adduct formation in organic, isocyanate reactive compounds as continuous phase, which suspensions are stable in storage at room temperature and heat curable and optionally contain auxiliary agents and additives, the continuous phase containing at least 10% by weight of ether group- and ester group-containing polyhydroxyl compounds having an (average) hydroxyl functionality of from 0.5 to 3 and an (average) hydroxyl number of from 15 to 150 constituting esterification products of (i) polyether polyols having an (average) hydroxyl functionality of from 3 to 8 and an (average) hydroxyl number of from 200 to 1000 with (ii) from 40 to 90 equivalents percent of inorganic monocarboxylic acids and the use of these suspensions for the production of coatings, adhesives or sealing compounds, in particular as underseal and doorseal compounds for motor vehicles.

    摘要翻译： 固体多异氰酸酯的悬浮液在有机异氰酸酯反应性化合物的连接相上在加合物形成的表面上失活，该悬浮液在室温下储存稳定并且可热固化并且任选地含有助剂和添加剂，连续相含有至少10％ （平均）羟基官能度为0.5〜3，（平均）羟基数为15〜150的含醚基和酯基的多羟基化合物的重量构成（i）具有（平均）羟基官能度的聚醚多元醇的酯化产物， 羟基官能度为3至8，（平均）羟基数为200至1000，（ii）40至90当量无机一元羧酸，以及这些悬浮液用于生产涂料，粘合剂或密封剂的用途， 特别是用于机动车辆的下侧和门锁化合物。

    Powder coating compositions containing polyurethanes having (meth)acryloyl groups as binders
    5.
    发明授权
    Powder coating compositions containing polyurethanes having (meth)acryloyl groups as binders 失效
    含有（甲基）丙烯酰基作为粘合剂的聚氨酯的粉末涂料组合物

    公开(公告)号：US5068305A

    公开(公告)日：1991-11-26

    申请号：US556223

    申请日：1990-07-20

    申请人： Jurgen Meixner ,  Josef Pedain ,  Peter Hohlein ,  Hans-Joachim Kreuder

    发明人： Jurgen Meixner ,  Josef Pedain ,  Peter Hohlein ,  Hans-Joachim Kreuder

    IPC分类号： C08F299/00 ,  C08F290/00 ,  C08F299/06 ,  C08G18/67 ,  C08G18/81 ,  C09D5/03 ,  C09D5/46 ,  C09D175/14 ,  C09D175/16

    CPC分类号： C09D175/16 ,  C08F299/06 ,  C08G18/8175 ,  C08G2150/20

    摘要： The present invention relates to powder coating compositions which can be cured in the presence of heat and/or high energy radiation and contain polyurethanes which melt at temperatures of 50.degree. to 180.degree. C., have 3 to 10% by weight of olefinic double bonds in the form of (meth)acryloyl groups (calculated as .dbd.C.dbd.C.dbd., molecular weight=24) and are based on the reaction product ofA) 40 to 80 parts by weight of one or more organic polyisocyanates withB) 15 to 50 parts of weight of one or more monohydric alcohols containing (meth)acryloyl groups andC) 2 to 20 parts by weight one or more compounds which are free from (meth)acryloyl groups and contain isocyanate reactive groups.

    摘要翻译： 本发明涉及粉末涂料组合物，其可以在热和/或高能量辐射的存在下固化，并且包含在50-180℃的温度下熔化的聚氨酯，具有3至10重量％的烯属双键 以（甲基）丙烯酰基的形式（以C = C =分子量= 24计算），并且基于A）的反应产物：40至80重量份的一种或多种有机多异氰酸酯与B）15至 50重量份的一种或多种含（甲基）丙烯酰基的一元醇和C）2至20重量份的一种或多种不含（甲基）丙烯酰基并含有异氰酸酯反应性基团的化合物。

    Storable, saponification-resistant aqueous lacquer binders
    6.
    发明授权
    Storable, saponification-resistant aqueous lacquer binders 失效
    可储存，可皂化的水性漆粘合剂

    公开(公告)号：US4410663A

    公开(公告)日：1983-10-18

    申请号：US377625

    申请日：1982-05-13

    申请人： Peter Hohlein ,  Jochen Schoeps

    发明人： Peter Hohlein ,  Jochen Schoeps

    IPC分类号： C08L33/06 ,  C08L33/04 ,  C08L61/20 ,  C09D125/14 ,  C09D133/04 ,  C09D161/20 ,  C08L61/28

    CPC分类号： C09D125/14 ,  C08L61/20

    摘要： This invention relates to lacquer binders which can be diluted with water, consisting of a mixture of:A. 50-94% by weight, preferably 55-80% by weight of a copolymer consisting of copolymerized units ofa. 30-65% by weight of an aromatic vinyl or isopropenyl compound having 8-14 C-atoms or of a methacrylic acid alkyl ester having 1-4 C-atoms in the alcohol component or mixtures thereof,b. 10-30% by weight of at least one acrylic acid alkyl ester having 1-8 C-atoms in the alcohol component,c. 1-20% by weight of maleic acid, fumaric acid, itaconic acid or semiesters thereof having 1-8 C-atoms in the alcohol component, or (meth)acrylic acid or mixtures of the aforesaid monomers,d. 0-20% by weight of at least one hydroxyalkyl ester of (meth)acrylic acid having 2-4 C-atoms in the alkyl group or glycidyl (meth)acrylate or mixtures of the aforesaid monomers,e. 10-30% by weight of N-methylol(meth)acrylic acid amide or N-methoxymethyl (meth)acrylic acid amide, preferably N-methoxymethyl(meth)acrylic acid amide, andf. 2-40% by weight of a reaction product of an allyl glycidyl ether and aliphatic, cycloaliphatic, araliphatic or aromatic monocarboxylic acid having 2-30 C-atoms or mixtures thereof, preferably saturated aliphatic branched chain monocarboxylic acids having 5-20 C-atoms, in particular .alpha.-ethyl-hexanoic acid isononanoic acid; andB. 6-50% by weight, preferably 20 to 55% by weight of an aminoplast resin; andC. 0-30% by weight, based on the copolymer, of a lactam, 30-100% of the number of carboxyl groups of component A.c. incorporated in the copolymer being neutralised by ammonia or mono- or polyamines.

    摘要翻译： 本发明涉及可用水稀释的漆粘合剂，其由以下混合物组成：A.50-94重量％，优选55-80重量％的由共聚单元组成的共聚物。 b）在醇组分或其混合物中含有30-65重量％的具有8-14个碳原子的芳族乙烯基或异丙烯基化合物或具有1-4个C原子的甲基丙烯酸烷基酯。 10-30重量％的至少一种在醇组分中具有1-8个C原子的丙烯酸烷基酯，c。 1-20重量％的在醇组分中具有1-8个碳原子的马来酸，富马酸，衣康酸或其半酯或（甲基）丙烯酸或上述单体的混合物，d。 0-20重量％的至少一种在烷基中具有2-4个C原子的（甲基）丙烯酸的羟烷基酯或（甲基）丙烯酸缩水甘油酯或上述单体的混合物， 10-30重量％的N-羟甲基（甲基）丙烯酸酰胺或N-甲氧基甲基（甲基）丙烯酸酰胺，优选N-甲氧基甲基（甲基）丙烯酸酰胺，和f。 2-40重量％的烯丙基缩水甘油醚与具有2-30个碳原子的脂族，脂环族，芳脂族或芳族一元羧酸或其混合物的反应产物，优选具有5-20个C原子的饱和脂肪族支链单羧酸 ，特别是α-乙基 - 己酸异壬酸; 和B. 6-50重量％，优选20至55重量％的氨基塑料树脂; 和基于共聚物的0-30重量％的内酰胺，30-100重量份的组分A.c.的羧基数。 掺入共聚物中被氨或单胺或多胺中和。

    Aqueous binder composition and a process for its preparation
    7.
    发明授权
    Aqueous binder composition and a process for its preparation 失效
    水性粘合剂组合物及其制备方法

    公开(公告)号：US5387642A

    公开(公告)日：1995-02-07

    申请号：US7219

    申请日：1993-01-22

    申请人： Harald Blum ,  Werner Kubitza ,  Peter Hohlein

    发明人： Harald Blum ,  Werner Kubitza ,  Peter Hohlein

    IPC分类号： C08G18/08 ,  C08G18/10 ,  C08G18/12 ,  C08G18/66 ,  C08J3/20 ,  C08K3/20 ,  C08L51/00 ,  C08L67/00

    CPC分类号： C08G18/6659 ,  C08G18/0823 ,  C08G18/10 ,  C08G18/12 ,  C08G2190/00

    摘要： This invention relates to an aqueous binder composition containingA) an aqueous solution or dispersion of an organic polyol component which can be diluted with water and contains at least one polyester resin containing urethane, carboxylate and hydroxyl groups andB) a polyisocyanate component which has a viscosity of 50 to 10,000 mPa.s at 23.degree. C. and contains at least one organic polyisocyanate which is present as an emulsion in component A),wherein the NCO/OH equivalent ratio, based on the isocyanate groups of component B) and the hydroxyl groups of the polyol component present in A), is 0.5:1 to 5:1.The invention also relates to a process for the preparation of these coating compositions by emulsifying a polyisocyanate component having a viscosity of 50 to 10,000 mPa.s at 23.degree. C. and containing at least one organic polyisocyanate in an aqueous solution or dispersion of a polyester resin containing urethane, carboxylate and hydroxyl groups in an sufficient to provide an an NCO/OH equivalent ratio, based on the isocyanate groups of the polyisocyanate component and the hydroxyl groups of the polyester resin, of 0.5:1 to 5:1.

    摘要翻译： 本发明涉及一种水性粘合剂组合物，其含有A）有机多元醇组分的水溶液或分散体，其可以用水稀释并含有至少一种含有氨基甲酸酯，羧酸酯和羟基的聚酯树脂，和B）多异氰酸酯组分，其具有 粘度在23℃为50至10,000mPa.s，并且含有至少一种有机多异氰酸酯，其作为组分A）中的乳液存在，其中基于组分B）的异氰酸酯基和NCO / OH当量比 存在于A）中的多元醇组分的羟基为0.5:1至5:1。 本发明还涉及一种制备这些涂料组合物的方法，该方法是在23℃下将粘度为50至10,000mPa.s的多异氰酸酯组分乳化并在聚酯的水溶液或分散体中含有至少一种有机多异氰酸酯 含有聚氨酯，羧酸酯和羟基的树脂，其量足以提供基于多异氰酸酯组分的异氰酸酯基团和聚酯树脂的羟基的NCO / OH当量比为0.5:1至5:1。

    New polyester polyols and their use as polyol component in two-component polyurethane lacquers
    9.
    发明授权
    New polyester polyols and their use as polyol component in two-component polyurethane lacquers 失效
    新型聚酯多元醇及其在双组分聚氨酯漆中作为多元醇成分的用途

    公开(公告)号：US4894430A

    公开(公告)日：1990-01-16

    申请号：US278056

    申请日：1988-11-30

    申请人： Peter Hohlein ,  Hans-Joachim Hofer ,  Josef Pedain ,  Manfred Schonfelder

    发明人： Peter Hohlein ,  Hans-Joachim Hofer ,  Josef Pedain ,  Manfred Schonfelder

    IPC分类号： C08F299/04 ,  C08F283/01 ,  C08G18/42 ,  C08G18/68 ,  C08G63/16 ,  C08G63/52 ,  C09D175/06

    CPC分类号： C08G18/686

    摘要： The present invention is directed to polyester polyols in the hydroxyl number range of about 80 to 250 which are based on reaction products of(a) about 52 to 60 mole % of a polyol component with(b) about 40 to 48 mole % of dicarboxylic acid component, characterized in that(a) the polyol component is based on (i) about 2 to 30 mole % of at least one dihydric aliphatic alcohol which has at least two carbon atoms and is different from neopentyl glycol, (ii) about 5 to 40 mole % of at least one aliphatic alcohol which is at least trihydric and has at least 3 carbon atoms, (iii) about 20 to 60 mole % of bis-(hydroxymethyl)-cyclohexane and (iv) about 10 to 50 mole % of neopentyl glycol, and(b) the dicarboxylic acid component is based on (v) about 50 to 99 mole % of at least one aliphatic, saturated dicarboxylic acid or an anhydride of such an acid containing at least 2 carbon atoms and (vi) about 0.5 to 50 mole % of at least one aliphatic unsaturated dicarboxylic acid or its anhydride having at least 4 carbon atoms,the percentages under (a) and (b) adding up to 100.The present invention is also directed to the use of these polyester polyols as a binder component for two-component polyurethane lacquers containing lacquer polyisocyanates for the production of lacquer coats on molded plastic parts.

    摘要翻译： 本发明涉及羟基数约80至250的聚酯多元醇，其基于（a）约52至60摩尔％的多元醇组分与（b）约40至48摩尔％的二羧酸的反应产物 酸组分，其特征在于（a）多元醇组分基于（i）约2至30摩尔％的至少一种具有至少两个碳原子且不同于新戊二醇的二元脂肪醇，（ii）约5摩尔％ 至少一种至少三个并且具有至少三个碳原子的脂族醇，（iii）约20至60摩尔％的双 - （羟甲基） - 环己烷和（iv）约10至50摩尔％ 的新戊二醇，和（b）二羧酸组分基于（v）约50至99摩尔％的至少一种脂族，饱和二羧酸或含有至少2个碳原子的酸的酸酐，和（vi） 约0.5至50摩尔％的至少一种脂肪族不饱和二羧酸或其酸酐ha 至少4个碳原子，（a）和（b）的百分数加到100上。本发明还涉及这些聚酯多元醇作为粘合剂组分用于含有漆多异氰酸酯的双组分聚氨酯漆的用途， 在模制塑料部件上生产漆面。

    Process for the preparation of (meth)acrylic acid esters and their use
    10.
    发明授权
    Process for the preparation of (meth)acrylic acid esters and their use 失效
    制备（甲基）丙烯酸酯的方法及其用途

    公开(公告)号：US4748269A

    公开(公告)日：1988-05-31

    申请号：US851742

    申请日：1986-04-14

    申请人： Jurgen Meixner ,  Josef Pedain ,  Peter Hohlein ,  Dieter Margotte

    发明人： Jurgen Meixner ,  Josef Pedain ,  Peter Hohlein ,  Dieter Margotte

    IPC分类号： C07C69/54 ,  C08F2/46 ,  C08F220/36 ,  C07C69/52

    CPC分类号： C07C69/54 ,  C07C67/08 ,  C07C67/60

    摘要： (Meth)acrylic acid esters can be prepared by acid-catalyzed reaction of (meth)acrylic acid with alcohols in a water-immiscible solvent. After the esterification, the reaction mixture is washed with aqueous solutions having an alkaline reaction and then reacted at elevated temperature with carbodiimides. Acid numbers below 0.5 (mg of KOH/g of substance) are obtained in this way. (Meth)acrylic acid esters are used, for example, as reactive diluents or as comonomers.

    摘要翻译： （甲基）丙烯酸酯可以通过（甲基）丙烯酸与醇在水不混溶溶剂中的酸催化反应来制备。 酯化后，反应混合物用碱性反应的水溶液洗涤，然后在高温下与碳二亚胺反应。 以这种方式获得酸值低于0.5（KOH / g的物质）。 （甲基）丙烯酸酯用作例如作为反应性稀释剂或共聚单体。