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    Optical semiconductor sealing material
    6.
    发明授权
    Optical semiconductor sealing material 失效
    光学半导体密封材料

    公开(公告)号：US08648160B2

    公开(公告)日：2014-02-11

    申请号：US13587250

    申请日：2012-08-16

    申请人： Tomoaki Takebe ,  Tsuyoshi Ota ,  Yutaka Obata ,  Hiroyuki Higuchi

    发明人： Tomoaki Takebe ,  Tsuyoshi Ota ,  Yutaka Obata ,  Hiroyuki Higuchi

    IPC分类号： C08F220/10 ,  C08F220/28

    CPC分类号： C08F220/10 ,  C08F220/18 ,  C08F220/28 ,  C09J133/14 ,  H01L31/0203

    摘要： The present invention provides an optical semiconductor sealing material comprising a radically polymerized polymer of a methacrylate ester having an alicyclic hydrocarbon group containing 7 or more carbon atoms, e.g. an adamantyl group, a norbornyl group, or a dicyclopentanyl group; and an optical semiconductor sealing material comprising a radically polymerized polymer of 50 to 97 mass % of the methacrylate ester and 3 to 50 mass % of acrylate ester having a hydroxyl group. The optical semiconductor sealing material of the present invention is highly transparent and stable to UV light and thus does not undergo yellowing. In addition, the material exhibits excellent compatibility between heat resistance and refractive index, does not undergo deformation or cracking during heating processes such as reflow soldering, and shows high processability. The material can be preferably used as a sealing material for light-emitting elements and light-receiving elements of optical semiconductor devices (semiconductor light-emitting devices).

    摘要翻译： 本发明提供一种光学半导体密封材料，其包含具有含有7个或更多个碳原子的脂环族烃基的甲基丙烯酸酯的自由基聚合的聚合物， 金刚烷基，降冰片基或二环戊基; 以及包含50〜97质量％的甲基丙烯酸酯的自由基聚合物和3〜50质量％的具有羟基的丙烯酸酯的光学半导体密封材料。 本发明的光半导体密封材料高度透明，对紫外光稳定，因此不会发黄。 此外，该材料在耐热性和折射率之间表现出优异的相容性，在诸如回流焊接的加热过程中不会发生变形或开裂，并且显示出高加工性。 该材料可以优选用作光半导体器件（半导体发光器件）的发光元件和光接收元件的密封材料。

    Solid catalyst components for olefin polymerization, catalysts for olefin polymerization and process for producing olefin polymers
    8.
    发明授权
    Solid catalyst components for olefin polymerization, catalysts for olefin polymerization and process for producing olefin polymers 失效
    用于烯烃聚合的固体催化剂组分，用于烯烃聚合的催化剂和用于生产烯烃聚合物的方法

    公开(公告)号：US06331620B1

    公开(公告)日：2001-12-18

    申请号：US09463999

    申请日：2000-02-22

    申请人： Yasunori Kadoi ,  Tsuyoshi Ota ,  Toshio Isozaki ,  Kiyokazu Katayama ,  Takanori Sadashima

    发明人： Yasunori Kadoi ,  Tsuyoshi Ota ,  Toshio Isozaki ,  Kiyokazu Katayama ,  Takanori Sadashima

    IPC分类号： C08F200

    CPC分类号： C08F10/00 ,  C08F110/06 ,  C08F4/6548 ,  C08F4/651 ,  C08F2500/15 ,  C08F2500/17

    摘要： Solid catalyst components for the polymerization of olefins, comprising titanium, magnesium and a compound of general formula (I), wherein R1 and R2 may be the same or different and each represents a linear or branched hydrocarbon group having 1 to 20 carbon atoms, and n is an integer of 1 to 10, as an electron donor, which are combined with organoaluminum compounds to form polymerization catalysts for the production of olefin polymers. This electron donor has no problems of safety and hygiene, and is inexpensive and easily synthesized. This compound can provide highly active and highly stereoregular solid catalyst components for the polymerization of olefins, catalysts for the polymerization of olefins, and processes for producing olefin polymers.

    摘要翻译： 用于烯烃聚合的固体催化剂组分，包括钛，镁和通式（I）的化合物，其中R 1和R 2可以相同或不同，并且各自表示具有1至20个碳原子的直链或支链烃基，和 n为1〜10的整数，作为电子给体，与有机铝化合物结合形成用于制备烯烃聚合物的聚合催化剂。 该电子给体没有安全和卫生的问题，并且便宜且易于合成。 该化合物可以为烯烃的聚合，烯烃聚合用催化剂和烯烃聚合物的制备方法提供高活性和高度立构规整的固体催化剂组分。

    Propylene/ethylene block copolymer
    9.
    发明授权
    Propylene/ethylene block copolymer 有权
    丙烯/乙烯嵌段共聚物

    公开(公告)号：US06201090B1

    公开(公告)日：2001-03-13

    申请号：US09463983

    申请日：2000-02-16

    申请人： Takashi Sumitomo ,  Sueto Miyazaki ,  Tsuyoshi Ota ,  Kazuo Sato

    发明人： Takashi Sumitomo ,  Sueto Miyazaki ,  Tsuyoshi Ota ,  Kazuo Sato

    IPC分类号： C08F21000

    CPC分类号： C08F297/083

    摘要： Provided are propylene-ethylene block copolymers having the advantage of well-balanced physical properties of rigidity, impact resistance, etc. The propylene-ethylene block copolymers are characterized by (a), (b), (c1), (c2) and (c3): (a) The melt flow rate falls between 0.01 and 1000 g/10 min. (b) The room-temperature xylene-insoluble component has an [mmmm] fraction of not smaller than 98.9%. (cl) The amount of the room-temperature xylene-soluble component falls between 3 and 50% by weight. (c2) The T1 relaxation time component in pulse NMR is of a single relaxation component. (c3) The ethylene content, x % by weight, as measured through 13C-NMR, and the T1 relaxation time satisfy y≦0.0014x3−0.0897x2−1.0593x +231.6. The block copolymers may be characterized by (a), (b), (c1) and (c4): (a) The melt flow rate falls between 0.01 and 1000 g/10 min. (b) The room-temperature xylene-insoluble component has an [mmmm] fraction of not smaller than 98.9%. (c1) The amount of the room-temperature xylene-soluble component falls between 3 and 50 % by weight. (c4) The ethylene content, x% by weight, and the ratio by weight of the crystalline polyethylene segments to the total of the ethylene-propylene copolymer segments and the crystalline polyethylene segments, z (%), as obtained from the TEM (transmission electron microscope) image of the propylene-ethylene block copolymers, satisfy 2≦0.016x2−0.069x−1.34.

    摘要翻译： 丙烯 - 乙烯嵌段共聚物的特征在于（a），（b），（c1），（c2）和（c2）和 c3）：（a）熔体流动速率为0.01-1000g / 10min。 （b）室温二甲苯不溶成分的[mmmm]分数不小于98.9％。 （c1）室温二甲苯可溶成分的量为3〜50重量％。 （c2）脉冲NMR中的T1弛豫时间分量是单个弛豫分量。 （c3）通过13 C-NMR测量的乙烯含量，x重量％，以及T1弛豫时间满足y <= 0.0014×3-0.0897x2-1.0593x + 231.6。嵌段共聚物的特征可以是（a）， （b），（c1）和（c4）：（a）熔体流动速率为0.01-1000g / 10min。 （b）室温二甲苯不溶成分的[mmmm]分数不小于98.9％。 （c1）室温二甲苯可溶成分的量为3〜50重量％。 （c4）从TEM（透射率）获得的乙烯含量，x重量％以及结晶聚乙烯链段的重量比与乙烯 - 丙烯共聚物链段和结晶聚乙烯链段的总和z（％） 电子显微镜）图像的丙烯 - 乙烯嵌段共聚物满足2 <= 0.016x2-0.069x-1.34。

    (Meth)acrylate copolymer for syrup and resin composition thereof
    10.
    发明授权
    (Meth)acrylate copolymer for syrup and resin composition thereof 有权
    （甲基）丙烯酸酯共聚物和其树脂组合物

    公开(公告)号：US08138287B2

    公开(公告)日：2012-03-20

    申请号：US12515757

    申请日：2007-11-19

    申请人： Tsuyoshi Ota ,  Shinichi Yukimasa ,  Yutaka Obata ,  Tomoaki Takebe

    发明人： Tsuyoshi Ota ,  Shinichi Yukimasa ,  Yutaka Obata ,  Tomoaki Takebe

    IPC分类号： C08F230/08 ,  C08F220/10 ,  C08F220/26

    CPC分类号： C08F265/04 ,  C08F220/10 ,  C08F220/26 ,  C08F265/06 ,  C08F285/00 ,  C08F290/06 ,  C08F290/061 ,  C08F290/068 ,  C08L51/003 ,  C08F220/16 ,  C08L2666/02

    摘要： The present invention provides a copolymer for syrup, characterized by being formed from (A) 1 to 60 mass % of at least one (meth)acrylate compound selected from among a (meth)acrylate-modified silicone oil, an alkyl(meth)acrylate, a monoalkylene glycol(meth)acrylate, and a polyalkylene glycol(meth)acrylate, and (B) 99 to 40 mass % of a (meth)acrylate compound having a C≧6 alicyclic hydrocarbon group bonded thereto via an ester bond; a (meth)acrylate composition containing a (meth)acrylate monomer and 1 to 60 mass % of the (meth)acrylate copolymer for syrup; and a cured product of the composition. The (meth)acrylate copolymer for syrup of the present invention has excellent solubility, particularly in a (meth)acrylate compound having an alicyclic ester substituent, and a (meth)acrylate resin composition containing the copolymer provides a stable cured product having high transparency and high resistance to UV rays and heat. Thus, the cured product is suitably used as a material for lenses, illumination devices, automobiles, displays, optical-semiconductors, etc.

    摘要翻译： 本发明提供一种用于糖浆的共聚物，其特征在于由（A）1至60质量％的至少一种（甲基）丙烯酸酯改性硅油，（甲基）丙烯酸烷基酯 ，（甲基）丙烯酸单亚烷基二醇酯，（甲基）丙烯酸聚亚烷基二醇酯，（B）99〜40质量％的具有通过酯键与C键6的脂肪族烃基结合的（甲基）丙烯酸酯化合物; 含有（甲基）丙烯酸酯单体和1〜60质量％的（甲基）丙烯酸酯共聚物的（甲基）丙烯酸酯组合物， 和该组合物的固化产物。 本发明的用于糖浆的（甲基）丙烯酸酯共聚物具有优异的溶解性，特别是在具有脂环族酯取代基的（甲基）丙烯酸酯化合物中，含有共聚物的（甲基）丙烯酸酯树脂组合物提供了具有高透明度的稳定的固化产物， 高耐紫外线和热量。 因此，固化物适合用作透镜，照明装置，汽车，显示器，光学半导体等的材料。