-
公开(公告)号：US07022842B2
公开(公告)日：2006-04-04
申请号：US10450450
申请日：2001-03-07
IPC分类号： C07B43/06 , C07D205/08
CPC分类号： C07D201/08 , Y02P20/582
摘要： It is an object of the present invention to provide a method for synthesizing β-lactams and a method for manufacturing β-lactams in water of high-temperature and under high-pressure, and the present invention relates to a β-lactam synthesis method which is characterized in that β-lactams are synthesized by reacting β-amino acids in water at high-temperature and under high-pressure, this method being further characterized in that β-lactams are synthesized at a high speed by cyclizing β-amino acids in water at high-temperature and under high-pressure in which the temperature range is 200° C. or higher and the pressure range is 10 MPa or greater, and the present invention also relates to a method for manufacturing β-lactams which is characterized in that β-lactams are synthesized by reacting β-amino acids in water at high-temperature and under high-pressure, and are then separated and purified using a column separation medium.
摘要翻译： 本发明的一个目的是提供一种合成β-内酰胺的方法和一种在高温和高压水中制备β-内酰胺的方法，本发明涉及一种β-内酰胺合成方法， 其特征在于β-内酰胺是通过在高温和高压下在水中使β-氨基酸反应合成的，该方法的进一步特征在于通过使β-氨基酸在高温和高压下环化β-氨基酸来高速合成β-内酰胺 在温度范围为200℃以上且压力范围为10MPa以上的高温高压下的水，本发明还涉及β-内酰胺的制造方法，其特征在于， 该β-内酰胺通过在高温和高压下在水中使β-氨基酸反应合成，然后使用柱分离介质分离和纯化。
-
2.发明授权Method of introducing amino group and method of synthesizing amino acid compound 失效引入氨基的方法和合成氨基酸化合物的方法公开(公告)号：US07071350B2
公开(公告)日：2006-07-04
申请号：US10450157
申请日：2001-10-30
IPC分类号： C07C61/00 , C07C229/00 , C07C205/00
CPC分类号： C07C227/08 , C07C227/40 , C07C229/08 , C07C229/24 , C07C229/26
摘要： The present invention relates to a method for introducing an amino group into an organic acid or an organic ester by reacting an organic salt or an organic ester and ammonia under high-temperature and high-pressure water conditions, a method for synthesizing an amino acid or an amino ester by the above method, and a method for manufacturing an amino acid compound by synthesizing an amino acid or an amino ester by the above method and separating and refining it with an ion exchange resin.
摘要翻译： 本发明涉及通过有机盐或有机酯与氨在高温高压水条件下反应而将氨基引入有机酸或有机酯的方法，用于合成氨基酸或 通过上述方法的氨基酯，以及通过用上述方法合成氨基酸或氨基酯制备氨基酸化合物的方法，并用离子交换树脂分离和精制。
-
公开(公告)号：US06750336B2
公开(公告)日：2004-06-15
申请号：US10285571
申请日：2002-11-01
申请人： Osamu Sato , Kiyotaka Hatakeda , Yutaka Ikushima , Kazuo Torii
发明人： Osamu Sato , Kiyotaka Hatakeda , Yutaka Ikushima , Kazuo Torii
IPC分类号： C07D20104
CPC分类号： C07D201/04 , Y02P20/582
摘要： A method for producing a lactam by using an organic solvent as a substrate solution, which makes it possible to introduce a high-concentration oxime into flowing high-temperature and high-pressure water, thereby allowing the high-concentration lactam to be synthesized with a high efficiency. With this method, the lactam is continuously synthesized at a high rate from the oxime under high-temperature and high-pressure water mixture conditions within a temperature range of no less than 250° C. and a pressure range of no less than 15 MPa.
摘要翻译： 通过使用有机溶剂作为底物溶液制备内酰胺的方法，可以将高浓度肟引入流动的高温高压水中，从而使高浓度的内酰胺与 高效率。 通过该方法，在不低于250℃的温度范围和不低于15MPa的压力范围内，在高温和高压水混合条件下，从肟连续合成内酰胺。
-
公开(公告)号：US07084269B2
公开(公告)日：2006-08-01
申请号：US10471750
申请日：2002-03-05
申请人： Kiyotaka Hatakeda , Osamu Sato , Yutaka Ikushima , Kazuo Torii
发明人： Kiyotaka Hatakeda , Osamu Sato , Yutaka Ikushima , Kazuo Torii
IPC分类号： C07D201/04
CPC分类号： C07D201/04
摘要： It is an object of the present invention to provide an efficient method of continuously producing a lactam in high-temperature high-pressure water, and the present invention relates to a method of producing a lactam characterized by efficiently synthesizing the lactam while suppressing oxime hydrolysis by introducing an oxime as a reaction substrate and an acid into a reaction zone through which high-temperature high-pressure water is flowing, or introducing an oxime into flowing high-temperature high-pressure water containing an acid, thus raising the temperature of the reaction substrate to put the reaction substrate into a prescribed high-temperature high-pressure state within a short time and subjecting the reaction substrate to reaction; through the method, the lactam can be efficiently and continuously synthesized at a high rate from the oxime using an acid catalyst in water at a high temperature of at least 250° C. and a high pressure of at least 15 MPa.
摘要翻译： 本发明的目的是提供一种在高温高压水中连续生产内酰胺的有效方法，本发明涉及一种制备内酰胺的方法，其特征在于在抑制肟水解的同时有效地合成内酰胺 将肟作为反应基质和酸引入高温高压水流过的反应区，或将肟引入流入含有酸的高温高压水中，从而提高反应温度 将反应基材在短时间内放入规定的高温高压状态，使反应基板反应; 通过该方法，可以使用酸催化剂在高温下在高温至少250℃，高压至少15MPa的水中，以高速从肟高效连续地合成内酰胺。
-
公开(公告)号：US07045622B2
公开(公告)日：2006-05-16
申请号：US10469533
申请日：2001-03-23
申请人： Kiyotaka Hatakeda , Osamu Sato , Yutaka Ikushima , Kazuo Torii
发明人： Kiyotaka Hatakeda , Osamu Sato , Yutaka Ikushima , Kazuo Torii
IPC分类号： C07D201/04 , C07D223/10
CPC分类号： C07D201/06 , C07D201/04 , C07D223/10
摘要： It is an object of the present invention to provide a method of continuously producing a lactam in high-temperature high-pressure water, and the present invention relates to a method for producing a lactam characterized by selectively synthesizing the lactam without bringing about hydrolysis by introducing an oxime into flowing high-temperature high-pressure water, wherein the lactam is continuously synthesized at a high rate from the oxime in water at a high temperature of at least 250° C. and a high pressure of at least 12 MPa.
摘要翻译： 本发明的目的是提供一种在高温高压水中连续生产内酰胺的方法，本发明涉及一种制备内酰胺的方法，其特征在于，通过引入不引起水解而选择性合成内酰胺 将肟流入高温高压水中，其中在至少250℃的高温和至少12MPa的高压下，从肟在水中以高速连续合成内酰胺。
-
公开(公告)号：US06774262B1
公开(公告)日：2004-08-10
申请号：US09659821
申请日：2000-09-11
申请人： Yutaka Ikushima , Osamu Sato , Kiyotaka Hatakeda
发明人： Yutaka Ikushima , Osamu Sato , Kiyotaka Hatakeda
IPC分类号： C07C51235
CPC分类号： C07C29/147 , C07C51/16 , Y02P20/544 , C07C63/06 , C07C29/14 , C07C33/22
摘要： The invention provides a method of increasing the reaction rate of an organic synthesis reaction by utilizing supply of OH− from water in the absence of catalyst without adding a basic catalyst in supercritical water or subcritical water of at least 350 ° C., and a method of generating alcohol and carboxylic acid with high reaction rate by performing a Cannizzaro reaction in the absence of catalyst without adding a basic catalyst in supercritical water, and to a method of synthesis of alcohol and carboxylic acid from an aldehyde in the absence of catalyst without adding a basic catalyst near the critical point (375 to 380 ° C., 22.5 to 25 MPa) of supercritical water.
摘要翻译： 本发明提供了一种通过在不存在催化剂的情况下从水中提供OH而不增加至少350℃的超临界水或亚临界水中的碱性催化剂来提高有机合成反应的反应速率的方法，以及 通过在不存在催化剂的情况下进行坎尼扎罗反应而不在超临界水中添加碱性催化剂的情况下以高反应速度生成醇和羧酸的方法，以及在不存在催化剂的情况下由醛合成醇和羧酸的方法 在临界点附近（375〜380℃，22.5〜25MPa）的超临界水附近不添加碱性催化剂。
-
公开(公告)号：US06300523B1
公开(公告)日：2001-10-09
申请号：US09427761
申请日：1999-10-27
申请人： Yutaka Ikushima , Osamu Sato
发明人： Yutaka Ikushima , Osamu Sato
IPC分类号： C07C4500
CPC分类号： C07C45/52 , B01J3/008 , Y02P20/544 , Y10S210/908
摘要： This invention is intended to provide a method for producing pinacoline by means of pinacol rearrangement in supercritical water, which affords an extremely high reaction rate without the addition of high concentrations of acid, and this invention is directed to a method for increasing the reaction rate during organic synthesis by utilizing the supply of protons from water under noncatalytic conditions in supercritical water, a method of pinacol rearrangement comprising the production of pinacoline by pinacol rearrangement under noncatalytic conditions without the addition of an acid catalyst in supercritical water, and a method of synthesis comprising the production of cyclic compounds from pinacol under noncatalytic conditions without the addition of an acid catalyst around the critical point (375 to 380° C., 22.5 to 25 MPa) in supercritical water.
摘要翻译： 本发明旨在提供一种在超临界水中通过频哪醇重排生产pinacoline的方法，其提供极高的反应速率而不加入高浓度的酸，本发明涉及一种提高反应速率的方法 利用在超临界水中的非催化条件下从水中提供质子的有机合成，包括在非催化条件下在非催化条件下通过频哪醇重排制备频哪醇的方法，而不在超临界水中加入酸催化剂，以及合成方法，包括 在非催化条件下从频哪醇生产环状化合物，而不在超临界水中在临界点（375至380℃，22.5至25MPa）附近加入酸催化剂。
-
公开(公告)号：US09613732B2
公开(公告)日：2017-04-04
申请号：US13500086
申请日：2011-02-10
申请人： Osamu Sato
发明人： Osamu Sato
IPC分类号： H01B13/012 , H01B13/00 , B29C47/08 , B29C47/02 , B29C47/88 , H01B13/24 , B05D7/20 , H01B7/00 , B29C47/00 , B29C47/20 , B29C47/90
CPC分类号： H01B13/0013 , B05D7/20 , B29C47/0016 , B29C47/003 , B29C47/025 , B29C47/0828 , B29C47/20 , B29C47/8805 , B29C47/8815 , B29C47/908 , H01B7/0045 , H01B13/01263 , H01B13/24
摘要： A wire harness manufacturing method prevents inadvertent deformation of thermoplastic material and separation of thermoplastic material. A predetermined part of an electric wire 91 is accommodated in a through hole of a tubular body formed by connection between a first and second nest members (123, 124) of a nozzle (12), by integrally connecting first and second case body members (121, 122) of the nozzle (12), with the predetermined part of the electric wire 91 therebetween. An approximately tubular covering member (92) covering the predetermined part of the electric wire (91) is molded integrally with the thermoplastic material, by discharging thermoplastic material plasticized by a material plasticizing unit (11) from thermoplastic material discharge orifices (1213) and (1223) in the nozzle (12) to the outer periphery of the electric wire (91), while moving the electric wire (91) and the nozzle (12) relatively to each other.
-
公开(公告)号：US09010937B2
公开(公告)日：2015-04-21
申请号：US13904521
申请日：2013-05-29
申请人： Osamu Sato
发明人： Osamu Sato
CPC分类号： F21K9/00 , G03B21/2013 , G03B21/2033 , G03B33/06 , G03B33/12 , H04N5/74 , H04N5/7416 , H04N9/31 , H04N9/3111 , H04N9/3158 , H04N9/3164 , H04N9/3182
摘要： A light source apparatus includes a red light emitting device to emit red light; a green light emitting device to emit green light; a blue light emitting device to emit blue light, each of the red light emitting device, the green light emitting device, and the blue light emitting device disposed separately from any other. Among the red light emitting device, the green light emitting device and the blue light emitting device, at least two light emitting devices each includes a first light source and a second light source, the first light source emitting light having a wavelength of a light of a primary color, and the second light source emitting light having a wavelength deviated from the wavelength of the light of the primary color.
摘要翻译： 光源装置包括发射红光的红色发光装置; 发出绿光的绿色发光装置; 蓝色发光装置发出蓝色光，红色发光装置，绿色发光装置和蓝色发光装置中的每一个分开设置。 在红色发光器件中，绿色发光器件和蓝色发光器件中，至少两个发光器件各自包括第一光源和第二光源，第一光源发射具有波长为 原色，并且第二光源发射具有偏离原色光的波长的波长的光。
-
公开(公告)号：US08933422B2
公开(公告)日：2015-01-13
申请号：US13812842
申请日：2011-06-08
申请人： Ryoichi Ishii , Takashi Doi , Osamu Sato , Yasushi Ebizuka
发明人： Ryoichi Ishii , Takashi Doi , Osamu Sato , Yasushi Ebizuka
CPC分类号： H01J37/18 , H01J37/16 , H01J37/185 , H01J2237/2001 , H01J2237/2802
摘要： The objective of the present invention is to provide a charged particle beam device such that a tip part can be effectually maintained in a clean state, while the frequency of valve body replacements is also reduced. To achieve the objective, a charged particle beam device is offered, comprising: a partition that is positioned between a charged particle source-side vacuum space and a specimen stage-side vacuum space, said partition further comprising an opening for a charged particle beam to pass through; a driver mechanism that moves a shutter member between a first location within the optical axis of the charged particle beam and a second location outside the optical axis of the charged particle beam; and a control device that controls the driver mechanism. The first location is a location wherein the shutter member is distanced from the partition, and the control device carries out a control that opens a valve between the specimen chamber and the exchange chamber when the shutter member is in a state of being located in the first location.
摘要翻译： 本发明的目的是提供一种带电粒子束装置，使得尖端部分可以有效地保持在清洁状态，同时阀体更换的频率也降低。 为了实现该目的，提供一种带电粒子束装置，包括：分隔件，位于带电粒子源侧真空空间和样品台侧真空空间之间，所述隔板还包括用于带电粒子束的开口 通过; 驱动器机构，其将快门部件移动到带电粒子束的光轴内的第一位置与带电粒子束的光轴外的第二位置; 以及控制驱动器机构的控制装置。 第一位置是其中挡板构件与分隔件隔开的位置，并且当挡板构件处于位于第一位置的状态时，控制装置执行在样本室和更换室之间打开阀的控制 位置。
-
-
-
-
-
-
-
-
-
搜索结果
243 条记录 (耗时 0.028 秒)
