DOUBLE-TILT IN-SITU MECHANICAL SAMPLE HOLDER FOR TEM BASED ON PIEZOELECTRIC CERAMIC DRIVE

    公开(公告)号:US20170301511A1

    公开(公告)日:2017-10-19

    申请号:US15387534

    申请日:2016-12-21

    IPC分类号: H01J37/20 H01J37/26

    摘要: A double-tilt in-situ mechanical sample holder for TEM based on piezoelectric ceramic drive belongs to the field of material microstructure-mechanical properties in-situ characterization, and it comprise two parts of sample holder shaft body and piezoelectric ceramic drive system. The sample holder shaft body comprise tilt stage, sample holder, linear stepping motor, drive rod, drive linkage. The piezoelectric ceramic drive system comprise piezoelectric ceramic loading stage, piezoelectric ceramic, connecting base and the sample loading stage realizing stretch or compression function. The double-axis tilt of the samples in X and Y axis directions is realized by the reciprocating motion back and forth of the drive rod driven by the linear stepping motor. The stretch or compression of the samples is realized by applying voltage on the piezoelectric ceramic to generate displacement and push the sample loading stage by the connecting base. The invention coordinating with high resolution TEM realizes the observation of the microstructure in atomic and even sub angstrom scales, and at the same time it ensures the controllable deformation of nanomaterials, further realizes the integrative research on the material microstructure-mechanical properties and reveals the deformation mechanism of the materials.

    Phase plate, method of fabricating same, and electron microscope

    公开(公告)号:US09786467B2

    公开(公告)日:2017-10-10

    申请号:US15067394

    申请日:2016-03-11

    申请人: JEOL Ltd.

    发明人: Hirofumi Iijima

    摘要: A phase plate capable of suppressing electrification and a method of fabricating the plate are provided. The phase plate is for use in an electron microscope and includes a phase control layer provided with a through-hole and at least one conductive layer covering and closing off the through-hole. The conductive layer is formed on at least one of a first surface and a second surface of the phase control layer, the second surface being on the opposite side of the first surface. The phase control layer produces a given phase difference between electron waves transmitted through the phase control layer and electron waves transmitted through the through-hole.