公开(公告)号：US20180315584A1

公开(公告)日：2018-11-01

申请号：US15771462

申请日：2016-10-25

申请人： COMMISSARIAT A L'ENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES

发明人： Marc DELAUNAY ,  Anne GHIS

IPC分类号： H01J37/32 ,  H01J37/34 ,  C23C14/06 ,  C23C14/35

CPC分类号： H05H1/46 ,  C23C14/0605 ,  C23C14/357 ,  H01J37/32192 ,  H01J37/32229 ,  H01J37/32651 ,  H01J37/3266 ,  H01J37/32678 ,  H05H2001/4622 ,  H05H2245/124

摘要： A device for producing an amorphous carbon layer by electron cyclotron resonance plasma, the device including a plasma chamber; a gas supply; a magnetic mirror; a waveguide extending along a reference axis; a system for injecting microwave power; a magnetic field generator for generating a magnetic field in the plasma chamber, the magnetic field generator being configured to create a beam of magnetic field lines along which plasma is diffused; a target made from carbon; a substrate holder, wherein the target is arranged at a distance from the reference axis of between Rtarget/2 and Rtarget, and wherein the device further includes a screen arranged between the waveguide and the substrate holder.

公开(公告)号：US07485348B2

公开(公告)日：2009-02-03

申请号：US10984079

申请日：2004-11-09

申请人： Yoshikazu Kondo

发明人： Yoshikazu Kondo

IPC分类号： H05H1/24

CPC分类号： H05H1/48 ,  B82Y10/00 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/158 ,  C01B32/162 ,  C01B2202/02 ,  D01F9/12 ,  H01J2201/30469 ,  H05H2240/10 ,  H05H2245/124

摘要： A method for forming nanostructured carbons comprising the steps of: generating a plasma by supplying at least a discharge gas between opposing electrodes and applying a high-frequency voltage between the electrodes under an approximately atmospheric pressure; existing a material gas for forming the nanostructured carbons with the plasma to generate an activated material gas; and exposing a substrate to the activated material gas.

摘要翻译： 一种形成纳米结构碳的方法，包括以下步骤：通过在相对电极之间至少提供放电气体并在大气压下在电极之间施加高频电压来产生等离子体; 存在用于与等离子体形成纳米结构碳的材料气体以产生活化材料气体; 以及将基底暴露于活化材料气体。

公开(公告)号：US20180051382A1

公开(公告)日：2018-02-22

申请号：US15537279

申请日：2015-12-15

申请人： UNIVERSITÉ LAVAL

发明人： Marc-André FORTIN ,  Mathieu BOUCHARD ,  Christian SARRA-BOURNET ,  Stéphane TURGEON

IPC分类号： C25C7/06 ,  B22F1/00 ,  B22F9/16 ,  C25C1/20 ,  C25C5/02 ,  C25C7/02 ,  H05H1/24

CPC分类号： C25C7/06 ,  B22F1/0014 ,  B22F1/0018 ,  B22F9/12 ,  B22F9/16 ,  B22F2301/255 ,  B22F2999/00 ,  C25C1/20 ,  C25C5/02 ,  C25C7/00 ,  C25C7/02 ,  H05H1/00 ,  H05H1/2406 ,  H05H2001/2412 ,  H05H2242/10 ,  H05H2245/124 ,  B22F9/24 ,  B22F2202/13 ,  B22F2201/013 ,  B22F2201/02 ,  B22F2201/03 ,  B22F2201/04 ,  B22F2201/05 ,  B22F2201/10 ,  B22F2201/50

摘要： A dielectric barrier discharge (DBD) plasma apparatus for synthesizing metal particles is provided. The DBD plasma apparatus includes an electrolyte vessel for receiving an electrolyte solution comprising metal ions; an electrode spaced-apart from the electrolyte vessel; a dielectric barrier interposed between the electrolyte vessel and the electrode such that, when the electrolyte solution is present in the electrolyte vessel, the dielectric barrier and an upper surface of the electrolyte solution are spaced-apart from each other and define a discharge area therebetween; and gas inlet and outlet ports in fluid communication with the discharge area such that supplying gas in the discharge area while applying an electrical potential difference between the electrode and the electrolyte solution cause a plasma to be produced onto the electrolyte solution, the plasma interacting with the metal ions and synthesizing metal particles. A method for synthesizing metal particles using a DBD plasma apparatus is also provided.

公开(公告)号：US20040262145A1

公开(公告)日：2004-12-30

申请号：US10479230

申请日：2003-12-01

发明人： Georgy Andreevich Duzhev ,  Igor Vladimirovich Basargin ,  Boris Mikhailovich Filippov ,  Nikolay Igorevich Alekseev ,  Dmitry Vladimirovich Afanasiev ,  Aleksandr Alekseevich Bognadov

IPC分类号： H05F003/00 ,  C01B031/00 ,  B01J019/08

CPC分类号： B82Y30/00 ,  B01J19/088 ,  B01J2219/0809 ,  B01J2219/0822 ,  B01J2219/083 ,  B01J2219/0839 ,  B01J2219/0847 ,  B01J2219/0869 ,  B01J2219/0871 ,  B01J2219/0894 ,  B82Y40/00 ,  C01B32/15 ,  C01B32/152 ,  H05H1/48 ,  H05H2245/124

摘要： The inventive method for producing fullerene-containing carbon and the device for carrying out said method relate to the chemical industry and are used for producing fullerenes. Said method for producing fullerene-containing carbon consists in vaporising graphite in an electric arc between coaxial graphite electrodes. The graphite electrode is continuously moved inside the electric arc zone through the glow discharge zone. The products formed inside the electric arc are removed therefrom with the aid of an annular inert gas flow which is directed along the axes of the electrodes through an area arranged at a defined distance from a discharge axis. The inventive device for producing fullerene-containing carbon comprises a plasma reactor provided with a system for circulating inert gas and a system for recuperating fullerene carbon. Said reactor is provided with a chamber for degassing the graphite electrode which is continuously moved by the glow discharge towards the arc. The system for circulating inert gas is provided with an annular slot nozzle coaxially arranged in relation to the moving graphite electrode.

公开(公告)号：US06827823B2

公开(公告)日：2004-12-07

申请号：US10094622

申请日：2002-03-12

申请人： Hirofumi Takikawa ,  Yoshihiko Hibi ,  Shigeo Itoh

发明人： Hirofumi Takikawa ,  Yoshihiko Hibi ,  Shigeo Itoh

IPC分类号： B01J1908

CPC分类号： B82Y30/00 ,  B01J19/088 ,  B01J2219/082 ,  B01J2219/0839 ,  B01J2219/0869 ,  B01J2219/0875 ,  B01J2219/0879 ,  B01J2219/0892 ,  B01J2219/0894 ,  B82Y10/00 ,  B82Y40/00 ,  C01B32/152 ,  C01B32/162 ,  C01B2202/02 ,  H01J37/32055 ,  H01J2201/30469 ,  H01J2209/022 ,  H05H1/48 ,  H05H2001/483 ,  H05H2245/124 ,  Y10S977/844 ,  Y10T428/30

摘要： Described herein is a method of preparing nano-carbon; a method of preparing an electron emitting source by supporting the soot; and an apparatus for preparing the same. A torch electrode 10 of an arc torch 1 as a first electrode is placed opposite to a material to be arced 2 using graphite as a second electrode. A voltage is applied between the torch electrode 10 and an edge portion of the material to be arced 2 to generate are discharge, to evaporate the edge portion of the material to be arced 2 exposed to the arc discharge, to generate soot. The soot thus generated is deposited on the surface of a substrate opposite to an arc discharge-generating area through a mask having a patterned opening.

摘要翻译： 本文描述了制备纳米碳的方法; 一种通过支持烟灰来制备电子发射源的方法; 及其制备装置。 作为第一电极的电弧焊炬1的焊炬电极10与使用石墨作为第二电极的待弧焊材料2相对放置。 在焊炬电极10和待弧形材料2的边缘部分之间施加电压以产生放电，以使待暴露于电弧放电的待蚀刻材料的边缘部分蒸发，以产生烟灰。 这样生成的烟炱通过具有图案化开口的掩模沉积在与电弧放电产生区域相对的基板的表面上。

公开(公告)号：US09630162B1

公开(公告)日：2017-04-25

申请号：US13439592

申请日：2012-04-04

申请人： Mahendra Kumar Sunkara ,  Jeong H. Kim ,  Vivekanand Kumar

发明人： Mahendra Kumar Sunkara ,  Jeong H. Kim ,  Vivekanand Kumar

IPC分类号： B01J12/02 ,  C01F7/42 ,  C01G19/02 ,  C01G25/02 ,  C01G9/03

CPC分类号： B01J12/02 ,  B82Y30/00 ,  C01B13/14 ,  C01B13/32 ,  C01F7/424 ,  C01G1/02 ,  C01G9/00 ,  C01G9/03 ,  C01G19/02 ,  C01G23/047 ,  C01G23/07 ,  C01G25/02 ,  C01P2002/82 ,  C01P2004/03 ,  C01P2004/16 ,  C01P2004/17 ,  C01P2004/64 ,  H01J37/32192 ,  H01J37/3244 ,  H01J37/32449 ,  H01J37/32834 ,  H05H1/46 ,  H05H2001/4622 ,  H05H2245/124

摘要： A reactor and method for production of nanostructures, including metal oxide nanowires or nanoparticles, are provided. The reactor includes a regulated metal powder delivery system in communication with a dielectric tube; a plasma-forming gas inlet, whereby a plasma-forming gas is delivered substantially longitudinally into the dielectric tube; a sheath gas inlet, whereby a sheath gas is delivered into the dielectric tube; and a microwave energy generator coupled to the dielectric tube, whereby microwave energy is delivered into a plasma-forming gas. The method for producing nanostructures includes providing a reactor to form nanostructures and collecting the formed nanostructures, optionally from a filter located downstream of the dielectric tube.

公开(公告)号：US07153398B2

公开(公告)日：2006-12-26

申请号：US10479230

申请日：2002-03-05

申请人： Georgy Andreevich Duzhev ,  Igor Vladimirovich Basargin ,  Boris Mikhailovich Filippov ,  Nikolay Igorevich Alekseev ,  Dmitry Vladimirovich Afanasiev ,  Aleksandr Alekseevich Bogdanov

发明人： Georgy Andreevich Duzhev ,  Igor Vladimirovich Basargin ,  Boris Mikhailovich Filippov ,  Nikolay Igorevich Alekseev ,  Dmitry Vladimirovich Afanasiev ,  Aleksandr Alekseevich Bogdanov

IPC分类号： C01B31/00 ,  B23K15/00 ,  B23K9/02 ,  B01J19/08

CPC分类号： B82Y30/00 ,  B01J19/088 ,  B01J2219/0809 ,  B01J2219/0822 ,  B01J2219/083 ,  B01J2219/0839 ,  B01J2219/0847 ,  B01J2219/0869 ,  B01J2219/0871 ,  B01J2219/0894 ,  B82Y40/00 ,  C01B32/15 ,  C01B32/152 ,  H05H1/48 ,  H05H2245/124

摘要： The inventive method for producing fullerene-containing carbon and the device for carrying out said method relate to the chemical industry and are used for producing fullerenes. Said method for producing fullerene-containing carbon consists in vaporising graphite in an electric arc between coaxial graphite electrodes. The graphite electrode is continuously moved inside the electric arc zone through the glow discharge zone. The products formed inside the electric arc are removed therefrom with the aid of an annular inert gas flow which is directed along the axes of the electrodes through an area arranged at a defined distance from a discharge axis. The inventive device for producing fullerene-containing carbon comprises a plasma reactor provided with a system for circulating inert gas and a system for recuperating fullerene carbon. Said reactor is provided with a chamber for degassing the graphite electrode which is continuously moved by the glow discharge towards the arc. The system for circulating inert gas is provided with an annular slot nozzle coaxially arranged in relation to the moving graphite electrode.

摘要翻译： 本发明的含有富勒烯的碳的制造方法以及用于实施所述方法的装置涉及化学工业，并且用于制造富勒烯。 所述含有富勒烯的碳的制造方法包括在同轴石墨电极之间的电弧中汽化石墨。 石墨电极通过辉光放电区在电弧区内连续移动。 形成在电弧内部的产品借助于沿着电极的轴线穿过布置在与放电轴线限定距离的区域的环形惰性气体流动而被除去。 本发明的含有富勒烯的碳的装置包括具有用于循环惰性气体的系统的等离子体反应器和用于使富勒烯碳还原的系统。 所述反应器设置有用于使通过辉光放电持续移动的石墨电极脱气的腔室。 用于循环惰性气体的系统设置有相对于移动的石墨电极同轴地布置的环形狭槽喷嘴。

公开(公告)号：US20060083856A1

公开(公告)日：2006-04-20

申请号：US11296448

申请日：2005-12-08

申请人： Junri Ishikura ,  Makoto Kameyama ,  Yasuyuki Saito

发明人： Junri Ishikura ,  Makoto Kameyama ,  Yasuyuki Saito

IPC分类号： C23C14/00 ,  C23C16/00

CPC分类号： C23C14/228 ,  C23C14/325 ,  H05H1/48 ,  H05H2001/483 ,  H05H2245/124

摘要： A particle film deposition apparatus and method are provided, with which ultra fine particles are generated by arc heating. The generated ultra fine particles can be efficiently sucked up into a transfer tube regardless of an arc voltage, and the resulting film can be stable in shape. An evaporation material 8 to be evaporated by arc heating and to generate ultra fine particles is connected to an electrode. As other electrodes, a plurality of rods 17 each having a discharge section at the tip thereof are provided. These rods 17 are so arranged as to be directed in each different direction with respect to the evaporation material 8.

公开(公告)号：US06465052B1

公开(公告)日：2002-10-15

申请号：US09996325

申请日：2001-11-30

申请人： L. W. Wu

发明人： L. W. Wu

IPC分类号： H05H132

CPC分类号： H05H1/44 ,  H05H2245/123 ,  H05H2245/124

摘要： A method for producing a nano-porous coating onto a substrate, including the steps of: (a) operating a twin-wire arc nozzle to heat and at least partially vaporize two wires of a metal for providing a stream of nanometer-sized vapor clusters of the metal into a chamber in which the substrate is disposed; (b) injecting a stream of reactive gas into the chamber to impinge upon the stream of metal vapor clusters and exothermically react therewith to produce substantially nanometer-sized metal compound or ceramic clusters; (c) operating heat treatment devices to heat treat the metal compound or ceramic clusters so that a non-zero proportion of the clusters is in a solid state when impinging upon the substrate; and (d) directing the metal compound or ceramic clusters to impinge and deposit onto the substrate for forming the nano-porous coating.

摘要翻译： 一种用于在基材上制备纳米多孔涂层的方法，包括以下步骤：（a）操作双线弧形喷嘴以加热和至少部分蒸发金属的两条线，以提供纳米级蒸汽团簇流 的金属进入其中设置基板的室中; （b）将反应性气体流注入室中以冲击金属蒸气簇并与其放热反应以产生基本上纳米级的金属化合物或陶瓷簇; （c）操作热处理装置以热处理金属化合物或陶瓷簇，使得非零比例的簇在撞击基板时处于固态; 和（d）引导金属化合物或陶瓷簇撞击并沉积到基底上以形成纳米多孔涂层。

公开(公告)号：US20180050120A1

公开(公告)日：2018-02-22

申请号：US15611098

申请日：2017-06-01

申请人： Plasmology4, Inc.

发明人： Emilia M. Kulaga

IPC分类号： A61L2/00 ,  A01N59/16 ,  A01N59/20 ,  A61K41/00 ,  A61K33/24 ,  A61K33/38 ,  A61K33/34 ,  A61N1/44

CPC分类号： A61L2/0011 ,  A01N59/16 ,  A01N59/20 ,  A61K33/00 ,  A61K33/24 ,  A61K33/242 ,  A61K33/243 ,  A61K33/34 ,  A61K33/38 ,  A61K41/00 ,  A61K41/0052 ,  A61L2/0082 ,  A61L2/14 ,  A61L2/18 ,  A61N1/44 ,  B22F1/0044 ,  B22F9/14 ,  B22F2202/13 ,  H01J37/00 ,  H05H1/00 ,  H05H1/46 ,  H05H2001/4682 ,  H05H2001/469 ,  H05H2240/20 ,  H05H2245/124 ,  A61K2300/00

摘要： A method of forming metal nanoparticles includes applying a substance to an area of interest, applying cold plasma to the area of interest, and synthesizing nanoparticles from the substance using the cold plasma in the area of interest, wherein the substance is a solution that contains metal ions, and the nanoparticles synthesized are metallic in nature.