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公开(公告)号：US06965057B2
公开(公告)日：2005-11-15
申请号：US10807818
申请日：2004-03-24
CPC分类号： C07C1/20 , B01J38/30 , B01J38/32 , C10G3/49 , C10G3/62 , C10G2300/4093 , C10G2300/708 , C10G2300/802 , C10G2300/805 , C10G2400/20 , Y02P20/584 , Y02P30/42 , C07C11/02
摘要： The invention relates to a process for converting an oxygenate feedstock into an olefin product stream comprising (a) contacting an oxygenate feedstock with a molecular sieve catalyst in a reactor under conditions effective to convert the feedstock into an olefin product stream and to form carbonaceous deposits on the catalyst; (b) contacting at least a portion of the catalyst having said carbonaceous deposits with an oxygen containing gas under conditions effective to obtain a regenerated catalyst having a reduced carbonaceous deposit level and having an increased molecular oxygen content; (c) removing at least 60% by volume of said molecular oxygen from the regenerated catalyst based upon the total volume of molecular oxygen; (d) returning said regenerated catalyst to said reactor; and (e) repeating steps (a)–(d).
摘要翻译： 本发明涉及一种将含氧化合物原料转化成烯烃产物流的方法，该方法包括（a）在有效将原料转化成烯烃产物流并形成碳质沉积物的条件下，使反应器中的含氧化合物原料与分子筛催化剂接触 催化剂; （b）在有效获得具有降低的碳沉积物水平并且具有增加的分子氧含量的再生催化剂的条件下使至少一部分具有所述碳质沉积物的催化剂与含氧气体接触; （c）基于分子氧的总体积从再生催化剂中除去至少60体积％的所述分子氧; （d）将所述再生催化剂返回到所述反应器; 和（e）重复步骤（a） - （d）。
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公开(公告)号：US07060866B2
公开(公告)日：2006-06-13
申请号：US10125138
申请日：2002-04-18
摘要： Disclosed is a method of removing dimethyl ether from an ethylene and/or propylene containing stream. Dimethyl ether is removed at a high pressure, preferably in a distillation column. The high pressure separation has the benefit of providing a relatively low bottoms temperature separation, while allowing for recovery of a highly concentrated ethylene and/or propylene stream.
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公开(公告)号：US07879920B2
公开(公告)日：2011-02-01
申请号：US11097809
申请日：2005-04-01
IPC分类号： C07C27/26
摘要： This invention is directed to methods for forming an olefin stream from a methanol stream. A lower grade methanol, such as chemical grade or crude methanol, can be used as feed to form the olefin stream. The process uses a relatively simple distillation type step to vaporize a portion of the methanol feed stream and send the resulting vapor stream to a reaction unit to form the olefin stream. In addition, the invention provides the ability to operate the downstream recovery units with reduced fouling or plugging due to the presence of fine solids components.
摘要翻译： 本发明涉及从甲醇流形成烯烃流的方法。 低级甲醇如化学级或粗甲醇可用作进料以形成烯烃流。 该方法使用相对简单的蒸馏步骤来蒸发一部分甲醇进料流并将所得蒸气流送至反应单元以形成烯烃流。 此外，本发明提供了由于存在细固体组分而使下游回收单元具有减少的结垢或堵塞的能力。
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公开(公告)号：US07598197B2
公开(公告)日：2009-10-06
申请号：US11050574
申请日：2005-02-03
CPC分类号： B01J8/12 , B01J8/087 , B01J19/0013 , B01J29/90 , B01J38/30 , B01J38/32 , B01J2208/00123 , C07C1/20 , C07C2529/83 , C07C2529/85 , F22B1/04 , F22B21/20 , F22G1/06 , F28D7/0066 , F28D7/0083 , F28D7/06 , F28D7/12 , Y02P20/584 , Y10S502/514 , C07C11/02
摘要： This invention provides processes, systems and devices for cooling catalyst, preferably regenerated catalyst, by superheating steam and boiling water. The inventive process advantageously provides ideal cooling conditions while ensuring minimal hydrothermal deactivation of the catalyst during the cooling process. The invention is particularly well-suited for cooling catalyst in an oxygenate to olefins reaction system.
摘要翻译： 本发明提供了通过过热蒸汽和沸水来冷却催化剂，优选再生催化剂的方法，系统和装置。 本发明的方法有利地提供理想的冷却条件，同时确保在冷却过程中催化剂的最小水热失活。 本发明特别适用于在含氧化合物至烯烃反应体系中冷却催化剂。
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5.发明授权Method of circulating catalyst between a catalyst regenerator and an external catalyst cooler 有权在催化剂再生器和外部催化剂冷却器之间循环催化剂的方法公开(公告)号：US07906697B2
公开(公告)日：2011-03-15
申请号：US12059717
申请日：2008-03-31
申请人： James H. Beech, Jr. , Chunshe Cao , Michael P. Nicoletti , James R. Lattner , Jesse F. Goellner , Rutton D. Patel , Timothy M. Healy
发明人： James H. Beech, Jr. , Chunshe Cao , Michael P. Nicoletti , James R. Lattner , Jesse F. Goellner , Rutton D. Patel , Timothy M. Healy
IPC分类号： C07C2/04
CPC分类号： C07C1/20 , B01J29/90 , B01J38/30 , B01J38/32 , C07C2529/40 , C07C2529/70 , C07C2529/83 , C07C2529/85 , C10G3/49 , C10G3/62 , C10G2300/802 , C10G2400/20 , Y02P20/584 , Y02P30/20 , C07C11/02
摘要： This invention relates to efficiently regenerating catalyst particles by minimizing the formation of localized “hot spots” and “cold spots” in a regeneration zone. Specifically this invention relates to a method for controlling regenerator temperature in an oxygenates-to-olefins system, comprising the steps of: contacting an oxygenate feed in a reactor with a catalytically effective amount of molecular sieve-containing catalyst under conditions effective for converting said oxygenate to a product containing light olefins and forming a coked catalyst; contacting a portion of the coked catalyst in a regenerator, having a catalyst bed height (Hc), an inlet height (Hi), and an outlet height (Ho), with an oxygen-containing regeneration medium under conditions effective to at least partially regenerate the coked catalyst; and conducting a portion of the catalyst from the regenerator to a catalyst cooler to form a cooled catalyst portion, wherein Ho is greater than Hi.
摘要翻译： 本发明涉及通过最小化再生区中局部“热点”和“冷点”的形成来有效地再生催化剂颗粒。 具体地说，本发明涉及一种用于控制含氧化合物至烯烃体系中的再生器温度的方法，其包括以下步骤：在有效转化所述含氧化合物的条件下使反应器中的含氧化合物进料与催化有效量的含分子筛催化剂接触 涉及含有轻质烯烃并形成焦化催化剂的产品; 在具有催化剂床高度（Hc），入口高度（Hi）和出口高度（Ho））的再生器中使一部分焦化催化剂与含氧再生介质在有效至少部分再生的条件下接触 焦化催化剂; 并将催化剂的一部分从再生器导入催化剂冷却器以形成冷却的催化剂部分，其中Ho大于Hi。
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6.发明授权Processes for lifting spent catalyst into a regenerator in an oxygenate to olefins reaction system 有权将废催化剂提升到含氧化合物到烯烃反应体系中的再生器的方法公开(公告)号：US07459595B2
公开(公告)日：2008-12-02
申请号：US11050199
申请日：2005-02-03
CPC分类号： B01J38/16 , B01J29/90 , B01J38/14 , B01J38/28 , C07C1/20 , C10G3/49 , C10G3/60 , C10G3/62 , C10G2300/701 , C10G2300/708 , C10G2300/807 , C10G2400/20 , Y02P20/584 , Y02P30/42 , C07C11/02
摘要： This invention provides processes for transporting catalyst, preferably in an oxygenate to olefins reaction system. In one embodiment, an oxygenate contacts molecular sieve catalyst particles in a reactor under conditions effective to form an effluent stream comprising light olefins and forming coked catalyst particles. At least a portion of the coked catalyst particles are transported from the reactor or a device associated therewith to a catalyst regenerator through a conduit in a fluidized manner with a fluidizing medium comprising air and steam. At least a portion of the coked catalyst particles are regenerated in the catalyst regenerator to form regenerated catalyst particles, which are ultimately directed back to the reactor.
摘要翻译： 本发明提供了将催化剂，优选在含氧化合物转化为烯烃反应体系的方法。 在一个实施方案中，含氧化合物在有效形成包含轻质烯烃和形成焦化催化剂颗粒的流出物流的条件下在反应器中与分子筛催化剂颗粒接触。 焦化的催化剂颗粒的至少一部分从反应器或与其相关的装置通过管道以流化方式通过导管从包含空气和蒸汽的流化介质输送到催化剂再生器。 焦化催化剂颗粒的至少一部分在催化剂再生器中再生以形成再生的催化剂颗粒，其最终被引导回反应器。
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公开(公告)号：US07309383B2
公开(公告)日：2007-12-18
申请号：US10948984
申请日：2004-09-23
CPC分类号： C10G3/62 , C10G3/49 , C10G3/57 , C10G2300/4093 , C10G2400/20 , Y10S585/91 , Y10S585/911
摘要： Catalyst losses are prevented in riser reactor systems by using a low inlet velocity for the first cyclone separator in each multi-stage cyclone separator in the reactor. Catalyst particles not separated from the product output flow in an oxygenate-to-olefin reactor are also recaptured by cooling the product output flow and passing the flow through an electrostatic precipitator.
摘要翻译： 通过在反应器中的每个多级旋风分离器中使用低入口速度用于第一旋风分离器，在提升管反应器系统中防止催化剂损失。 通过冷却产物输出流量并使流过静电除尘器也可以重新捕获在含氧化合物至烯烃反应器中未与产物输出流分离的催化剂颗粒。
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8.发明申请Method Of Circulating Catalyst Between A Catalyst Regenerator And An External Catalyst Cooler 有权催化剂再生器与外部催化剂冷却器之间循环催化剂的方法公开(公告)号：US20090192341A1
公开(公告)日：2009-07-30
申请号：US12059717
申请日：2008-03-31
申请人： James H. Beech, JR. , Chunshe Cao , Michael P. Nicoletti , James R. Lattner , Jesse F. Goellner , Rutton D. Patel , Timothy M. Healy
发明人： James H. Beech, JR. , Chunshe Cao , Michael P. Nicoletti , James R. Lattner , Jesse F. Goellner , Rutton D. Patel , Timothy M. Healy
IPC分类号： C07C2/04
CPC分类号： C07C1/20 , B01J29/90 , B01J38/30 , B01J38/32 , C07C2529/40 , C07C2529/70 , C07C2529/83 , C07C2529/85 , C10G3/49 , C10G3/62 , C10G2300/802 , C10G2400/20 , Y02P20/584 , Y02P30/20 , C07C11/02
摘要： This invention relates to efficiently regenerating catalyst particles by minimizing the formation of localized “hot spots” and “cold spots” in a regeneration zone. Specifically this invention relates to a method for controlling regenerator temperature in an oxygenates-to-olefins system, comprising the steps of: contacting an oxygenate feed in a reactor with a catalytically effective amount of molecular sieve-containing catalyst under conditions effective for converting said oxygenate to a product containing light olefins and forming a coked catalyst; contacting a portion of the coked catalyst in a regenerator, having a catalyst bed height (Hc), an inlet height (Hi), and an outlet height (Ho), with an oxygen-containing regeneration medium under conditions effective to at least partially regenerate the coked catalyst; and conducting a portion of the catalyst from the regenerator to a catalyst cooler to form a cooled catalyst portion, wherein Ho is greater than Hi.
摘要翻译： 本发明涉及通过最小化再生区中局部“热点”和“冷点”的形成来有效地再生催化剂颗粒。 具体地说，本发明涉及一种用于控制含氧化合物至烯烃体系中的再生器温度的方法，包括以下步骤：在有效转化所述含氧化合物的条件下使反应器中的含氧化合物进料与催化有效量的含分子筛的催化剂接触 涉及含有轻质烯烃并形成焦化催化剂的产品; 在具有催化剂床高度（Hc），入口高度（Hi）和出口高度（Ho））的再生器中使一部分焦化催化剂与含氧再生介质在有效至少部分再生的条件下接触 焦化催化剂; 并将催化剂的一部分从再生器导入催化剂冷却器以形成冷却的催化剂部分，其中Ho大于Hi。
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公开(公告)号：US06437208B1
公开(公告)日：2002-08-20
申请号：US09481364
申请日：2000-01-11
申请人： Keith H. Kuechler , Marcel J. G. Janssen , Stephen N. Vaughn , Shun C. Fung , Nicolas P. Coute , Jeffrey Scott Smith , James R. Lattner , Jeffrey L. White , Teng Xu , William L. Kuechler, Sr. , Machteld M. Mertens , Cornelius W. M. Van Oorschot
发明人： Keith H. Kuechler , Marcel J. G. Janssen , Stephen N. Vaughn , Shun C. Fung , Nicolas P. Coute , Jeffrey Scott Smith , James R. Lattner , Jeffrey L. White , Teng Xu , William L. Kuechler, Sr. , Machteld M. Mertens , Cornelius W. M. Van Oorschot
IPC分类号： C07C120
CPC分类号： C10G50/00 , B01J29/85 , B01J29/90 , B01J35/0006 , B01J2229/123 , C10G3/49 , C10G3/57 , C10G3/62 , C10G2300/1022 , C10G2300/1029 , C10G2300/4018 , C10G2300/708 , C10G2400/02 , C10G2400/20 , C10G2400/22 , Y02P30/42
摘要： Disclosed is a method for making olefin product from an oxygenate-containing feedstock. In the method, a silicoaluminophosphate molecular sieve catalyst is contacted with the oxygenate-containing feedstock in a reactor at an average catalyst feedstock exposure index of at least 1.0. The method produces lower coke yield and provides an olefin product which is low in C1-C4 paraffin content. The invention is particularly effective in producing an olefin product having a very low propane content.
摘要翻译： 公开了一种从含氧化合物的原料制备烯烃产物的方法。 在该方法中，将硅铝磷酸盐分子筛催化剂在反应器中与含氧化合物的原料接触，平均催化剂原料暴露指数为至少1.0。 该方法产生较低的焦炭产量，并提供C1-C4链烷烃含量低的烯烃产物。 本发明在生产丙烷含量非常低的烯烃产物方面特别有效。
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公开(公告)号：US09024078B2
公开(公告)日：2015-05-05
申请号：US13515104
申请日：2010-12-17
申请人： Jihad M. Dakka , Lorenzo C. Decaul , Sabato Miseo , James R. Lattner , Tan-Jen Chen , Terry E. Helton , Teng Xu
发明人： Jihad M. Dakka , Lorenzo C. Decaul , Sabato Miseo , James R. Lattner , Tan-Jen Chen , Terry E. Helton , Teng Xu
IPC分类号： C07C37/08 , C07C5/32 , C07C37/07 , C07C45/53 , C07C407/00
CPC分类号： C07C37/08 , B01J23/58 , B01J35/1019 , B01J35/1061 , B01J37/0009 , B01J37/0203 , C07C5/367 , C07C37/07 , C07C45/53 , C07C407/00 , C07C2521/08 , C07C2523/42 , C07C2523/58 , C07C2601/14 , Y02P20/52 , C07C39/04 , C07C49/403 , C07C409/14 , C07C15/04
摘要： A dehydrogenation process for the dehydrogenation of at least one dehydrogenatable hydrocarbon, the process comprising contacting a feed comprising the at least one dehydrogenatable hydrocarbon under dehydrogenation conditions with a catalyst composition comprising a support and at least one dehydrogenation component wherein said conditions include a temperature of from 400° C. to 750° C. and a pressure of at least 50 psig (345 kPag).
摘要翻译： 用于脱氢至少一种可脱氢烃的脱氢方法，该方法包括在脱氢条件下使包含至少一种可脱氢烃的进料与包含载体和至少一种脱氢组分的催化剂组合物接触，其中所述条件包括 400℃至750℃，压力至少为50psig（345kPag）。
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