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1.发明申请公开(公告)号：US20140076070A1
公开(公告)日：2014-03-20
申请号：US13629723
申请日：2012-09-28
IPC分类号： G01N1/28
CPC分类号： G01N1/28 , B01J20/264 , B01J20/28042 , B01J20/28047 , B01J20/28085 , B01J20/291 , B01J2220/86 , G01N2001/4061
摘要： The present invention provides a monolithic silicone in the form of an aerogel or a xerogel having flexibility and capable of dissolving molecules of a substance. This silicone monolithic body having continuous through passages is synthesized by copolymerizing starting materials of both a bifunctional alkoxysilane and a trifunctional alkoxysilane or tri- or higher functional alkoxysilanes through a sol-gel reaction for forming a Si—O network while causing phase separation.
摘要翻译： 本发明提供了具有柔性并能够溶解物质分子的气凝胶或干凝胶形式的整体硅胶。 具有连续通过的硅胶整体通过使双官能烷氧基硅烷和三官能烷氧基硅烷或三官能或更高官能的烷氧基硅烷的起始物质通过溶胶 - 凝胶反应共聚而形成Si-O网络而合成，同时引起相分离。
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2.发明授权公开(公告)号：US09285300B2
公开(公告)日：2016-03-15
申请号：US13629723
申请日：2012-09-28
CPC分类号： G01N1/28 , B01J20/264 , B01J20/28042 , B01J20/28047 , B01J20/28085 , B01J20/291 , B01J2220/86 , G01N2001/4061
摘要： The present invention provides a monolithic silicone in the form of an aerogel or a xerogel having flexibility and capable of dissolving molecules of a substance. This silicone monolithic body having continuous through passages is synthesized by copolymerizing starting materials of both a bifunctional alkoxysilane and a trifunctional alkoxysilane or tri- or higher functional alkoxysilanes through a sol-gel reaction for forming a Si—O network while causing phase separation.
摘要翻译： 本发明提供了具有柔性并能够溶解物质分子的气凝胶或干凝胶形式的整体硅胶。 具有连续通过的硅胶整体通过使双官能烷氧基硅烷和三官能烷氧基硅烷或三官能或更高官能的烷氧基硅烷的起始物质通过溶胶 - 凝胶反应共聚而形成Si-O网络而合成，同时引起相分离。
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3.发明申请Process for Producing Organic Porous Material and Organic Porous Column and Organic Porous Material 审中-公开生产有机多孔材料和有机多孔柱和有机多孔材料的方法公开(公告)号：US20090178966A1
公开(公告)日：2009-07-16
申请号：US12083208
申请日：2006-10-06
CPC分类号： C08F6/003 , B01J20/26 , B01J20/28083 , B01J20/28085 , B01J20/28092 , B01J20/285 , C08F2/38 , C08F4/00 , C08J9/28 , C08J2201/0502
摘要： An organic porous material is provided being excellent in mechanical properties such as strength and in which structures of a skeleton and pores are controlled more precisely. By a production process including (i) subjecting a low molecular compound having living radical and/or anionic polymerizability to living radical or anionic polymerization in a system including the compound, an organic polymer as a phase separation inducing component, a polymerization initiator, and a polymerization solvent, and thereby forming a gel including a skeletal phase rich in a polymer of the compound and a solvent phase rich in the solvent and having a co-continuous structure formed of the skeletal and solvent phases, and (ii) removing the solvent from the gel thus formed to form a skeleton containing the polymer as a base material thereof from the skeletal phase while forming first pores from the solvent phase, and thereby obtaining an organic porous material with a co-continuous structure formed of the skeleton and the first pores.
摘要翻译： 提供了机械性能如强度优异的有机多孔材料，并且更精确地控制骨架和孔的结构。 通过包括（i）在包含该化合物的体系中使具有活性自由基和/或阴离子聚合性的低分子化合物进行活性自由基或阴离子聚合的生产方法，作为相分离诱导组分的有机聚合物，聚合引发剂和 聚合溶剂，从而形成凝胶，其包含富含化合物的聚合物的骨架相和富含溶剂的溶剂相，并且具有由骨架和溶剂相形成的共连续结构，和（ii）从 由此形成凝胶，从骨架相形成含有作为其基材的聚合物的骨架，同时从溶剂相形成第一孔，从而获得由骨架和第一孔形成的共连续结构的有机多孔材料 。
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4.发明申请Method for Producing Alkylsiloxane Aerogel, Alkylsiloxane Aerogel, Apparatus for Producing Same, and Method for Manufacturing Panel Containing Same 审中-公开烷基硅氧烷气凝胶的制造方法，烷基硅氧烷气凝胶，其制造装置及其制造方法公开(公告)号：US20090104401A1
公开(公告)日：2009-04-23
申请号：US11989042
申请日：2006-07-19
CPC分类号： C08G77/04 , C08G77/06 , Y10T428/24273
摘要： A method for producing an alkylsiloxane aerogel of the invention includes (a) a step of letting a reaction to produce a sol and a reaction to convert the sol to a gel take place in one step by adding a silicon compound whose molecules have a hydrolysable functional group and a nonhydrolysable functional group to an acidic aqueous solution containing a surfactant, and (b) a step of drying the gel produced in the step (a). In the step (b), the gel is dried at a temperature and a pressure below the critical point of a solvent used to dry the gel.
摘要翻译： 制备本发明的烷基硅氧烷气凝胶的方法包括：（a）通过加入分子具有可水解官能团的硅化合物，在一个步骤中进行产生溶胶的反应和将溶胶转化为凝胶的反应的步骤 和含有表面活性剂的酸性水溶液的非水解性官能团，和（b）干燥步骤（a）中生成的凝胶的步骤。 在步骤（b）中，将凝胶在低于用于干燥凝胶的溶剂的临界点的温度和压力下干燥。
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公开(公告)号：US20070154379A1
公开(公告)日：2007-07-05
申请号：US11599015
申请日：2006-11-14
IPC分类号： C01B33/12
CPC分类号： C01B33/1585
摘要： Silica aerogels that are controlled in pore diameter and pore diameter distribution can be produced as follows: a surfactant is dissolved in an acidic aqueous solution; a silicon compound having a hydrolysable functional group and a hydrophobic functional group is added thereto, so that a hydrolysis reaction is carried out to yield a gel; and after the gel is solidified, the gel is dried supercritically. Preferably, the surfactant is one selected from the group consisting of a nonionic surfactant, a cationic surfactant, and an anionic surfactant, or a mixture of at least two of them. The silica aerogels produced as described above are usable for heat insulators for solar-heat collector panels or heat-insulating window materials for housing.
摘要翻译： 孔径和孔径分布控制的二氧化硅气凝胶可以如下制备：将表面活性剂溶解在酸性水溶液中; 向其中加入具有可水解官能团和疏水官能团的硅化合物，进行水解反应以产生凝胶; 凝胶凝固后，凝胶被超临界干燥。 优选地，表面活性剂选自非离子表面活性剂，阳离子表面活性剂和阴离子表面活性剂，或它们中至少两种的混合物。 如上所述生产的二氧化硅气凝胶可用于太阳能集热板或用于壳体的绝热窗材料的隔热材料。
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公开(公告)号：US20070077409A1
公开(公告)日：2007-04-05
申请号：US11520738
申请日：2006-09-14
申请人： Takayuki Hirano , Nobuyuki Kawakami , Takeharu Tanaka , Tetsuo Suzuki , Yoshito Fukumoto , Kazuki Nakanishi , Kazuyoshi Kanamori
发明人： Takayuki Hirano , Nobuyuki Kawakami , Takeharu Tanaka , Tetsuo Suzuki , Yoshito Fukumoto , Kazuki Nakanishi , Kazuyoshi Kanamori
CPC分类号： H05K3/0011 , B32B21/04 , H05K1/024 , H05K1/0306 , H05K2201/0116 , Y10T428/249953 , Y10T428/249969
摘要： The porous substrate, comprises: three-dimensional-network skeletal solid phase inside the substrate, and a skin layer same in quality as the skeletal solid phase formed on at least one surface of the substrate, and a production method thereof, comprising: forming a wet gel having a three-dimensional-network skeletal solid phase and a fluid phase rich in solvent that are separated from each other in a space between a pair of flat plates by sol-gel reaction, removing the solvent in the wet gel by drying, and removing at least one flat plate of the pair of flat plates.
摘要翻译： 多孔基材包括：基材内部的三维网状骨架固相，和在基材的至少一个表面上形成的骨架固相质量相同的皮肤层及其制造方法，其特征在于， 湿凝胶，其具有通过溶胶 - 凝胶反应在一对平板之间的空间中彼此分离的富含溶剂的三维网络骨架固相和流体相，通过干燥除去湿凝胶中的溶剂， 以及去除所述一对平板中的至少一个平板。
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公开(公告)号：US07291383B2
公开(公告)日：2007-11-06
申请号：US11049280
申请日：2005-02-02
申请人： Kazuki Nakanishi , Shigeru Hanzawa , Yousuke Sato
发明人： Kazuki Nakanishi , Shigeru Hanzawa , Yousuke Sato
CPC分类号： B01J20/28097 , B01D15/22 , B01J20/08 , B01J20/103 , B01J20/28045 , B01J20/284 , B01J20/287 , B01J2220/86 , G01N1/405 , G01N30/603 , Y10T428/249953 , Y10T428/249957 , Y10T428/249969
摘要： A support for solid phase extraction is provided for preventing the fracture of the porous body of the support and the space between the porous body and its container, and for processing various amounts of liquids to be processed while maintaining the ease of passage of liquid in use. The support for solid phase extraction comprises a ceramic substrate with one or more holes formed therein, and an inorganic porous material, filled in the hole or holes, which is produced by sol-gel transition accompanied by phase transition.
摘要翻译： 提供固相萃取用支撑体，用于防止支撑体的多孔体的破裂以及多孔体与容器之间的空间，并且用于处理各种量的待处理液体，同时保持使用中液体易于通过 。 固相萃取的载体包括其中形成有一个或多个孔的陶瓷基体和填充在孔或孔中的无机多孔材料，其通过伴随相变的溶胶 - 凝胶转变而产生。
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公开(公告)号：US20050063890A1
公开(公告)日：2005-03-24
申请号：US10481231
申请日：2002-06-28
申请人： Kazuki Nakanishi
发明人： Kazuki Nakanishi
CPC分类号： C01B33/124 , C01B33/163
摘要： Disclosed is a method for producing an inorganic porous body having precisely controlled macropores concurrently with mesopores of a narrow pore size distribution. The method comprises dissolving an amphiphilic substance as template component in an aqueous solution containing a sol-gel reaction catalyst, adding an inorganic low molecular weight compound having hydrolysable functional groups to the solution, forming a gel including a solvent-rich phase for the macropores, drying the gel to remove the solvent, and removing the template component by such means as thermal decomposition.
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公开(公告)号：US07217359B2
公开(公告)日：2007-05-15
申请号：US10894222
申请日：2004-07-19
申请人： Kazuki Nakanishi , Shigeru Hanzawa , Yousuke Sato
发明人： Kazuki Nakanishi , Shigeru Hanzawa , Yousuke Sato
IPC分类号： B01D15/08
CPC分类号： B01J20/28045 , B01D15/22 , B01J20/283 , G01N30/6043 , G01N2030/528
摘要： The present invention provides a column for a liquid chromatograph having a honeycomb substrate including holes through which a sample flows and a separation phase filled in the holes. The separation phase is a porous bone structure composed of an inorganic material having open pores formed therein, and the porous bone structure is generated by a sol-gel transition process accompanied by a phase transition.
摘要翻译： 本发明提供了一种液相色谱柱，其具有蜂窝状基材，该蜂窝基材包括样品流过的孔和填充在孔中的分离相。 分离相是由其中形成有开孔的无机材料构成的多孔骨结构，并且通过伴随相变的溶胶 - 凝胶转变过程产生多孔骨结构。
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公开(公告)号：US20050285290A1
公开(公告)日：2005-12-29
申请号：US11188699
申请日：2005-07-26
申请人： Kazuki Nakanishi
发明人： Kazuki Nakanishi
CPC分类号： C01B37/02 , B01J20/28047 , B01J20/28078 , B01J20/28083 , B01J20/28085 , B01J20/2809 , B01J20/28092 , B01J20/283 , B01J20/287 , B01J20/291 , C07F7/0874
摘要： In a method of manufacturing an organic/inorganic hybrid porous material containing both mesopores and macropores, a homogenous solution is prepared where a water-soluble polymer or amphipathic material as a phase separation induction element is dissolved in an aqueous solution containing sol-gel reaction catalyst elements, and a continuous 3-dimensional mesh-structured gel including a solvent-rich phase is formed. The gel is immersed in an aqueous solution containing a compound generating ammonia via hydrolysis and curing under hydrothermal conditions by heating in a closed state to form macropores by drying the gel and to evaporate the solvent from the solvent rich phase. Mesopores is formed in the skeletal phase by removing the phase separation induction elements from the gel after drying via thermolysis or extraction.
摘要翻译： 在制造含有中孔和大孔的有机/无机混合多孔材料的方法中，制备均匀的溶液，其中将作为相分离诱导元素的水溶性聚合物或两亲性材料溶解在含有溶胶 - 凝胶反应催化剂的水溶液中 形成包含富溶相的连续3维网状结构凝胶。 将凝胶浸入含有通过在水热条件下水解和固化的化合物生成氨的水溶液中，通过在封闭状态下加热以形成大孔，通过干燥凝胶并使溶剂从富溶相中蒸发。 通过热分解或萃取干燥后，通过从凝胶中除去相分离诱导元素，在骨架相中形成中孔。
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