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公开(公告)号:US20240199438A1
公开(公告)日:2024-06-20
申请号:US18504209
申请日:2023-11-08
Inventor: TAKESHI KOIWASAKI , TAKESHI UEDA , HISAO NAGAI , TAKAFUMI OKUMA
IPC: C01G3/02 , B01J21/06 , B01J23/72 , B01J35/39 , B01J37/34 , C01G23/047 , C09D133/06 , C08K3/22
CPC classification number: C01G3/02 , B01J21/063 , B01J23/72 , B01J35/39 , B01J37/34 , C01G23/047 , C09D133/06 , C01P2004/62 , C01P2004/64 , C08K2003/2241 , C08K2003/2248
Abstract: A composite microparticle manufacturing method includes: a step of preparing a first selective element-containing raw material and a second selective element-containing raw material, the first selective element-containing raw material containing one or more first selective elements selected from a copper element, a molybdenum element, and a silver element, the second selective element-containing raw material containing one or more second selective elements selected from titanium, germanium, silicon, tin, aluminum, zinc, zirconium, hafnium, iron, yttrium, niobium, tantalum, calcium, magnesium, indium, tungsten, molybdenum, and nickel; and a composite microparticle generation step of introducing both of the prepared raw materials into thermal plasma, evaporating the raw materials, and cooling the evaporated raw materials to generate composite microparticles including base particles and first selective element-containing microparticles being present on surfaces of the base particles, the base particles having an average particle diameter of from 10 nm to 300 nm inclusive.
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公开(公告)号:US20180290208A1
公开(公告)日:2018-10-11
申请号:US15915017
申请日:2018-03-07
Inventor: HISAO NAGAI , TAKESHI KOIWASAKI , MASAAKI TANABE , TAKAFUMI OKUMA
IPC: B22F1/00 , B22F9/14 , H01J37/32 , H05H1/42 , C04B35/628
CPC classification number: B22F1/0018 , B01J2219/0809 , B01J2219/0841 , B01J2219/0898 , B22F9/14 , B22F2201/20 , B22F2202/13 , B22F2999/00 , C04B35/62834 , H01J37/32055 , H05H1/42 , H05H1/48 , H05H2245/124
Abstract: A production apparatus for fine particles includes a vacuum chamber, a material supply device, a plurality of electrodes arranged and a collection device connecting to the other end of the vacuum chamber and collecting fine particles, which generates plasma and produces fine particles from the material particles, in which a first electrode arrangement region on the material supply port's side and a second electrode arrangement region apart from the first electrode arrangement region to the collection device's side which respectively cross a direction in which the material flows between the vicinity of the material supply port and the collection device are provided in the intermediate part of the vacuum chamber, and both the first electrode arrangement region and the second electrode arrangement region are provided with a plurality of electrodes respectively to form the electrodes in multi-stages.
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公开(公告)号:US20220200044A1
公开(公告)日:2022-06-23
申请号:US17522964
申请日:2021-11-10
Inventor: SHUZO TSUCHIDA , AKIHIRO HORIKAWA , TAKESHI KOIWASAKI
IPC: H01M10/0562 , H01M10/0585
Abstract: All-solid-state battery 100 has a structure in which positive electrode current collector 6, positive electrode layer 20 containing positive electrode active material 3 and solid electrolyte 1, solid electrolyte layer 10 containing solid electrolyte 2, negative electrode layer 30 containing negative electrode active material 4 and solid electrolyte 5, and negative electrode current collector 7 are stacked in this order. Solid electrolyte 2 contains first material 21 and second material 22 having an ionic conductivity lower than an ionic conductivity of first material 21. First material 21 includes first particles 40, and at least a part of a surface of first particles 40 is covered with second material 22.
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公开(公告)号:US20170136546A1
公开(公告)日:2017-05-18
申请号:US15251840
申请日:2016-08-30
Inventor: HISAO NAGAI , TAKESHI KOIWASAKI , DAISUKE SUETSUGU , TAKAFUMI OKUMA
IPC: B22F9/16 , C01B33/18 , B01J19/08 , C01B31/36 , C01F7/02 , C01B33/021 , C01B21/068
CPC classification number: B22F9/16 , B01J19/088 , B01J2219/0875 , B01J2219/0898 , B22F9/14 , B22F2201/013 , B22F2201/11 , B22F2201/20 , B22F2301/10 , B22F2301/15 , B22F2301/255 , B22F2304/05 , B22F2998/10 , B22F2999/00 , C01B21/068 , C01B32/956 , C01B33/021 , C01B33/181 , C01F7/02 , B22F3/003 , B22F2202/13
Abstract: To provide an apparatus and a method of producing fine particles capable of increasing evaporation efficiency of a material, increasing the production of fine particles and reducing costs by heating the inputted material by a gas heated by thermal plasma. A fine particle production apparatus includes a vacuum chamber, a material feeding device connected to the vacuum chamber and feeding material particles from a material feeding port into the vacuum chamber, electrodes arranged in the vacuum chamber for generating plasma and a collection device connected to the vacuum chamber and collecting fine particles, which produces the fine particles from the material by generating electric discharge inside the vacuum chamber, in which the collection device and the material feeding device are connected by piping, and a material heating and circulation device which heats the material by heat of a gas inside the chamber heated by the plasma through the piping is provided.
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公开(公告)号:US20230331573A1
公开(公告)日:2023-10-19
申请号:US18337804
申请日:2023-06-20
Inventor: HISAO NAGAI , HIROKI MARUYAMA , TAKESHI KOIWASAKI , TAKAFUMI OKUMA
CPC classification number: C01F11/04 , C08K7/18 , C01P2004/51 , C01P2004/64 , C01P2004/62 , C01P2006/12 , C08K2201/005 , C08K2201/006
Abstract: A method for producing a fine-particle powder containing calcium oxide or calcium hydroxide includes: preparing a pulverized powder of shells or eggshells; introducing the pulverized powder of shells or eggshells into a controlled atmosphere, vaporizing the pulverized powder under thermal plasma and then solidifying the pulverized powder in a gas phase to produce fine particles containing calcium oxide or calcium hydroxide; and collecting a powder of the fine particles containing calcium oxide or calcium hydroxide produced with the thermal plasma.
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公开(公告)号:US20250059059A1
公开(公告)日:2025-02-20
申请号:US18937721
申请日:2024-11-05
Inventor: TAKESHI KOIWASAKI , HISAO NAGAI , HIROKI MARUYAMA
IPC: C01G23/047 , C08K3/22
Abstract: A method of manufacturing a composite particle includes: a step of preparing a first raw material including an element selected from any of copper, molybdenum, and silver, and a second raw material including one or more types of elements selected from aluminum, titanium, zirconium, hafnium, iron, yttrium, niobium, tantalum, silicon, calcium, magnesium, tungsten, indium, tin, germanium, nickel, zinc, and molybdenum; and a thermal plasma evaporation and cooling step of introducing the prepared first and second raw materials into thermal plasma to evaporate the first raw materials, and cooling the evaporated first raw materials to generate a composite particle. The composite particle includes the second raw material, and a fine particle carried on a surface of the second raw material and generated from the first raw material having an average particle size of 0.5 nm or more and 300 nm or less.
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公开(公告)号:US20190247822A1
公开(公告)日:2019-08-15
申请号:US16255135
申请日:2019-01-23
Inventor: HISAO NAGAI , TAKESHI KOIWASAKI , TAKAFUMI OKUMA
CPC classification number: B01J19/088 , B01J2219/0809 , B01J2219/0879 , B01J2219/0898 , B22F1/0018 , B22F1/0048 , B22F9/14 , B22F2202/13 , B22F2304/05
Abstract: A fine particle producing apparatus includes a reaction chamber extending vertically from the lower side to the upper side; a material supply device which is connected to a central part on one end side of the vertically lower side inside the reaction chamber and supplies a material particle into the reaction chamber of a vertically upper side from a material supply port; a first electrode arrangement region which protrudes in an inward radial direction to be disposed on an inner peripheral wall in the reaction chamber which is vertically above the material supply device, and includes a plurality of lower electrodes to which AC power is applied; a second electrode arrangement region which protrudes in an inward radial direction to be disposed on an inner peripheral wall in the reaction chamber which is vertically above the first electrode arrangement region, and includes a plurality of upper electrodes to which AC power is applied; a collector which is connected to the other end side in the reaction chamber of the vertically upper side so as to collect fine particles; a power source which is capable of changing a frequency of AC power applied to at least one of the lower electrode included in the first electrode arrangement region and the upper electrode included in the second electrode arrangement region; and a controller which sets the frequency of AC power applied to the lower electrode as a frequency equal to or higher than a frequency of AC power applied to the upper electrode, in which a fine particle is generated from the material particle by generating arc discharge by the lower electrode and the upper electrode, and generating plasma in the reaction chamber.
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公开(公告)号:US20180304374A1
公开(公告)日:2018-10-25
申请号:US15922838
申请日:2018-03-15
Inventor: MASAAKI TANABE , HISAO NAGAI , TAKESHI KOIWASAKI , TAKAFUMI OKUMA
IPC: B22F9/14 , C01B32/956 , C01B33/021 , B22F9/16 , B22F1/00 , B01J19/08
CPC classification number: B22F9/14 , B01J19/088 , B01J2219/0875 , B01J2219/0894 , B22F1/0018 , B22F9/16 , B22F2201/013 , B22F2201/11 , B22F2201/20 , B22F2202/13 , B22F2301/10 , B22F2301/15 , B22F2301/255 , B22F2304/05 , B22F2998/10 , B22F2999/00 , C01B32/956 , C01B33/021 , C01P2004/64
Abstract: A production apparatus and method for fine particles are capable of increasing a production amount and producing fine particles at low cost by efficiently inputting a large amount of material to plasma. The production apparatus includes a material supply device, which includes a plurality of material supply ports that supply a material gas containing material particles and are arranged below a plurality of electrodes in a vertical direction inside a vacuum chamber. The material supply device further includes a first gas supply port that supplies a first shield gas arranged in an inner periphery of the plural material supply ports and plural second gas supply ports that supply a second shield gas arranged in an outer periphery of the plural material supply ports.
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