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    MASS SPECTROMETER AND MASS SPECTROMETRY METHOD
    1.
    发明申请
    MASS SPECTROMETER AND MASS SPECTROMETRY METHOD 审中-公开
    质谱仪和质谱方法

    公开(公告)号：US20110248157A1

    公开(公告)日：2011-10-13

    申请号：US13123901

    申请日：2009-10-13

    申请人： Masuyuki Sugiyama ,  Yuichiro Hashimoto ,  Hideki Hasegawa ,  Masuyoshi Yamada ,  Hiroyuki Yasuda ,  Shinji Nagai ,  Shintaro Kubo ,  Takefumi Yokokura

    发明人： Masuyuki Sugiyama ,  Yuichiro Hashimoto ,  Hideki Hasegawa ,  Masuyoshi Yamada ,  Hiroyuki Yasuda ,  Shinji Nagai ,  Shintaro Kubo ,  Takefumi Yokokura

    IPC分类号： H01J49/42

    CPC分类号： H01J49/063 ,  H01J49/4215

    摘要： Objects of the present invention is to provide a quadrupole mass filter that can be fabricated at low cost and has a high transmission efficiency even under a high pressure (0.5 mTorr or more), and to provide a mass spectrometer or mass spectrometry method that reduces crosstalk in a wide mass range. Now, in a mass spectrometer, an ion separating unit is configured to include quadrupole rod electrodes that form a quadrupole radio-frequency electric field, electrodes that form a quadrupole electrostatic field, and a power supply that allows the voltage of the electrodes to form a quadrupole electrostatic field to change. In a collision cell configured to perform collision induced dissociation, harmonic potentials in a plurality of stages are produced to resonance excite ions in the axial direction, so that the ions obtain kinetic energy to move in the direction of the detector. This energy allows a time period to shorten for which ions stay in the collision cell.

    摘要翻译： 本发明的目的是提供一种即使在高压（0.5mTorr以上）下也能低成本制造且具有高透射率的四极质量过滤器，并提供降低串扰的质谱仪或质谱法 在广泛的质量范围。 现在，在质谱仪中，离子分离单元被构造为包括形成四极射频电场的四极杆电极，形成四极静电场的电极和允许电极的电压形成的电源 四极静电场改变。 在被配置为执行碰撞诱导解离的碰撞单元中，产生多个级中的谐波电位以使轴向上的激发离子共振，使得离子获得沿检测器的方向移动的动能。 该能量允许缩短时间段，离子停留在碰撞池中。

    MASS SPECTROMETER AND MASS ANALYZING METHOD
    3.
    发明申请
    MASS SPECTROMETER AND MASS ANALYZING METHOD 有权
    质谱仪和质谱分析方法

    公开(公告)号：US20120326022A1

    公开(公告)日：2012-12-27

    申请号：US13527627

    申请日：2012-06-20

    申请人： Shun KUMANO ,  Masuyuki Sugiyama ,  Yuichiro Hashimoto ,  Hideki Hasegawa ,  Masuyoshi Yamada ,  Hidetoshi Morokuma ,  Shuhei Hashiba

    发明人： Shun KUMANO ,  Masuyuki Sugiyama ,  Yuichiro Hashimoto ,  Hideki Hasegawa ,  Masuyoshi Yamada ,  Hidetoshi Morokuma ,  Shuhei Hashiba

    IPC分类号： H01J49/04

    CPC分类号： H01J49/0409 ,  H01J49/0495

    摘要： A mass spectrometer including a sample attaching member of attaching a sample, an ionizing chamber including an introductory port of the sample attaching member and an ionization source of generating a sample ion, a vacuumed chamber having a mass analyzer of analyzing the sample ion, and an opening/closing mechanism provided between the ionizing chamber and the vacuumed chamber, in which the opening/closing mechanism is controlled from a closed state to an open state after introducing the sample attaching member into the ionizing chamber to thereby enable to perform ionization with inconsiderable fragmentation at a high sensitivity with a high throughput

    摘要翻译： 一种质谱仪，包括附着样品的样品附着构件，包括样品附着构件的入口的电离室和产生样品离子的离子源，具有分析样品离子的质量分析器的真空室，以及 设置在离子化室和真空室之间的开/关机构，其中将样品附着构件引入电离室之后，将开/关机构从关闭状态控制到打开状态，从而能够以不可分割的碎片进行电离 灵敏度高，吞吐量高

    Mass spectrometer and mass analyzing method
    7.
    发明授权
    Mass spectrometer and mass analyzing method 有权
    质谱仪和质量分析方法

    公开(公告)号：US09184037B2

    公开(公告)日：2015-11-10

    申请号：US13527627

    申请日：2012-06-20

    申请人： Shun Kumano ,  Masuyuki Sugiyama ,  Yuichiro Hashimoto ,  Hideki Hasegawa ,  Masuyoshi Yamada ,  Hidetoshi Morokuma ,  Shuhei Hashiba

    发明人： Shun Kumano ,  Masuyuki Sugiyama ,  Yuichiro Hashimoto ,  Hideki Hasegawa ,  Masuyoshi Yamada ,  Hidetoshi Morokuma ,  Shuhei Hashiba

    IPC分类号： H01J49/00 ,  H01J49/04

    CPC分类号： H01J49/0409 ,  H01J49/0495

    摘要： A mass spectrometer including a sample attaching member of attaching a sample, an ionizing chamber including an introductory port of the sample attaching member and an ionization source of generating a sample ion, a vacuumed chamber having a mass analyzer of analyzing the sample ion, and an opening/closing mechanism provided between the ionizing chamber and the vacuumed chamber, in which the opening/closing mechanism is controlled from a closed state to an open state after introducing the sample attaching member into the ionizing chamber to thereby enable to perform ionization with inconsiderable fragmentation at a high sensitivity with a high throughput.

    摘要翻译： 一种质谱仪，包括附着样品的样品附着构件，包括样品附着构件的入口的电离室和产生样品离子的离子源，具有分析样品离子的质量分析器的真空室，以及 设置在离子化室和真空室之间的开/关机构，其中将样品附着构件引入电离室之后，将开/关机构从关闭状态控制到打开状态，从而能够以不可分割的碎片进行电离 灵敏度高，吞吐量高。

    Mass spectrometer
    8.
    发明授权
    Mass spectrometer 有权
    质谱仪

    公开(公告)号：US08866070B2

    公开(公告)日：2014-10-21

    申请号：US13289633

    申请日：2011-11-04

    申请人： Hidetoshi Morokuma ,  Yuichiro Hashimoto ,  Masuyuki Sugiyama ,  Masuyoshi Yamada ,  Hideki Hasegawa

    发明人： Hidetoshi Morokuma ,  Yuichiro Hashimoto ,  Masuyuki Sugiyama ,  Masuyoshi Yamada ,  Hideki Hasegawa

    IPC分类号： H01J49/00 ,  H01J49/24 ,  H01J49/10 ,  H01J49/04

    CPC分类号： H01J49/0013 ,  H01J49/0031 ,  H01J49/0422 ,  H01J49/0495 ,  H01J49/10 ,  H01J49/105 ,  H01J49/24 ,  H01J49/26

    摘要： A mass spectrometer of reduced size and weight is provided which is capable to conduct highly accurate mass spectroscopy. The mass spectrometer includes an ion source adapted to ionize gas flowing in from outside in order to ionize a measurement sample and a mass spectroscopy section for separating the ionized measurement sample. The ion source has its interior reduced in pressure by differential pumping from the mass spectroscopy section and ionizes the gas when the interior pressure rises as it inhales the gas, and the mass spectroscopy section separates the ionized measurement sample when its interior pressure falls after inhale of the gas. The mass spectrometer may further include a restriction device for suppressing a flow rate of the gas the ion source inhales and an open/close device for opening and closing a flow of the gas the ion source inhales.

    摘要翻译： 提供了减小尺寸和重量的质谱仪，其能够进行高精度的质谱。 质谱仪包括离子源，其适于使从外部流入的气体电离，以便电离测量样品和用于分离离子化测量样品的质谱部分。 离子源的内部通过从质谱分析部分的差分泵送而在内部减压，并且当吸入气体时内部压力升高时电离气体，质谱仪分离离子化测量样品，当其内部压力在吸入后 气体。 质谱仪还可以包括用于抑制离子源吸入的气体的流量的限制装置和用于打开和关闭离子源吸入的气体流的打开/关闭装置。

    Mass spectrometer and mass spectrometry method
    9.
    发明授权
    Mass spectrometer and mass spectrometry method 有权
    质谱仪和质谱法

    公开(公告)号：US07800058B2

    公开(公告)日：2010-09-21

    申请号：US11979811

    申请日：2007-11-08

    申请人： Masuyuki Sugiyama ,  Yuichiro Hashimoto ,  Hideki Hasegawa ,  Izumi Waki

    发明人： Masuyuki Sugiyama ,  Yuichiro Hashimoto ,  Hideki Hasegawa ,  Izumi Waki

    IPC分类号： H01J49/00

    CPC分类号： H01J49/4225 ,  H01J49/4215

    摘要： A mass spectrometer that is switchable to operate as a linear trap or as a mass filter, and attaining both high ejection efficiency when operated as a linear trap and high mass resolving power when operated as a mass filter. A mass spectrometer includes an ion source for ionizing a sample, a linear trap quadrupole rod lens supplied with ionized ions, a trap electrode for forming a potential to trap the supplied ions between one end of the quadrupole lens and the other end, a control unit to regulate the trap lens voltage, and a mass analyzer or detector to detect ions ejected from the linear trap, and characterized in switching between an operation where the supplied ions are trapped in a section quadrupole rod lens and ejected by the controller unit regulating the trap electrode voltage; and an operation where ions are selective passed through according to their mass. The ejection efficiency when operated as an ion trap, and the mass resolving power when operated as a quadrupole mass filter are vastly improved compared to conventional methods.

    摘要翻译： 可以切换为线性捕集器或质量过滤器的质谱仪，当作为质量过滤器操作时，作为线性捕集器操作时获得高喷射效率和高质量分辨能力的质谱仪。 质谱仪包括用于电离样品的离子源，提供有离子化离子的线性捕获四极杆透镜，用于形成用于捕获四极透镜的一端与另一端之间的供应离子的电位的捕获电极，控制单元 调节陷波透镜电压，以及质量分析器或检测器，用于检测从线性阱捕获的离子，并且其特征在于，在所提供的离子被捕获在四极杆棒状透镜中并由调节阱的控制器单元喷射的操作之间进行切换 电极电压; 以及根据其质量选择性地通过离子的操作。 当作为离子阱操作时的喷射效率以及当作为四极质量过滤器操作时的质量分辨能力与常规方法相比大大提高。

    Mass spectrometer and mass spectrometry method
    10.
    发明申请
    Mass spectrometer and mass spectrometry method 有权
    质谱仪和质谱法

    公开(公告)号：US20080121795A1

    公开(公告)日：2008-05-29

    申请号：US11979811

    申请日：2007-11-08

    申请人： Masuyuki Sugiyama ,  Yuichiro Hashimoto ,  Hideki Hasegawa ,  Izumi Waki

    发明人： Masuyuki Sugiyama ,  Yuichiro Hashimoto ,  Hideki Hasegawa ,  Izumi Waki

    IPC分类号： H01J49/42

    CPC分类号： H01J49/4225 ,  H01J49/4215

    摘要： A mass spectrometer that is switchable to operate as a linear trap or as a mass filter, and attaining both high ejection efficiency when operated as a linear trap and high mass resolving power when operated as a mass filter. A mass spectrometer includes an ion source for ionizing a sample, a linear trap quadrupole rod lens supplied with ionized ions, a trap electrode for forming a potential to trap the supplied ions between one end of the quadrupole lens and the other end, a control unit to regulate the trap lens voltage, and a mass analyzer or detector to detect ions ejected from the linear trap, and characterized in switching between an operation where the supplied ions are trapped in a section quadrupole rod lens and ejected by the controller unit regulating the trap electrode voltage; and an operation where ions are selective passed through according to their mass. The ejection efficiency when operated as an ion trap, and the mass resolving power when operated as a quadrupole mass filter are vastly improved compared to conventional methods.

    摘要翻译： 可以切换为线性捕集器或质量过滤器的质谱仪，当作为质量过滤器操作时，作为线性捕集器操作时获得高喷射效率和高质量分辨能力的质谱仪。 质谱仪包括用于电离样品的离子源，提供有离子化离子的线性捕获四极杆透镜，用于形成用于捕获四极透镜的一端与另一端之间的供应离子的电位的捕获电极，控制单元 调节陷波透镜电压，以及质量分析器或检测器，用于检测从线性阱捕获的离子，并且其特征在于，在所提供的离子被捕获在四极杆棒状透镜中并由调节阱的控制器单元喷射的操作之间进行切换 电极电压; 以及根据其质量选择性地通过离子的操作。 当作为离子阱操作时的喷射效率以及当作为四极质量过滤器操作时的质量分辨能力与常规方法相比大大提高。