摘要:
The compound thiohumic acid resulting from replacing at least a part of the carboxyl groups in humic acid by thiocarboxyl groups, i.e., ##EQU1## as well as a heavy metal adsorbent containing thiohumic acid as its active ingredient. This new compound is obtained by treating humic acid with a halogenating agent to form humic acid halide and treating such halide with a thiolating agent.
摘要:
A method is provided for producing a weight-reduced FRP cylinder which can attain high strength, and also such an FRP cylinder is provided. This FRP cylinder producing method, in which a plurality of prepregs formed by impregnating reinforced fibers with thermosetting resin sheets are wound into a cylinder and thermally cured to be formed as a plurality of FRP layers, includes a simultaneous multilayer winding process in which a torsional rigidity retaining prepreg and a buckling prevention prepreg are continuously wound a plurality of turns with being layered on each other when the plurality of prepregs are wound into a cylinder, wherein the torsional rigidity retaining prepreg includes a layer of fibers oblique to a cylindrical axis direction of the FRP cylinder, and wherein the buckling prevention prepreg includes a layer of fibers orthogonal to the cylindrical axis direction.
摘要:
Disclosed is a method for producing a biphenyltetracarboxylic acid ester by oxidative coupling a phthalic acid ester by using a catalyst comprising at least a palladium salt, a copper salt and a β-dicarbonyl compound in the presence of a molecular oxygen, wherein the β-dicarbonyl compound is supplied into a reaction mixture liquid intermittently at an interval of less than 30 minutes, or continuously. This method allows, in particular, the selective and economical production of an asymmetric biphenyltetracarboxylic acid tetraester such as 2,3,3′,4′-biphenyltetracarboxylic acid tetraester.
摘要:
An object of the present invention is to provide a single-phase film of a metal sulfide with good quality, and a method for preparing a metal sulfide film at a low cost in a convenient manner. The present invention provides a preparation method of a metal sulfide film, comprising the steps of providing metal halide, such as iron halide (FeCl3, FeI3, FeBr3, FeCl2, FeI2 and FeBr2), as a first raw material and a thioamide compound, such as thioacetamide, as a second raw material, preferably vaporizing these raw materials and reacting them at atmospheric pressure; and a metal sulfide film prepared by this method.
摘要:
A process for manufacturing a quartz crystal element consists of the steps of producing plural quartz layers on a surface of a crystalline substrate having a lattice constant differing from that of quartz crystal, in which each of the quartz layers consists of a crystalline phase and an amorphous phase, and percentage of the crystalline phase in the quartz layer farther from the substrate is larger than percentage of the crystalline phase in the quartz layer adjacent to the substrate; and producing an epitaxially grown quartz crystal film on the surface of the quartz layer farther from the substrate by a reaction between silicon alkoxide and oxygen.
摘要:
A prepreg winding method includes the steps of preparing a plate, a mandrel movable toward and away from the plate, and a press roll movable toward and away from the mandrel and having an axis parallel to the mandrel; mounting a prepreg on the plate, the prepreg being formed by impregnating reinforced fibers with a thermosetting resin sheet; winding a leading end of the prepreg mounted on the plate around the mandrel, and making a pressing force act on the plate and the mandrel therebetween with the prepreg sandwiched between the plate and the mandrel and making a pressing force act on the mandrel and the press roll therebetween with the prepreg sandwiched between the mandrel and the press roll; and winding the prepreg around the mandrel by rotating the mandrel and the press roll.
摘要:
A scratch-resistant blade such as an FRP wind turbine blade and a blade protective sheet which can be easily repaired when scratched. A blade is provided with a laminated protective sheet bonded to at least part of a leading edge of an FRP blade body of said blade, wherein the laminated protective sheet comprises an adhesive layer, a intermediate fabric layer and a durable surface layer, in that order from the blade body.
摘要:
A printing blanket including a base fabric and a surface layer in a laminated structure wherein a surface reforming agent containing a perfluoroalkyl group is applied to the surface layer such that a critical surface tension ranging from 10 to 16 dyn/cm appears on the surface of the surface layer is disclosed. To practically manufacture a printing blanket of the foregoing type, there is also disclosed a method wherein a compressible layer is placed on a base fabric, a surface layer is then placed on the compressible layer thereby to form a laminated structure with the base fabric and the compressible layer, and thereafter, a surface modifier containing a perfluoroalkyl group is applied to the surface layer such that a critical surface tension ranging from 10 to 16 dyne/cm appears on the surface of the surface layer. It is preferable that the surface layer is molded of a compound based on a nitrile butadiene rubber. Usually, the surface modifier contains a perfluoroalkyl group of which carbon number remains within the range of 3 to 12.
摘要:
A process for preparing protocatechualdehyde or a 3-alkoxy-4-hydroxybenzaldehyde which comprises subjecting catechol or a 2-alkoxyphenol to reaction with glyoxylic acid in a basic aqueous medium in the presence of a catalyst containing one or more compounds selected from aluminium oxide, silicon oxide and hydrated aluminium oxide in an amount of not less than 0.01 g per 1 g of the starting catechol or 2-alkoxyphenol at a temperature of 0.degree. to 50.degree. C., and then oxidizing the thus obtained reaction mixture in a basic medium.
摘要:
An FRP drive shaft is formed by joining metal end-joints to each end of an FRP cylinder, wherein each of the metal end-joints includes a press-fitting joint having a serrated portion which is press-fitted into the FRP cylinder, and a cylindrical outer collar which is fixed to an outer periphery of the FRP cylinder, and non-circular engaging portions which are engaged with each other to transfer rotation are formed on the press-fitting joint and the cylindrical outer collar, respectively.