Method for producing fluoride fluorescent material

    公开(公告)号:US11572506B2

    公开(公告)日:2023-02-07

    申请号:US16719051

    申请日:2019-12-18

    Inventor: Tomokazu Yoshida

    Abstract: A method for producing a fluoride fluorescent material comprises: preparing fluoride particles having a composition containing at least one element or ion A selected from the group consisting of alkaline metal elements and NH4+, at least one element M selected from the group consisting of Group-4 elements and Group-14 elements, Mn4+, and F, in which a molar ratio of A in 1 mol of the composition is 2, a total molar ratio of M and Mn4+ is 1, a molar ratio of Mn4+ is in a range of more than 0 and less than 0.2, and a molar ratio of F is 6; subjecting the fluoride particles to a first heat treatment at a temperature of 500° C. or more in an inert gas atmosphere; washing the first heat-treated fluoride particles with a washing liquid; and bringing the washed fluoride particles into contact with a fluorine-containing substance and subjecting the resulting fluoride particles to a second heat treatment at a temperature of 400° C. or more.

    Method for producing fluoride fluorescent material

    公开(公告)号:US10214688B2

    公开(公告)日:2019-02-26

    申请号:US15375619

    申请日:2016-12-12

    Abstract: The present invention provides a method for producing a fluoride fluorescent material comprising a chemical composition represented by the following formula (I): K2[M1−aMn4+aF6]  (I) wherein M is at least one element selected from the group consisting of elements belonging to Groups 4 and 14 of the Periodic Table, and a is a value that satisfies the relationship: 0

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