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    Process for production of moldings or films from polyisocyanate polyadducts by rim procedure
    3.
    发明授权
    Process for production of moldings or films from polyisocyanate polyadducts by rim procedure 失效
    通过RIM程序从聚异氰酸酯多糖生产模具或薄膜的工艺

    公开(公告)号：US5064600A

    公开(公告)日：1991-11-12

    申请号：US614798

    申请日：1990-11-14

    申请人： Joachim Wagner ,  Werner Rasshofer ,  Ulrich Eisele ,  Eberhard Jurgens ,  Christian Weber ,  Erich Meier

    发明人： Joachim Wagner ,  Werner Rasshofer ,  Ulrich Eisele ,  Eberhard Jurgens ,  Christian Weber ,  Erich Meier

    IPC分类号： C08G18/65 ,  B29C43/00 ,  B29K75/00 ,  C08G18/10 ,  C08G18/50 ,  C08G18/66 ,  C08G18/80

    CPC分类号： C08G18/8019 ,  C08G18/10 ,  C08G18/5048 ,  C08G18/6685 ,  C08G2120/00

    摘要： The present invention relates to a process for the preparation of moldings or films based on polyisocyanate polyadducts comprising thermoplastically molding, at a temperature of at least 50.degree. C. and at a pressure of at least 5 bar, polyisocyanate polyadducts obtained by reacting in closed molds using the reaction injection molding technique aromatic polyisocyanates; compounds having a molecular weight of from 1800 to 12,000 and containing on a statistical average at least 2.5 isocyanate-reactive groups; and one or more components selected from a diamine containing two primary and/or secondary aromatically bound amino groups and and an aliphatic or cycloaliphatic polyol or polyamine; with the provisos that the quantity of isocyanate-reactive compound is at least 30% by weight based on the total quantity of the components and that at least one of the diamine, polyol, or polyamine components comprises at least 5% by weight based on the weight of the isocyanate-reactive compound.

    摘要翻译： 本发明涉及一种用于制备基于多异氰酸酯多加成物的模制品或薄膜的方法，所述方法包括在至少50℃和至少5巴的压力下热塑性模塑，所述多异氰酸酯加合物通过在封闭模具 使用反应注塑技术芳族聚异氰酸酯; 化合物的分子量为1800至12,000，并且统计平均含有至少2.5个异氰酸酯反应性基团; 和选自含有两个伯和/或二个芳族结合氨基的二胺的一种或多种组分和脂族或脂环族多元醇或多胺; 条件是异氰酸酯反应性化合物的量基于组分的总量为至少30重量％，并且至少一种二胺，多元醇或多胺组分包含至少5重量％，基于 异氰酸酯反应性化合物的重量。

    Process for the production of composite structures
    5.
    发明授权
    Process for the production of composite structures 失效
    复合结构生产工艺

    公开(公告)号：US5154871A

    公开(公告)日：1992-10-13

    申请号：US658278

    申请日：1991-02-20

    申请人： Joachim Wagner ,  Karl Peltzer ,  Werner Rasshofer

    发明人： Joachim Wagner ,  Karl Peltzer ,  Werner Rasshofer

    IPC分类号： B32B25/14 ,  B32B18/00 ,  B32B27/08 ,  B32B27/40 ,  C08G18/50 ,  C08G18/65

    CPC分类号： B32B27/08 ,  Y10T428/2495 ,  Y10T428/263 ,  Y10T428/31551 ,  Y10T442/67

    摘要： Composite structures are produced by placing at least two flat, thermoplastically formable plastic materials one above the other and thermoplasticially molding the materials under sufficient conditions of temperature and pressure that molding is accompanied by intimate union of individual layers of the structure. At least one of the plastic materials is based on a polyisocyanate polyaddition product having a density of at least 0.8 g/cm.sup.3 and is prepared by reacting:a) an aromatic polyisocyanate,b) a compound having a molecular weight of about 1800 to 12,000 and containing an average of at least 2.5 isocyanate reactive groups,c) optionally a diamine having a molecular weight of from 108 to 400 and containing two primary and/or secondary aromatically bound amino groups, andd) optionally an aliphatic or cycloaliphatic polyol and/or an aliphatic or cycloaliphatic polyamine having a molecular weight of from 60 to 1799 and which may contain ether groups,at an isocyanate index of from about 60 to 140. The total combined amount of components c) and d) is at least 5% by weight, based on the weight of component b).

    摘要翻译： 通过在足够的温度和压力条件下放置至少两个平坦的，热塑性可成形的塑料材料一个在另一个之上并热塑性地模制材料来生产复合结构，该模塑伴随着结构的各个层的紧密结合。 至少一种塑料材料是基于密度为至少0.8g / cm 3的多异氰酸酯加聚产物，其通过以下方法制备：a）芳族多异氰酸酯，b）分子量为约1800至12,000的化合物和 含有至少2.5个异氰酸酯反应性基团的平均值，c）任选分子量为108-400的二胺，并含有两个伯和/或二次芳香结合的氨基，和d）任选的脂族或脂环族多元醇和/或 分子量为60至1799的脂族或脂环族多胺，其可含有醚基，异氰酸酯指数为约60至140.组分c）和d）的总组合量为至少5重量％ ，基于组分b）的重量。

    Composite structures
    6.
    发明授权
    Composite structures 失效
    复合结构

    公开(公告)号：US5009950A

    公开(公告)日：1991-04-23

    申请号：US323454

    申请日：1989-03-14

    申请人： Joachim Wagner ,  Karl Peltzer ,  Werner Rasshofer

    发明人： Joachim Wagner ,  Karl Peltzer ,  Werner Rasshofer

    IPC分类号： B32B25/14 ,  B32B18/00 ,  B32B27/08 ,  B32B27/40 ,  C08G18/50 ,  C08G18/65

    CPC分类号： B32B27/08 ,  Y10T428/2495 ,  Y10T428/263 ,  Y10T428/31551 ,  Y10T442/67

    摘要： The present invention is directed to composite structures by thermoplastically shaping an assembly of at least two flat thermoplastically formable plastic materials placed in layers one above the other and optionally at least one upper, lower and/or intermediate layer containing a reinforcing or filler material under such conditions of temperature and pressure that shaping is accompanied by intimate union of the individual layers of the assembly, characterized in that at least one of the flat plastic materials is based on a polyisocyanate polyaddition product having a density of at least 0.8 g/cm.sup.3 which has been prepared by the reaction of(a) aromatic polyisocyanates,(b) compounds having a molecular weight of 1800 to about 12000 and containing a statistical average of at least 2.5 isocyanate-reactive groups, optionally(c) diamines in the molecular weight range of 108 to 400 containing two primary and/or secondary aromatically bound amino groups, and optionally(d) (cyclo)alkanepolyols and/or (cyclo)alkanepolyamines in the molecular weight range of 60 to 1799 optionally containing ether groups,by a single stage or multi-stage process at an isocyanate index of 60 to 140, wherein at least one of components (c) or (d) is used in a quantity such that the total quantity of components (c) and (d) is at least 5% by weight, based on the weight of component (b).

    摘要翻译： 本发明涉及复合结构，其通过将至少两个平坦的可塑成形塑料材料的组件热塑成形，一个层叠在另一层之上，以及任选地至少一层含有增强或填充材料的上，下和/或中间层 温度和压力的条件是成形伴随着组件的各个层的紧密结合，其特征在于，所述扁平塑料材料中的至少一种基于密度为至少0.8g / cm 3的多异氰酸酯加聚产物，其具有 通过（a）芳族多异氰酸酯的反应制备，（b）分子量为1800至约12000的化合物，并且含有至少2.5个异氰酸酯反应性基团的统计平均值，任选（c）分子量范围内的二胺 108至400，其含有两个伯和/或二次芳香结合的氨基，以及任选的（d）（环）烷撑多糖 通过在异氰酸酯指数为60至140的单级或多级方法，任选地含有醚基的分子量范围为60至1799的（环）链烷多胺和/或（环）链烷多胺，其中至少一种组分（c）或 （d）的使用量使得组分（c）和（d）的总量基于组分（b）的重量为至少5重量％。

    Process for producing moldings using a mold release agent
    7.
    发明授权
    Process for producing moldings using a mold release agent 失效
    使用脱模剂制造模制品的方法

    公开(公告)号：US5716580A

    公开(公告)日：1998-02-10

    申请号：US596970

    申请日：1996-02-05

    申请人： Joachim Wagner ,  Werner Rasshofer

    发明人： Joachim Wagner ,  Werner Rasshofer

    IPC分类号： B29C33/62 ,  B29C67/24 ,  B28B7/36

    CPC分类号： B29C33/62 ,  B29C67/246 ,  B29K2075/00

    摘要： The present invention is directed to a process for the production of moldings from plastic forming materials in metal molds comprising coating at least a portion of the internal walls of the mold with an external mold release agent, introducing the plastic forming material into the mold, closing the mold, and removing the product from the mold, the improvement wherein the external mold release agent comprises one or more organic compounds the molecules of contain on a statistical average A) from 0.5 to 1.2 polar groups selected from the group consisting of --CN, --NC, --NCO, --CNO, --OCN, --SCN and --NCS and B) at least one non-polar hydrocarbon chain with at least 12 carbon atoms, which chain may be at least partially fluorinated, and which may be interrupted by heteroatoms and/or carbonyl groups.

    摘要翻译： 本发明涉及从金属模具中的塑料成型材料制造模制品的方法，包括用外部脱模剂涂覆模具的内壁的至少一部分，将塑性成型材料引入模具中 模具，以及从模具中除去产品的改进，其中外部脱模剂包含一种或多种有机化合物，所述分子含有统计平均值A）0.5至1.2个极性基团，所述极性基团选自-CN， -NC，-NCO，-CNO，-OCN，-SCN和-NCS和B）至少一个具有至少12个碳原子的非极性烃链，该链可以是至少部分氟化的，并且其可以被 杂原子和/或羰基。

    Device and process for producing plastic components, especially polyurethane moldings
    8.
    发明授权
    Device and process for producing plastic components, especially polyurethane moldings 失效
    用于生产塑料部件，特别是聚氨酯模制品的装置和工艺

    公开(公告)号：US6136238A

    公开(公告)日：2000-10-24

    申请号：US142445

    申请日：1998-09-04

    申请人： Werner Rasshofer ,  Henry Muller ,  Achim Symannek

    发明人： Werner Rasshofer ,  Henry Muller ,  Achim Symannek

    IPC分类号： B29C33/38 ,  B29C44/00 ,  B29K75/00 ,  B29K105/04 ,  C08G18/66 ,  C22C38/00 ,  C22C38/22 ,  C22C38/24 ,  C22C38/30 ,  C22C38/52 ,  B29C41/38 ,  B29C44/02

    CPC分类号： C08G18/6696 ,  B29C33/38 ,  C08G2101/0033 ,  C08G2125/00

    摘要： The present invention relates to a process for preparing solid, microcellular or expanded plastic molded items, characterized in that said molded items are produced in molds in which the internal surfaces consist of steel with the percentage composition:a) Fe: having a wt % greater than 0 wt % and less than 100 wt %;b) at least one element selected from the group consisting of W, Mo, or V, wherein if W is selected, W is present from a range greater than 0 wt % to 40 wt %; wherein if Mo is selected, Mo is present from a range greater than 0 wt % to 12 wt %; and if V is selected, V is present from a range greater than 0 wt % to 5 wt %;c) at least one element selected from the group consisting of Cr, Al, wherein if Cr is selected, Cr is present in a concentration of greater than 0 wt % to 15 wt %; and if Al is selected, Al is present in a concentration of greater than 0 wt % to 15 wt %;d) optionally, carbon at a concentration ranging from 0.1 to 1.5 wt %;e) optionally, cobalt at a concentration ranging from 0.1 to 10 wt %; andf) optionally, nitrogen in a nitriding layer at a concentration ranging from greater than 0 wt % to 10 wt %.

    摘要翻译： PCT No.PCT / EP97 / 00952 Sec。 371日期：1998年9月4日 102（e）1998年9月4日PCT PCT 1997年2月27日提交PCT公布。 第WO97 / 34021号公报 日期：1997年9月18日本发明涉及一种制备固体，微孔或膨胀塑料模塑制品的方法，其特征在于，所述模制品在模具中制造，其中内表面由具有百分比组成的钢组成：a）Fe： 重量％大于0重量％且小于100重量％; b）选自W，Mo或V中的至少一种元素，其中如果选择W，W存在于大于0重量％至40重量％的范围内; 其中如果选择Mo，则Mo在大于0重量％至12重量％的范围内存在; 并且如果选择V，则V从大于0重量％至5重量％的范围存在; c）选自Cr，Al中的至少一种元素，其中如果选择Cr，则Cr以大于0wt％至15wt％的浓度存在; 并且如果选择Al，则Al以大于0重量％至15重量％的浓度存在; d）任选地，浓度为0.1至1.5重量％的碳; e）任选地，浓度为0.1至10重量％的钴; 和f）任选地，氮化层中的氮浓度范围为大于0重量％至10重量％。

    Polyamine crosslinking agent formulation and its preparation
    9.
    发明授权
    Polyamine crosslinking agent formulation and its preparation 失效
    多胺交联剂配方及其制备

    公开(公告)号：US5705594A

    公开(公告)日：1998-01-06

    申请号：US767564

    申请日：1996-12-16

    申请人： Klaus Konig ,  Otto Neuner ,  Werner Rasshofer

    发明人： Klaus Konig ,  Otto Neuner ,  Werner Rasshofer

    IPC分类号： C07D251/34 ,  C08G59/50 ,  C08J3/24 ,  C08K5/3492 ,  C08L63/00 ,  C08L73/02 ,  C08L79/02 ,  C08G18/08 ,  C08G18/10

    CPC分类号： C08G59/5086 ,  C07D251/34

    摘要： Liquid polyamine crosslinking agent formulations based on trimerized toluylene 2,4- and/or 2,6-diisocyanate, with formation of an isocyanurate structure and hydrolysis of the isocyanate groups to amine groups, are described. The novel crosslinking agent formulations have a content of 40 to 80% of the total weight of the solids content of the crosslinking agent formulation of 1,3,5-tris-(3-amino-4-methyl-phenyl,2-methyl-3-aminophenyl) isocyanurate (I) which is not further condensed, and a content of not more than 1.0% of the total weight of the crosslinking agent formulations of toluylene-2,4- and/or -2,6-diamine (III). For the preparation, toluylene diisocyanate is trimerized, to form the isocyanurate structure, until 10 to 25% of the NCO groups have been reacted. The toluylene diisocyanate which has not undergone condensation is then distilled off, the bottom product formed by this operation is taken up directly in a solvent A and the 30 to 70% strength by weight solution formed by this procedure is metered into a hydrolysis in water/N,N-dialkyl-carboxylic acid amide in the presence of a catalytic amount of a basic catalyst. After the hydrolysis, the crosslinking agent formulations are brought to a solids content of 35 to 60% of the total weight of the formulation by distilling off a portion of the solvents and adding a solvent B.

    摘要翻译： 描述了基于三聚甲苯2,4-和/或2,6-二异氰酸酯的液态多胺交联剂制剂，其形成异氰脲酸酯结构和将异氰酸酯基团水解为胺基。 新型交联剂配方的含量为交联剂配方的1,3,5-三（3-氨基-4-甲基 - 苯基，2-甲基 - 苯基） - 苯胺的固体含量的总重量的40-80％ 3-氨基苯基）异氰脲酸酯（I），其不再进一步缩合，并且不大于甲苯-2,4-和/或-2,6-二胺（III）的交联剂配方的总重量的1.0重量％ ）。 为了制备，将甲苯二异氰酸酯进行三聚，形成异氰脲酸酯结构，直到10〜25％的NCO基团都已反应。 然后蒸馏除去未进行冷凝的甲苯二异氰酸酯，将通过该操作形成的底部产物直接溶于溶剂A中，并将通过该方法形成的30-70重量％的重量浓度的溶液计量加入水/ N，N-二烷基 - 羧酸酰胺在催化量的碱性催化剂存在下反应。 水解后，通过蒸馏掉一部分溶剂并加入溶剂B使交联剂配方的固体含量达到制剂总重量的35至60％。