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    PROCESS FOR PRODUCING GLYCIDYL 2-HYDROXYISOBUTYRATE AND COMPOSITION CONTAINING THE PRODUCT
    4.
    发明申请
    PROCESS FOR PRODUCING GLYCIDYL 2-HYDROXYISOBUTYRATE AND COMPOSITION CONTAINING THE PRODUCT 有权
    生产甘油二羟基异丁酸酯的方法和含有产品的组合物

    公开(公告)号：US20090030163A1

    公开(公告)日：2009-01-29

    申请号：US11993999

    申请日：2006-06-30

    申请人： Rieko Nakano ,  Masaki Takemoto ,  Yoshikazu Shima

    发明人： Rieko Nakano ,  Masaki Takemoto ,  Yoshikazu Shima

    IPC分类号： C07D301/12 ,  C08L63/00

    CPC分类号： C07D301/12 ,  C07D303/16

    摘要： An efficient process for producing glycidyl 2-hydroxyisobutyrate useful as a reactive diluent is provided. When glycidyl 2-hydroxyisobutyrate is produced by reacting allyl 2-hydroxyisobutyrate with hydrogen peroxide, a solution in which allyl 2-hydroxyisobutyrate is dissolved in an aliphatic ester as a solvent is reacted with hydrogen peroxide in the presence of a crystalline titanosilicate catalyst. Thus, a production process of glycidyl 2-hydroxyisobutyrate, which is small in degradation of purity and yield due to generation of peroxides or the like, and products thereof are provided.

    摘要翻译： 提供了一种生产用作反应性稀释剂的2-羟基异丁酸缩水甘油酯的有效方法。 当2-羟基异丁酸缩水甘油酯是通过使2-羟基异丁酸烯丙酯与过氧化氢反应来制备的，其中将2-羟基异丁酸烯丙酯溶解在作为溶剂的脂肪族酯中的溶液与过氧化氢在结晶钛硅酸盐催化剂存在下反应。 因此，提供了由于产生过氧化物等而导致的纯度和产率降低小的2-羟基异丁酸缩水甘油酯的制备方法及其产物。

    Process for producing 3-methyltetrahydrofuran
    6.
    发明授权
    Process for producing 3-methyltetrahydrofuran 失效
    3-甲基四氢呋喃的制备方法

    公开(公告)号：US5872266A

    公开(公告)日：1999-02-16

    申请号：US925027

    申请日：1997-09-08

    申请人： Hiroyuki Nitobe ,  Masaki Takemoto ,  Takafumi Abe

    发明人： Hiroyuki Nitobe ,  Masaki Takemoto ,  Takafumi Abe

    IPC分类号： C07D307/06 ,  C07D307/00 ,  C07D307/02

    CPC分类号： C07D307/06

    摘要： There is disclosed a process for producing 3-methyltetrahydrofuran substantially free from any of an alcohol and water which comprises adding an organic solvent capable of forming an azeotropic mixture with an alcohol with an alkyl group having 1 to 3 carbon atoms to a mixed liquid containing 3-methyltetrahydrofuran, the alcohol and/or water as the principal components and, as the case may be, another substance, and distilling the resultant mixture of the mixed liquid and said organic solvent. According to the above process, it is made possible to efficiently separate a mixture of 3-methyltetrahydrofuran and an alcohol and/or water which mixture is difficult to separate with conventional distillation process alone, thereby efficiently producing the objective 3-methyltetrahydrofuran substantially free from any of an alcohol and water.

    摘要翻译： 公开了一种基本上不含任何醇和水的3-甲基四氢呋喃的制备方法，该方法包括将能够与具有1至3个碳原子的烷基的醇形成共沸混合物的有机溶剂加入到含有3 甲基四氢呋喃，醇和/或水作为主要成分，视情况而定，另一种物质，并蒸馏混合液和有机溶剂的混合物。 根据上述方法，可以有效地分离3-甲基四氢呋喃与醇和/或水的混合物，该混合物难以与常规的蒸馏方法分离，从而有效地制备基本上不含任何物质的目标3-甲基四氢呋喃 的酒精和水。