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1.发明申请WATER-SOLUBLE CARBON NANOTUBE COMPOSITIONS FOR DRUG DELIVERY AND MEDICINAL APPLICATIONS 有权用于药物递送和药物应用的可溶性碳纳米管组合物公开(公告)号：US20090170768A1
公开(公告)日：2009-07-02
申请号：US12245438
申请日：2008-10-03
申请人： James M. Tour , Valerie C. Moore , S. Ward Casscella , Jeffrey N. Myers , Zvonimir L. Milas , Kathy A. Mason , Luka Milas , Brandl Katherine Price , Jared L. Hudson , Jodie L. Conyers, JR. , Rebecca L. Lucente-Schultz , Ashley Leonard , Dmitry V. Kosynkin
发明人： James M. Tour , Valerie C. Moore , S. Ward Casscella , Jeffrey N. Myers , Zvonimir L. Milas , Kathy A. Mason , Luka Milas , Brandl Katherine Price , Jared L. Hudson , Jodie L. Conyers, JR. , Rebecca L. Lucente-Schultz , Ashley Leonard , Dmitry V. Kosynkin
IPC分类号： A61K38/18 , A61K31/337 , A61K47/04
CPC分类号： A61K31/337 , A61K38/1808 , A61K47/60 , A61K47/6925 , A61K47/6929 , B82Y5/00
摘要： Compositions comprising a plurality of functionalized carbon nanotubes and at least one type of payload molecule are provided herein. The compositions are soluble in water and PBS in some embodiments. In certain embodiments, the payload molecules are insoluble in water. Methods are described for making the compositions and administering the compositions. An extended release formulation for paclitaxel utilizing functionalized carbon nanotubes is also described.
摘要翻译： 本文提供了包含多个官能化碳纳米管和至少一种有效载荷分子的组合物。 在一些实施方案中，组合物可溶于水和PBS。 在某些实施方案中，有效载荷分子不溶于水。 描述了制备组合物和施用组合物的方法。 还描述了利用官能化碳纳米管的紫杉醇的延长释放制剂。
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2.发明授权Water-soluble carbon nanotube compositions for drug delivery and medicinal applications 有权用于药物输送和药物应用的水溶性碳纳米管组合物公开(公告)号：US08784866B2
公开(公告)日：2014-07-22
申请号：US12245438
申请日：2008-10-03
申请人： James M. Tour , Rebecca Lucente-Schultz , Ashley Leonard , Dmitry V. Kosynkin , Brandi Katherine Price , Jared L. Hudson , Jodie L. Conyers, Jr. , Valerie C. Moore , S. Ward Casscells , Jeffrey N. Myers , Zvonimir L. Milas , Kathy A. Mason , Luka Milas
发明人： James M. Tour , Rebecca Lucente-Schultz , Ashley Leonard , Dmitry V. Kosynkin , Brandi Katherine Price , Jared L. Hudson , Jodie L. Conyers, Jr. , Valerie C. Moore , S. Ward Casscells , Jeffrey N. Myers , Zvonimir L. Milas , Kathy A. Mason , Luka Milas
IPC分类号： A61F2/00
CPC分类号： A61K31/337 , A61K38/1808 , A61K47/60 , A61K47/6925 , A61K47/6929 , B82Y5/00
摘要： Compositions comprising a plurality of functionalized carbon nanotubes and at least one type of payload molecule are provided herein. The compositions are soluble in water and PBS in some embodiments. In certain embodiments, the payload molecules are insoluble in water. Methods are described for making the compositions and administering the compositions. An extended release formulation for paclitaxel utilizing functionalized carbon nanotubes is also described.
摘要翻译： 本文提供了包含多个官能化碳纳米管和至少一种有效载荷分子的组合物。 在一些实施方案中，组合物可溶于水和PBS。 在某些实施方案中，有效载荷分子不溶于水。 描述了制备组合物和施用组合物的方法。 还描述了利用官能化碳纳米管的紫杉醇的延长释放制剂。
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公开(公告)号：US20100197783A1
公开(公告)日：2010-08-05
申请号：US12593585
申请日：2008-03-26
申请人： James M. Tour , Meng Lu , Rebecca Lucente-Schultz , Ashley Leonard , Condell Dewayne Doyle , Dmitry V. Kosynkin , Brandi Katherine Price
发明人： James M. Tour , Meng Lu , Rebecca Lucente-Schultz , Ashley Leonard , Condell Dewayne Doyle , Dmitry V. Kosynkin , Brandi Katherine Price
IPC分类号： A61K31/215 , A61P43/00 , C07C229/00
CPC分类号： A61K9/0092 , A61K8/19 , A61K47/60 , A61K47/6925 , A61K2800/413 , A61Q17/04 , B82Y5/00 , B82Y30/00 , B82Y40/00 , C01B32/15 , C01B2202/02 , C01B2202/04 , C01B2202/06
摘要： A method of reducing side effects of damage in a human subject exposed to radiation includes administering to the human subject carbon nanotubes in a pharmaceutically acceptable carrier after or prior to exposure to radiation. A composition for reducing radical damage includes a carbon nanotube which is functionalized (1) for substantial water solubility and (2) with a radical trapping agent appended to the carbon nanotube forming a radical scavenger-carbon nanotube conjugate.
摘要翻译： 在暴露于辐射的人类受试者中减少损伤的副作用的方法包括在暴露于辐射之后或暴露于辐射之前向人受试者在药学上可接受的载体中施用碳纳米管。 用于还原自由基损伤的组合物包括官能化（1）用于大量水溶性的碳纳米管和（2）附着到形成自由基清除剂 - 碳纳米管缀合物的碳纳米管上的自由基捕获剂。
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公开(公告)号：US20110144386A1
公开(公告)日：2011-06-16
申请号：US12812169
申请日：2009-01-08
IPC分类号： C07C63/00 , C07C25/24 , C07C205/45 , C07C43/235 , C07C17/281 , C01B31/00
CPC分类号： C09K8/032 , B82Y30/00 , B82Y40/00 , C01B32/192 , C01B32/194 , C01B32/23 , C01B2204/04 , C01B2204/28 , C09K8/035 , C09K8/62 , Y10S977/734 , Y10S977/737 , Y10S977/738
摘要： Drilling fluids comprising graphenes and nanoplatelet additives and methods for production thereof are disclosed. Graphene includes graphite oxide, graphene oxide, chemically-converted graphene, and functionalized chemically-converted graphene. Derivatized graphenes and methods for production thereof are disclosed. The derivatized graphenes are prepared from a chemically-converted graphene through derivatization with a plurality of functional groups. Derivatization can be accomplished, for example, by reaction of a chemically-converted graphene with a diazonium species. Methods for preparation of graphite oxide are also disclosed.
摘要翻译： 公开了包含石墨烯和纳米血小板添加剂的钻井液及其生产方法。 石墨烯包括氧化石墨，氧化石墨烯，化学转化的石墨烯和官能化的化学转化的石墨烯。 公开了衍生化的石墨烯及其生产方法。 衍生的石墨烯通过具有多个官能团的衍生化由化学转化的石墨烯制备。 衍生化可以通过例如化学转化的石墨烯与重氮物质的反应来实现。 还公开了制备氧化石墨的方法。
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5.发明授权Methods for preparation of graphene nanoribbons from carbon nanotubes and compositions, thin films and devices derived therefrom 有权从碳纳米管和组合物制备石墨烯纳米带的方法，由其衍生的薄膜和器件公开(公告)号：US08703090B2
公开(公告)日：2014-04-22
申请号：US12544017
申请日：2009-08-19
IPC分类号： D01F9/12 , C01B31/00 , C08F290/14
CPC分类号： C01B31/0446 , B82Y30/00 , B82Y40/00 , C01B32/184 , C01B32/194 , C01B32/23 , C01B2204/06 , H01J9/025 , Y10S977/734 , Y10S977/842
摘要： Methods for producing macroscopic quantities of oxidized graphene nanoribbons are disclosed herein. The methods include providing a plurality of carbon nanotubes and reacting the plurality of carbon nanotubes with at least one oxidant to form oxidized graphene nanoribbons. The at least one oxidant is operable to longitudinally open the carbon nanotubes. In some embodiments, the reacting step takes place in the presence of at least one acid. In some embodiments, the reacting step takes place in the presence of at least one protective agent. Various embodiments of the present disclosure also include methods for producing reduced graphene nanoribbons by reacting oxidized graphene nanoribbons with at least one reducing agent. Oxidized graphene nanoribbons, reduced graphene nanoribbons and compositions and articles derived therefrom are also disclosed herein.
摘要翻译： 本文公开了生产宏观量的氧化石墨烯纳米带的方法。 所述方法包括提供多个碳纳米管并使多个碳纳米管与至少一种氧化剂反应以形成氧化石墨烯纳米带。 至少一种氧化剂可操作以纵向打开碳纳米管。 在一些实施方案中，反应步骤在至少一种酸的存在下进行。 在一些实施方案中，反应步骤在至少一种保护剂的存在下进行。 本公开的各种实施方案还包括通过使氧化石墨烯纳米带与至少一种还原剂反应来生产还原的石墨烯纳米带的方法。 氧化石墨烯纳米带，还原石墨烯纳米带以及由其衍生的组合物和制品也在本文中公开。
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公开(公告)号：US20140081067A1
公开(公告)日：2014-03-20
申请号：US14001255
申请日：2012-02-27
申请人： James M. Tour , Alexander Slesarev , Dmitry V. Kosynkin , Anna Y. Romanchuk , Stepan N. Kalmykov
发明人： James M. Tour , Alexander Slesarev , Dmitry V. Kosynkin , Anna Y. Romanchuk , Stepan N. Kalmykov
IPC分类号： B01J20/00
CPC分类号： B01J20/205 , B01D15/08 , B01D21/262 , B01D61/025 , B01D61/145 , B01J20/00 , B01J20/0296 , B01J20/3085 , B01J20/3204 , B01J20/3244 , B01J20/327 , B01J20/3272 , B01J20/3416 , B03C5/00 , C02F1/283 , C02F1/385 , C02F1/441 , C02F1/444 , C02F1/4696 , C02F1/52 , C02F1/66 , C02F1/683 , C02F9/00 , C02F2101/006 , C02F2101/14 , C02F2101/206 , C02F2303/18 , G21F9/12
摘要： Various aspects of the present invention pertain to methods of sorption of various materials from an environment, including radioactive elements, chlorates, perchlorates, organohalogens, and combinations thereof. Such methods generally include associating graphene oxides with the environment. This in turn leads to the sorption of the materials to the graphene oxides. In some embodiments, the methods of the present invention also include a step of separating the graphene oxides from the environment after the sorption of the materials to the graphene oxides. More specific aspects of the present invention pertain to methods of sorption of radionuclides (such as actinides) from a solution by associating graphene oxides with the solution and optionally separating the graphene oxides from the solution after the sorption.
摘要翻译： 本发明的各个方面涉及从环境中吸收各种材料的方法，包括放射性元素，氯酸盐，高氯酸盐，有机卤素及其组合。 这些方法通常包括将石墨烯氧化物与环境缔合。 这反过来导致材料对石墨烯氧化物的吸附。 在一些实施方案中，本发明的方法还包括在将材料吸附到石墨烯氧化物之后将石墨烯氧化物与环境分离的步骤。 本发明的更具体方面涉及通过将石墨烯氧化物与溶液缔合并且在吸附之后任选地从溶液中分离石墨烯氧化物从溶液中吸收放射性核素（例如锕系元素）的方法。
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7.发明申请METHODS FOR PREPARATION OF GRAPHENE NANORIBBONS FROM CARBON NANOTUBES AND COMPOSITIONS, THIN FILMS AND DEVICES DERIVED THEREFROM 审中-公开从碳纳米管和组合物制备石墨纳米颗粒的方法，薄膜和其衍生的器件公开(公告)号：US20140120024A1
公开(公告)日：2014-05-01
申请号：US14148159
申请日：2014-01-06
IPC分类号： C01B31/04
CPC分类号： C01B32/184 , B82Y30/00 , B82Y40/00 , C01B32/194 , C01B32/23 , C01B2204/06 , C04B14/024 , H01J9/025 , Y10S977/734 , Y10S977/842
摘要： Methods for producing macroscopic quantities of oxidized graphene nanoribbons are disclosed herein. The methods include providing a plurality of carbon nanotubes and reacting the plurality of carbon nanotubes with at least one oxidant to form oxidized graphene nanoribbons. The at least one oxidant is operable to longitudinally open the carbon nanotubes. In some embodiments, the reacting step takes place in the presence of at least one acid. In some embodiments, the reacting step takes place in the presence of at least one protective agent. Various embodiments of the present disclosure also include methods for producing reduced graphene nanoribbons by reacting oxidized graphene nanoribbons with at least one reducing agent. Oxidized graphene nanoribbons, reduced graphene nanoribbons and compositions and articles derived therefrom are also disclosed herein.
摘要翻译： 本文公开了生产宏观量的氧化石墨烯纳米带的方法。 所述方法包括提供多个碳纳米管并使多个碳纳米管与至少一种氧化剂反应以形成氧化石墨烯纳米带。 至少一种氧化剂可操作以纵向打开碳纳米管。 在一些实施方案中，反应步骤在至少一种酸的存在下进行。 在一些实施方案中，反应步骤在至少一种保护剂的存在下进行。 本公开的各种实施方案还包括通过使氧化石墨烯纳米带与至少一种还原剂反应来生产还原的石墨烯纳米带的方法。 氧化石墨烯纳米带，还原石墨烯纳米带以及由其衍生的组合物和制品也在本文中公开。
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8.发明申请Dissolution Of Graphite, Graphite And Graphene Nanoribbons In Superacid Solutions And Manipulation Thereof 有权石墨，石墨和石墨烯纳米带在超强酸溶液中的溶解及其操作公开(公告)号：US20120063988A1
公开(公告)日：2012-03-15
申请号：US13202352
申请日：2010-02-19
申请人： James M. Tour , Matteo Pasquali , Natnael Behabtu , Jay R. Lomeda , Dmitry V. Kosynkin , Amanda Duque , Micah J. Green , A. Nicholas Parra-Vasquez , Colin Young
发明人： James M. Tour , Matteo Pasquali , Natnael Behabtu , Jay R. Lomeda , Dmitry V. Kosynkin , Amanda Duque , Micah J. Green , A. Nicholas Parra-Vasquez , Colin Young
IPC分类号： C01B31/00 , C08L77/10 , C08L79/00 , D01F9/12 , B29C47/00 , B05D3/02 , C08K3/30 , C01B31/04 , B82Y30/00 , B82Y40/00
CPC分类号： D01D1/02 , B82Y30/00 , B82Y40/00 , C01B32/19 , C01B32/194 , C01B32/20 , C01B32/23 , D01D5/04 , D01F9/12
摘要： Methods for dissolving carbon materials such as, for example, graphite, graphite oxide, oxidized graphene nanoribbons and reduced graphene nanoribbons in a solvent containing at least one superacid are described herein. Both isotropic and liquid crystalline solutions can be produced, depending on the concentration of the carbon material The superacid solutions can be formed into articles such as, for example, fibers and films, mixed with other materials such as, for example, polymers, or used for functionalization of the carbon material. The superacid results in exfoliation of the carbon material to produce individual particles of the carbon material. In some embodiments, graphite or graphite oxide is dissolved in a solvent containing at least one superacid to form graphene or graphene oxide, which can be subsequently isolated. In some embodiments, liquid crystalline solutions of oxidized graphene nanoribbons in water are also described.
摘要翻译： 本文描述了将碳材料例如石墨，氧化石墨，氧化石墨烯纳米带和还原的石墨烯纳米带溶解在含有至少一种超强酸的溶剂中的方法。 根据碳材料的浓度，可以生产各向同性和液晶溶液。超强酸溶液可以形成为诸如纤维和薄膜的制品，与其它材料例如聚合物混合或使用 用于碳材料的官能化。 超强酸导致碳材料的剥离以产生碳材料的单个颗粒。 在一些实施方案中，将石墨或氧化石墨溶解在含有至少一种超强酸的溶剂中以形成石墨烯或氧化石墨烯，其可以随后分离。 在一些实施方案中，还描述了氧化石墨烯纳米带在水中的液晶溶液。
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9.发明申请Methods for Preparation of Graphene Nanoribbons From Carbon Nanotubes and Compositions, Thin Films and Devices Derived Therefrom 有权从碳纳米管和组合物制备石墨烯纳米带的方法，衍生自其的薄膜和器件公开(公告)号：US20100105834A1
公开(公告)日：2010-04-29
申请号：US12544017
申请日：2009-08-19
IPC分类号： C08F301/00 , D01F9/12 , C01B31/00 , C01B21/082
CPC分类号： C01B31/0446 , B82Y30/00 , B82Y40/00 , C01B32/184 , C01B32/194 , C01B32/23 , C01B2204/06 , H01J9/025 , Y10S977/734 , Y10S977/842
摘要： Methods for producing macroscopic quantities of oxidized graphene nanoribbons are disclosed herein. The methods include providing a plurality of carbon nanotubes and reacting the plurality of carbon nanotubes with at least one oxidant to form oxidized graphene nanoribbons. The at least one oxidant is operable to longitudinally open the carbon nanotubes. In some embodiments, the reacting step takes place in the presence of at least one acid. In some embodiments, the reacting step takes place in the presence of at least one protective agent. Various embodiments of the present disclosure also include methods for producing reduced graphene nanoribbons by reacting oxidized graphene nanoribbons with at least one reducing agent. Oxidized graphene nanoribbons, reduced graphene nanoribbons and compositions and articles derived therefrom are also disclosed herein.
摘要翻译： 本文公开了生产宏观量的氧化石墨烯纳米带的方法。 所述方法包括提供多个碳纳米管并使多个碳纳米管与至少一种氧化剂反应以形成氧化石墨烯纳米带。 至少一种氧化剂可操作以纵向打开碳纳米管。 在一些实施方案中，反应步骤在至少一种酸的存在下进行。 在一些实施方案中，反应步骤在至少一种保护剂的存在下进行。 本公开的各种实施方案还包括通过使氧化石墨烯纳米带与至少一种还原剂反应来生产还原的石墨烯纳米带的方法。 氧化石墨烯纳米带，还原石墨烯纳米带以及由其衍生的组合物和制品也在本文中公开。
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10.发明授权Dissolution of graphite, graphite and graphene nanoribbons in superacid solutions and manipulation thereof 有权石墨，石墨烯和石墨烯纳米带在超强酸溶液中的溶解及其操作公开(公告)号：US09534319B2
公开(公告)日：2017-01-03
申请号：US13202352
申请日：2010-02-19
申请人： James M. Tour , Matteo Pasquali , Natnael Behabtu , Jay R. Lomeda , Dmitry V. Kosynkin , Amanda Duque , Micah J. Green , A. Nicholas Parra-Vasquez , Colin Young
发明人： James M. Tour , Matteo Pasquali , Natnael Behabtu , Jay R. Lomeda , Dmitry V. Kosynkin , Amanda Duque , Micah J. Green , A. Nicholas Parra-Vasquez , Colin Young
IPC分类号： C01B31/00 , C08L77/10 , C08L79/00 , D01F9/12 , B29C47/00 , B05D3/02 , C08K3/30 , C01B31/04 , B82Y30/00 , B82Y40/00 , D01D1/02 , D01D5/04
CPC分类号： D01D1/02 , B82Y30/00 , B82Y40/00 , C01B32/19 , C01B32/194 , C01B32/20 , C01B32/23 , D01D5/04 , D01F9/12
摘要： Methods for dissolving carbon materials such as, for example, graphite, graphite oxide, oxidized graphene nanoribbons and reduced graphene nanoribbons in a solvent containing at least one superacid are described herein. Both isotropic and liquid crystalline solutions can be produced, depending on the concentration of the carbon material The superacid solutions can be formed into articles such as, for example, fibers and films, mixed with other materials such as, for example, polymers, or used for functionalization of the carbon material. The superacid results in exfoliation of the carbon material to produce individual particles of the carbon material. In some embodiments, graphite or graphite oxide is dissolved in a solvent containing at least one superacid to form graphene or graphene oxide, which can be subsequently isolated. In some embodiments, liquid crystalline solutions of oxidized graphene nanoribbons in water are also described.
摘要翻译： 本文描述了将碳材料例如石墨，氧化石墨，氧化石墨烯纳米带和还原的石墨烯纳米带溶解在含有至少一种超强酸的溶剂中的方法。 根据碳材料的浓度，可以生产各向同性和液晶溶液。超强酸溶液可以形成为诸如纤维和薄膜的制品，与其它材料例如聚合物混合或使用 用于碳材料的官能化。 超强酸导致碳材料的剥离以产生碳材料的单个颗粒。 在一些实施方案中，将石墨或氧化石墨溶解在含有至少一种超强酸的溶剂中以形成石墨烯或氧化石墨烯，其可以随后分离。 在一些实施方案中，还描述了氧化石墨烯纳米带在水中的液晶溶液。
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