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    Ore reduction process using carbon based materials having a low sulfur content and titanium oxide and iron metallization product therefrom
    1.
    发明授权
    Ore reduction process using carbon based materials having a low sulfur content and titanium oxide and iron metallization product therefrom 有权
    使用具有低硫含量的碳基材料和氧化钛的铁矿石还原工艺和由其制成的金属金属化产物

    公开(公告)号：US08372179B2

    公开(公告)日：2013-02-12

    申请号：US12680393

    申请日：2008-10-14

    申请人： John James Barnes ,  Stephen Erwin Lyke ,  Dat Nguyen ,  Joseph M. Shekiro, Jr. ,  Guangliang Liu

    发明人： John James Barnes ,  Stephen Erwin Lyke ,  Dat Nguyen ,  Joseph M. Shekiro, Jr. ,  Guangliang Liu

    IPC分类号： C22B1/16 ,  C22B7/04 ,  C21B13/10

    CPC分类号： C21B13/105 ,  C21B13/0046 ,  C21B13/006

    摘要： The present invention is one or more processes for producing separable iron and titanium oxides from an ore comprising titanium oxide and iron oxide, comprising: (a) forming agglomerates comprising carbon-based material and the ore, the quantity of carbon of the agglomerates being at least sufficient for forming a ferrous oxide-containing molten slag, at an elevated temperature; (b) introducing the agglomerates onto a bed of carbon-based material in a moving hearth furnace, wherein the carbon-based materials used for both the agglomerates and the bed have a low sulfur content; (c) heating the agglomerates in the moving hearth furnace to a temperature sufficient for liquefying the agglomerates to produce a liquid comprising ferrous oxide-containing slag; (d) metallizing the ferrous oxide of the slag by reaction of the ferrous oxide and the carbon of the carbon bed at a furnace temperature sufficient for maintaining the slag in a liquid state; (e) solidifying the slag after metallization of the ferrous oxide to form a matrix of titanium oxide-rich slag having a plurality of metallic iron granules distributed there through; and (f) separating the metallic iron granules from the slag, the slag comprising greater than 85% titanium dioxide based on the entire weight of the matrix after separation of the metallic iron.

    摘要翻译： 本发明是从包含氧化钛和氧化铁的矿石制备可分离的铁和氧化钛的一个或多个方法，包括：（a）形成包含碳基材料和矿石的附聚物，附聚物的碳量在 在升高的温度下至少足以形成含氧化亚铁的熔渣; （b）在移动的炉床炉中将附聚物引入到碳基材料床上，其中用于凝聚物和床的碳基材料具有低的硫含量; （c）将移动的炉床炉中的附聚物加热到足以使附聚物液化以产生包含含氧化亚铁的炉渣的液体的温度; （d）在炉渣温度足以使炉渣处于液态的情况下，通过氧化亚氮和碳床的碳的反应使炉渣的氧化亚金属化; （e）在氧化亚铁金属化之后固化炉渣，以形成富含氧化钛的炉渣的基体，其具有分布在其上的多个金属铁颗粒; 和（f）从矿渣中分离金属铁颗粒，在分离金属铁之后，炉渣基于基体的整个重量，包含大于85％的二氧化钛。

    ORE REDUCTION PROCESS USING CARBON BASED MATERIALS HAVING A LOW SULFUR CONTENT AND TITANIUM OXIDE AND IRON METALLIZATION PRODUCT THEREFROM
    2.
    发明申请
    ORE REDUCTION PROCESS USING CARBON BASED MATERIALS HAVING A LOW SULFUR CONTENT AND TITANIUM OXIDE AND IRON METALLIZATION PRODUCT THEREFROM 有权
    使用具有低硫含量和氧化钛的碳基材料的ORE还原过程和铁的金属化产物

    公开(公告)号：US20100237280A1

    公开(公告)日：2010-09-23

    申请号：US12680393

    申请日：2008-10-14

    申请人： John James Barnes ,  Stephen Erwin Lyke ,  Dat Nguyen ,  Joseph M. Shekiro, JR. ,  Guangliang Liu

    发明人： John James Barnes ,  Stephen Erwin Lyke ,  Dat Nguyen ,  Joseph M. Shekiro, JR. ,  Guangliang Liu

    IPC分类号： C22B34/12 ,  C09K3/00

    CPC分类号： C21B13/105 ,  C21B13/0046 ,  C21B13/006

    摘要： The disclosure is directed to a process for producing separable iron and titanium oxides from an ore comprising titanium oxide and iron oxide, comprising: (a) forming agglomerates comprising carbon-based material and the ore, the quantity of carbon of the agglomerates being at least sufficient for forming a ferrous oxide-containing molten slag, at an elevated temperature; (b) introducing the agglomerates onto a bed of carbon-based material in a moving hearth furnace, wherein the carbon-based materials used for both the agglomerates and the bed have a low sulfur content; (c) heating the agglomerates in the moving hearth furnace to a temperature sufficient for liquefying the agglomerates to produce a liquid comprising ferrous oxide-containing slag; (d) metallizing the ferrous oxide of the slag by reaction of the ferrous oxide and the carbon of the carbon bed at a furnace temperature sufficient for maintaining the slag in a liquid state; (e) solidifying the slag after metallization of the ferrous oxide to form a matrix of titanium oxide-rich slag having a plurality of metallic iron granules distributed there through; and (f) separating the metallic iron granules from the slag, the slag comprising greater than 85% titanium dioxide based on the entire weight of the matrix after separation of the metallic iron. The disclosure is also directed to a metallization product of a ferrous oxide-rich molten slag.

    摘要翻译： 本公开涉及从包含氧化钛和氧化铁的矿石制备可分离的铁和氧化钛的方法，包括：（a）形成包含碳基材料和矿石的附聚物，所述附聚物的碳量至少为 足以在升高的温度下形成含氧化亚铁的熔渣; （b）在移动的炉床炉中将附聚物引入到碳基材料床上，其中用于凝聚物和床的碳基材料具有低的硫含量; （c）将移动的炉床炉中的附聚物加热到足以使附聚物液化以产生包含含氧化亚铁的炉渣的液体的温度; （d）在炉渣温度足以使炉渣处于液态的情况下，通过氧化亚氮和碳床的碳的反应使炉渣的氧化亚金属化; （e）在氧化亚铁金属化之后固化炉渣，以形成富含氧化钛的炉渣的基体，其具有分布在其上的多个金属铁颗粒; 和（f）从矿渣中分离金属铁颗粒，在分离金属铁之后，炉渣基于基体的整个重量，包含大于85％的二氧化钛。 本公开还涉及富含氧化亚铁的熔渣的金属化产物。

    Ore reduction process and titanium oxide and iron metallization product
    3.
    发明授权
    Ore reduction process and titanium oxide and iron metallization product 有权
    矿石还原工艺和氧化钛和铁金属化产品

    公开(公告)号：US07780756B2

    公开(公告)日：2010-08-24

    申请号：US12430261

    申请日：2009-04-27

    申请人： John James Barnes ,  Stephen Erwin Lyke ,  Dat Nguyen ,  Akira Uragami ,  Isao Kobayashi ,  Mitsutaka Hino ,  Thomas Peter Battle ,  Joseph M. Shekiro, Jr.

    发明人： John James Barnes ,  Stephen Erwin Lyke ,  Dat Nguyen ,  Akira Uragami ,  Isao Kobayashi ,  Mitsutaka Hino ,  Thomas Peter Battle ,  Joseph M. Shekiro, Jr.

    IPC分类号： C22B1/14 ,  C22B1/00 ,  C22B1/16 ,  C21B3/04 ,  C21B13/10

    CPC分类号： C21B13/105 ,  C21B3/04 ,  C21B13/0046 ,  C21B13/006 ,  Y02W30/542 ,  Y10T428/12056

    摘要： The disclosure is directed to a process for producing separable iron and titanium oxides from an ore containing titanium oxide and ferric oxide, comprising: (a) forming agglomerates comprising carbon-based materials and the ore, the quantity of carbon of the agglomerates being sufficient for, at an elevated temperature, reducing ferric oxide to ferrous oxide and forming a ferrous oxide-rich molten slag, (b) introducing the agglomerates onto a carbon bed of a moving hearth furnace; (c) heating the agglomerates in the moving hearth furnace to a temperature sufficient for reducing and melting the agglomerates to produce a ferrous oxide-rich molten slag; (d) metallizing the ferrous oxide of the molten slag by reaction of the ferrous oxide and the carbon of the carbon bed at a furnace temperature sufficient for maintaining the slag in a molten state; and (e) solidifying the slag after metallization of the ferrous oxide to form a matrix of titanium oxide-rich slag having a plurality of metallic iron granules distributed there through; and (f) separating the metallic iron granules from the slag, the slag comprising greater than 85% titanium dioxide based on the entire weight of the matrix after separation of the metallic iron. The disclosure is also directed to a metallization product of a ferrous oxide-rich molten slag.

    摘要翻译： 本发明涉及从含有氧化钛和氧化铁的矿石中制备可分离的铁和钛氧化物的方法，其包括：（a）形成包含碳基材料和矿石的附聚物，附聚物的碳量足以 在升高的温度下，将氧化亚铁还原成氧化亚铁，形成富含氧化亚铁的熔渣，（b）将附聚物引入移动的炉底炉的碳床上; （c）将移动的炉底炉中的附聚物加热至足以减少和熔化附聚物以产生富含氧化亚铁的熔渣的温度; （d）在足以使炉渣处于熔融状态的炉温下，通过氧化亚氮和碳床的碳的反应使熔渣的氧化亚铁金属化; 和（e）在氧化亚铁金属化之后固化炉渣，以形成富含氧化钛的炉渣的基体，其具有分布在其上的多个金属铁颗粒; 和（f）从矿渣中分离金属铁颗粒，在分离金属铁之后，炉渣基于基体的整个重量，包含大于85％的二氧化钛。 本公开还涉及富含氧化亚铁的熔渣的金属化产物。

    ORE REDUCTION PROCESS AND TITANIUM OXIDE AND IRON METALLIZATION PRODUCT
    4.
    发明申请
    ORE REDUCTION PROCESS AND TITANIUM OXIDE AND IRON METALLIZATION PRODUCT 有权
    ORE还原工艺和氧化钛和铁金属化产品

    公开(公告)号：US20090217784A1

    公开(公告)日：2009-09-03

    申请号：US12430261

    申请日：2009-04-27

    申请人： John James Barnes ,  Stephen Erwin Lyke ,  Dat Nguyen ,  Mitsutaka Hino ,  Akira Uragami ,  Isao Kobayashi ,  Thomas Peter Battle ,  Joseph M. Shekiro, JR.

    发明人： John James Barnes ,  Stephen Erwin Lyke ,  Dat Nguyen ,  Mitsutaka Hino ,  Akira Uragami ,  Isao Kobayashi ,  Thomas Peter Battle ,  Joseph M. Shekiro, JR.

    IPC分类号： C22B1/14

    CPC分类号： C21B13/105 ,  C21B3/04 ,  C21B13/0046 ,  C21B13/006 ,  Y02W30/542 ,  Y10T428/12056

    摘要： The disclosure is directed to a process for producing separable iron and titanium oxides from an ore containing titanium oxide and ferric oxide, comprising: (a) forming agglomerates comprising carbon-based materials and the ore, the quantity of carbon of the agglomerates being sufficient for, at an elevated temperature, reducing ferric oxide to ferrous oxide and forming a ferrous oxide-rich molten slag, (b) introducing the agglomerates onto a carbon bed of a moving hearth furnace; (c) heating the agglomerates in the moving hearth furnace to a temperature sufficient for reducing and melting the agglomerates to produce a ferrous oxide-rich molten slag; (d) metallizing the ferrous oxide of the molten slag by reaction of the ferrous oxide and the carbon of the carbon bed at a furnace temperature sufficient for maintaining the slag in a molten state; and (e) solidifying the slag after metallization of the ferrous oxide to form a matrix of titanium oxide-rich slag having a plurality of metallic iron granules distributed there through; and (f) separating the metallic iron granules from the slag, the slag comprising greater than 85% titanium dioxide based on the entire weight of the matrix after separation of the metallic iron. The disclosure is also directed to a metallization product of a ferrous oxide-rich molten slag.

    摘要翻译： 本发明涉及从含有氧化钛和氧化铁的矿石中制备可分离的铁和钛氧化物的方法，其包括：（a）形成包含碳基材料和矿石的附聚物，附聚物的碳量足以 在升高的温度下，将氧化亚铁还原成氧化亚铁，形成富含氧化亚铁的熔渣，（b）将附聚物引入移动的炉底炉的碳床上; （c）将移动的炉底炉中的附聚物加热至足以减少和熔化附聚物以产生富含氧化亚铁的熔渣的温度; （d）在足以使炉渣处于熔融状态的炉温下，通过氧化亚氮和碳床的碳的反应使熔渣的氧化亚铁金属化; 和（e）在氧化亚铁金属化之后固化炉渣，以形成富含氧化钛的炉渣的基体，其具有分布在其上的多个金属铁颗粒; 和（f）从矿渣中分离金属铁颗粒，在分离金属铁之后，炉渣基于基体的整个重量，含有大于85％的二氧化钛。 本公开还涉及富含氧化亚铁的熔渣的金属化产物。

    Refractory lining for titanium ore beneficiation
    5.
    发明授权
    Refractory lining for titanium ore beneficiation 有权
    钛矿选矿耐火衬里

    公开(公告)号：US08569191B2

    公开(公告)日：2013-10-29

    申请号：US13318614

    申请日：2010-05-05

    申请人： John James Barnes ,  Dat Nguyen ,  Peter Hill ,  Jay Scott Schickling

    发明人： John James Barnes ,  Dat Nguyen ,  Peter Hill ,  Jay Scott Schickling

    IPC分类号： C04B35/106

    CPC分类号： C22B1/02 ,  C21B13/006 ,  C21B13/105 ,  C22B34/1209 ,  F27B9/16 ,  F27D1/0006 ,  F27D1/1684

    摘要： The disclosure relates to a refractory which is resistant to corrosion which degrades the refractory during titanium-ore beneficiation in a furnace, particularly a rotary hearth furnace. In particular, the disclosure relates to a layered refractory lining for a furnace, for use in a titanium ore beneficiation process wherein a titanium oxide-rich molten slag is formed, comprising: (a) a first layer comprising a major proportion of alumina and a minor proportion of zirconia; (b) a second layer comprising a resistant agent for the molten slag; wherein the second layer is between the slag and the first layer.

    摘要翻译： 本公开涉及耐腐蚀性耐火材料，其在炉，特别是转底炉中的钛矿选矿过程中使耐火材料劣化。 特别地，本公开涉及一种用于炉的层状耐火衬层，其用于钛矿选矿工艺中，其中形成富含氧化钛的熔渣，包括：（a）第一层，其包含主要比例的氧化铝和 次要比例的氧化锆; （b）第二层，包括用于熔渣的抗性剂; 其中所述第二层位于所述炉渣和所述第一层之间。

    REFRACTORY LINING FOR TITANIUM ORE BENEFICIATION
    6.
    发明申请
    REFRACTORY LINING FOR TITANIUM ORE BENEFICIATION 有权
    用于钛金属受益的耐火衬里

    公开(公告)号：US20120064371A1

    公开(公告)日：2012-03-15

    申请号：US13318614

    申请日：2010-05-05

    申请人： John James Barnes ,  Dat Nguyen ,  Peter Hill ,  Jay Scott Schickling

    发明人： John James Barnes ,  Dat Nguyen ,  Peter Hill ,  Jay Scott Schickling

    IPC分类号： B32B19/00 ,  C04B35/49

    CPC分类号： C22B1/02 ,  C21B13/006 ,  C21B13/105 ,  C22B34/1209 ,  F27B9/16 ,  F27D1/0006 ,  F27D1/1684

    摘要： The disclosure relates to a refractory which is resistant to corrosion which degrades the refractory during titanium-ore beneficiation in a furnace, particularly a rotary hearth furnace. In particular, the disclosure relates to a layered refractory lining for a furnace, for use in a titanium ore beneficiation process wherein a titanium oxide-rich molten slag is formed, comprising: (a) a first layer comprising a major proportion of alumina and a minor proportion of zirconia; (b) a second layer comprising a resistant agent for the molten slag; wherein the second layer is between the slag and the first layer.

    摘要翻译： 本公开涉及耐腐蚀性耐火材料，其在炉，特别是转底炉中的钛矿选矿过程中使耐火材料劣化。 特别地，本公开涉及一种用于炉的层状耐火衬层，其用于钛矿选矿工艺中，其中形成富含氧化钛的熔渣，包括：（a）第一层，其包含主要比例的氧化铝和 次要比例的氧化锆; （b）第二层，包括用于熔渣的抗性剂; 其中所述第二层位于所述炉渣和所述第一层之间。