Process for purification of germane
    1.
    发明申请
    Process for purification of germane 有权
    锗烷纯化方法

    公开(公告)号:US20050191854A1

    公开(公告)日:2005-09-01

    申请号:US10788223

    申请日:2004-02-26

    IPC分类号: C22B3/24 C22B41/00 H01L21/44

    CPC分类号: C22B41/00 C22B3/24 Y02P10/234

    摘要: A process and system for the synthesis and/or purification of crude germane to provide a purified germane product are disclosed herein. In one aspect of the present invention, there is provided a process for making a purified germane product containing less than 1 volume percent of one or more germanium-containing impurities comprising: providing a crude germane fluid; passing at least a portion of the crude germane fluid through a first adsorbent which selectively adsorbs water and carbon dioxide contained therein and withdrawing therefrom a partially purified germane fluid; passing at least a portion of the partially purified germane fluid through a second adsorbent which selectively adsorbs the one or more germanium-containing impurities contained therein and withdrawing therefrom a hydrogen-enriched purified germane fluid; and separating the purified germane product hydrogen from the hydrogen-enriched purified germane fluid.

    摘要翻译: 本文公开了用于合成和/或纯化粗锗烷以提供纯化的锗烷产物的方法和系统。 在本发明的一个方面,提供了一种制备含有少于1体积%的一种或多种含锗杂质的纯化的锗烷产物的方法,包括:提供粗锗烷流体; 使至少一部分粗锗烷流体通过第一吸附剂,该第一吸附剂选择性地吸附其中含有的水和二氧化碳并从其中提取部分纯化的锗烷流体; 使部分纯化的锗烷流体的至少一部分通过第二吸附剂,所述第二吸附剂选择性地吸附其中含有的一种或多种含锗杂质并从其中提取富含氢的纯化的锗烷流体; 并将纯化的锗烷产物氢与富氢纯化的锗烷流体分离。

    Storage and delivery systems for gases held in liquid medium
    3.
    发明申请
    Storage and delivery systems for gases held in liquid medium 失效
    保存在液体介质中的气体的储存和输送系统

    公开(公告)号:US20060008392A1

    公开(公告)日:2006-01-12

    申请号:US10887561

    申请日:2004-07-08

    IPC分类号: B01D53/34 B01D50/00

    CPC分类号: F17C11/00

    摘要: The present invention is directed to improvements in storage and delivery systems that allow for rapid fill and delivery of gases reversibly stored in a nonvolatile liquid medium, improvements in delivery and purity of the delivered gas. The low pressure storage and delivery system for gas which comprises: a container having an interior portion containing a reactive Lewis basic or Lewis acidic reactive liquid medium that is reversibly reacted with a gas having opposing Lewis acidity or basicity; a system for transferring energy into or out of the reactive liquid medium; or, a product gas purifier (e.g. a gas/liquid separator); or both.

    摘要翻译: 本发明涉及储存和输送系统的改进,其允许可逆地储存在非挥发性液体介质中的气体的快速填充和输送,输送气体的输送和纯度的改善。 用于气体的低压储存和输送系统包括:容器,其具有含有反应性路易斯碱性或路易斯酸性反应性液体介质的内部部分,其与具有相反路易斯酸度或碱度的气体可逆地反应; 用于将能量转移到或流出反应性液体介质的系统; 或产品气体净化器(例如气/液分离器); 或两者。

    Hybrid process for depositing electrochromic coating
    4.
    发明申请
    Hybrid process for depositing electrochromic coating 有权
    用于沉积电致变色涂层的混合工艺

    公开(公告)号:US20050213185A1

    公开(公告)日:2005-09-29

    申请号:US10806743

    申请日:2004-03-23

    IPC分类号: G02F1/15 G02F1/153

    CPC分类号: G02F1/1523 G02F1/153

    摘要: A method of producing an electrochromic device, includes the steps of: providing a first electron conducting layer on a substrate, providing a working electrode in communication with the first electron conducting layer, providing an ion conducting layer in communication with the working electrode, providing an ion storage electrode in communication with the ion conducting layer, and providing a second electron conducting layer in communication with the ion storage electrode, wherein at least one and less than all of the providing steps include(s) plasma chemical vapor deposition. An electrochromic device produced by the method of the invention is disclosed, as is an apparatus adapted to perform the method of the invention, including plasma CVD devices and vacuum sputtering devices.

    摘要翻译: 一种制造电致变色器件的方法,包括以下步骤:在衬底上提供第一电子传导层,提供与第一电子传导层连通的工作电极,提供与工作电极连通的离子传导层, 离子存储电极与离子传导层连通,并提供与离子存储电极连通的第二电子传导层,其中至少一个并且小于所有提供步骤包括等离子体化学气相沉积。 公开了通过本发明的方法制造的电致变色装置,以及适于执行本发明方法的装置,包括等离子体CVD装置和真空溅射装置。

    Method for depositing zinc oxide at low temperatures and products formed thereby
    5.
    发明申请
    Method for depositing zinc oxide at low temperatures and products formed thereby 有权
    低温沉积氧化锌的方法及由此形成的产品

    公开(公告)号:US20070116986A1

    公开(公告)日:2007-05-24

    申请号:US11284193

    申请日:2005-11-21

    IPC分类号: C23C16/00 H05H1/24 B32B9/00

    摘要: The present invention discloses plasma enhanced chemical vapor deposition (PECVD) process for depositing n-type and p-type zinc oxide-based transparent conducting oxides (TCOs) at low temperatures with excellent optical and electrical properties on glass and temperature sensitive materials such as plastics and polymers. Specifically, it discloses PECVD process for depositing n-type ZnO by doping it with B or F and p-type ZnO by doping it with nitrogen excellent optical and electrical properties on glass and temperature sensitive materials such as plastics and polymers for TCO application. The process utilizes a mixture of volatile zinc compound, argon and/or helium as a diluent gas, carbon dioxide as an oxidant, and a dopant or reactant to deposit the desired ZnO-based TCOs.

    摘要翻译: 本发明公开了一种用于在低温下沉积n型和p型氧化锌基透明导电氧化物(TCO)的等离子体增强化学气相沉积(PECVD)工艺,在玻璃和温度敏感材料如塑料上具有优异的光学和电学性能 和聚合物。 具体地说,它公开了用于通过用B或F和p型ZnO掺杂以将氮掺杂在玻璃上的优异的光学和电学性质以及用于TCO应用的诸如塑料和聚合物的温度敏感材料来沉积n型ZnO的PECVD工艺。 该方法利用挥发性锌化合物,氩和/或氦气作为稀释气体,二氧化碳作为氧化剂和掺杂剂或反应物的混合物以沉积所需的ZnO基TCO。

    Hybrid process for depositing electrochromic coating
    6.
    发明申请
    Hybrid process for depositing electrochromic coating 失效
    用于沉积电致变色涂层的混合工艺

    公开(公告)号:US20070008605A1

    公开(公告)日:2007-01-11

    申请号:US11518802

    申请日:2006-09-11

    IPC分类号: G02F1/15

    CPC分类号: G02F1/1523 G02F1/153

    摘要: A method of producing an electrochromic device, includes the steps of: providing a first electron conducting layer on a substrate, providing a working electrode in communication with the first electron conducting layer, providing an ion conducting layer in communication with the working electrode, providing an ion storage electrode in communication with the ion conducting layer, and providing a second electron conducting layer in communication with the ion storage electrode, wherein at least one and less than all of the providing steps include(s) plasma chemical vapor deposition. An electrochromic device produced by the method of the invention is disclosed, as is an apparatus adapted to perform the method of the invention, including plasma CVD devices and vacuum sputtering devices.

    摘要翻译: 一种制造电致变色器件的方法,包括以下步骤:在衬底上提供第一电子传导层,提供与第一电子传导层连通的工作电极,提供与工作电极连通的离子传导层, 离子存储电极与离子传导层连通,并提供与离子存储电极连通的第二电子传导层,其中至少一个并且小于所有提供步骤包括等离子体化学气相沉积。 公开了通过本发明的方法制造的电致变色装置,以及适于执行本发明方法的装置,包括等离子体CVD装置和真空溅射装置。

    Liquid media containing Lewis basic reactive compounds for storage and delivery of Lewis acidic gases
    8.
    发明申请
    Liquid media containing Lewis basic reactive compounds for storage and delivery of Lewis acidic gases 有权
    含有路易斯碱性反应性化合物的液体介质用于储存和输送路易斯酸性气体

    公开(公告)号:US20060081482A1

    公开(公告)日:2006-04-20

    申请号:US10966803

    申请日:2004-10-15

    IPC分类号: B65B3/00

    CPC分类号: F17C11/00 F17C2223/0123

    摘要: This invention relates to an improvement in a low-pressure storage and delivery system for gases having Lewis acidity, particularly hazardous specialty gases such as BF3 and diborane, which are utilized in the electronics industry. The improvement resides in storing the gases in a liquid incorporating a reactive compound having Lewis basicity capable of effecting a reversible reaction between a gas having Lewis acidity. The reactive compound comprises a reactive species that is dissolved, suspended, dispersed, or otherwise mixed with a nonvolatile liquid.

    摘要翻译: 本发明涉及用于电子工业中的具有路易斯酸性的气体的低压储存和输送系统的改进,特别是危险特种气体如BF 3和乙硼烷。 改进在于将气体储存在结合有能够在具有路易斯酸度的气体之间实现可逆反应的路易斯碱性的反应性化合物的液体中。 反应性化合物包括溶解,悬浮,分散或以其它方式与非挥发性液体混合的反应性物质。

    Method for removing titanium dioxide deposits from a reactor
    9.
    发明申请
    Method for removing titanium dioxide deposits from a reactor 失效
    从反应器中除去二氧化钛沉积物的方法

    公开(公告)号:US20050202167A1

    公开(公告)日:2005-09-15

    申请号:US10800880

    申请日:2004-03-15

    IPC分类号: B05D3/02 B08B6/00 C23C16/00

    摘要: A process for the selective removal of a TiO2-containing substance from an article for cleaning applications is disclosed herein. In one embodiment, there is provided a process for removing a TiO2-containing substance from an article comprising: providing the article having the TiO2-containing substance deposited thereupon; reacting the substance with a reactive gas comprising at least one selected from a fluorine-containing cleaning agent, a chlorine-containing cleaning agent and mixtures thereof to form a volatile product; and removing the volatile product from the article to thereby remove the substance from the article.

    摘要翻译: 本文公开了用于从用于清洁应用的制品中选择性除去含TiO 2的物质的方法。 在一个实施方案中,提供了从制品中除去含TiO 2的物质的方法,包括:提供其上沉积有含TiO 2的物质的制品; 使物质与包含选自含氟清洗剂,含氯清洗剂及其混合物中的至少一种的反应性气体反应以形成挥发性产物; 并从制品中除去挥发性产物,从而从制品中除去物质。

    Ionic liquid based mixtures for gas storage and delivery
    10.
    发明申请
    Ionic liquid based mixtures for gas storage and delivery 有权
    用于气体储存和输送的离子液体基混合物

    公开(公告)号:US20060060817A1

    公开(公告)日:2006-03-23

    申请号:US10948277

    申请日:2004-09-23

    IPC分类号: H01J7/18

    摘要: A mixture and method for the storage and delivery of at least one gas are disclosed herein. In one aspect, there is provided a mixture for the storage and delivery of at least one gas comprising: an ionic liquid comprising an anion and a cation; and at least one gas that is disposed within and is reversibly chemically reacted with the ionic liquid. In another aspect, there is provided a method for delivering at least one gas from a mixture comprising an ionic liquid and at least one gas comprising: reacting the at least one gas and the ionic liquid to provide the mixture and separating the at least one gas from the mixture wherein the at least one gas after the separating step is substantially the same as the at least one gas prior to the reacting step.

    摘要翻译: 本文公开了用于储存和输送至少一种气体的混合物和方法。 在一个方面,提供了用于储存和输送至少一种气体的混合物,其包括:包含阴离子和阳离子的离子液体; 以及至少一种气体,其设置在离子液体内并与其离子液体可逆地化学反应。 在另一方面,提供了一种从包含离子液体和至少一种气体的混合物输送至少一种气体的方法,包括:使至少一种气体和离子液体反应以提供混合物并将至少一种气体 从其中在分离步骤之后的至少一种气体与反应步骤之前的至少一种气体基本上相同的混合物。