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    Off-site treatment for hydrogenation catalysts
    1.
    发明授权
    Off-site treatment for hydrogenation catalysts 有权
    氢化催化剂的现场处理

    公开(公告)号：US07713905B2

    公开(公告)日：2010-05-11

    申请号：US10554873

    申请日：2004-04-28

    申请人： Pierre Dufresne ,  Franck Labruyere ,  François Locatelli

    发明人： Pierre Dufresne ,  Franck Labruyere ,  François Locatelli

    IPC分类号： B01J27/02 ,  B01J27/043 ,  B01J27/045

    CPC分类号： C10G49/02 ,  B01J37/14 ,  B01J37/20 ,  C10G49/04 ,  C10G2300/705

    摘要： The present invention concerns a process for “ex situ” treatment of a hydrogenation catalyst containing nickel prior to use, consisting of carrying out three steps, namely bringing the catalyst into contact with at least one sulphur-containing compound or agent (the step termed selectivation), treating said catalyst with hydrogen at a temperature of more than 250° C. (the step termed reduction) and passivation of said catalyst.

    摘要翻译： 本发明涉及一种在使用前对含镍的氢化催化剂进行“非原位”处理的方法，包括进行三个步骤，即使催化剂与至少一种含硫化合物或试剂接触（称为选择性的步骤 ），在大于250℃的温度（所述还原步骤）和所述催化剂的钝化下用氢气处理所述催化剂。

    Process for sulfiding an additive-containing catalyst
    6.
    发明授权
    Process for sulfiding an additive-containing catalyst 有权
    用于硫化含添加剂的催化剂的方法

    公开(公告)号：US06753291B2

    公开(公告)日：2004-06-22

    申请号：US09829638

    申请日：2001-04-10

    申请人： Sonja Eijsbouts ,  Frans Lodewijk Plantenga ,  Pierre Dufresne ,  Franck Labruyere ,  Leendert Arie Gerritsen

    发明人： Sonja Eijsbouts ,  Frans Lodewijk Plantenga ,  Pierre Dufresne ,  Franck Labruyere ,  Leendert Arie Gerritsen

    IPC分类号： B01J2702

    CPC分类号： B01J31/0254 ,  B01J23/85 ,  B01J27/188 ,  B01J31/0202 ,  B01J31/0205 ,  B01J31/0218 ,  B01J31/0237 ,  B01J37/20 ,  C10G45/08 ,  C10G2300/705

    摘要： The present invention pertains to a process for sulfiding a catalyst composition comprising at least one hydrogenation metal component of Group VI and/or Group VIII of the Periodic Table, and an organic additive wherein the catalyst composition is first contacted with an organic liquid, followed by the catalyst being contacted with hydrogen and a sulfur-containing compound in the gaseous phase, wherein less than about 40%, preferably less than about 35%, more preferably less than about 25%, most preferably less than about 15%, of the sulfur present in the sulfided catalyst is added with the organic liquid. The process of the present invention makes it possible to use additive-containing catalysts without loss of activity in units which cannot effect gas phase start-up or are required to carry out a pressure test. The organic liquid may be a hydrocarbon with a boiling range of about 150-500° C., preferably gasoline, white spirit, diesel, gas oil, mineral lube oil, or white oil. The step of contacting the catalyst with hydrogen and a sulfur-containing compound may take place in one step at a temperature of about 150-450° C. It may also take place in two steps, with the first step being performed at a temperature which is lower than that of the second step, with the first step being carried out at a temperature of about 100-250° C. and the second step at a temperature of about 150-450° C.

    摘要翻译： 本发明涉及一种硫化催化剂组合物的方法，该催化剂组合物包含至少一种元素周期表第VI族和/或第Ⅷ族氢化金属组分和一种有机添加剂，其中催化剂组合物首先与有机液体接触， 催化剂在气相中与氢气和含硫化合物接触，其中少于约40％，优选小于约35％，更优选小于约25％，最优选小于约15％的硫 存在于硫化催化剂中的有机液体中加入。 本发明的方法使得可以在不能实现气相启动或需要进行压力试验的单位中使用不含活性的添加剂的催化剂。 有机液体可以是沸点为约150-500℃的烃，优选汽油，白酒，柴油，瓦斯油，矿物润滑油或白油。 使催化剂与氢气和含硫化合物接触的步骤可以在约150-450℃的温度下在一个步骤中进行。它也可以在两个步骤中进行，第一步是在 低于第二步骤，第一步骤在约100-250℃的温度下进行，第二步在约150-450℃的温度下进行。

    Oxidizing heat treatment passivation of sulphide hydrotreatment catalyst
    8.
    发明授权
    Oxidizing heat treatment passivation of sulphide hydrotreatment catalyst 有权
    硫化氢加氢处理催化剂的氧化热处理钝化

    公开(公告)号：US07501376B2

    公开(公告)日：2009-03-10

    申请号：US10529378

    申请日：2003-09-25

    申请人： Pierre Dufresne ,  Franck Labruyere

    发明人： Pierre Dufresne ,  Franck Labruyere

    IPC分类号： B01J27/02 ,  B01J27/047 ,  B01J27/051 ,  B01J27/049 ,  B01J27/043 ,  B01J27/045

    CPC分类号： B01J37/20 ,  B01J23/882 ,  B01J33/00 ,  B01J37/14 ,  C10G49/02 ,  C10G2300/705

    摘要： This invention relates to a process of ex-situ oxidizing passivation of catalysts for hydroconversion of hydrocarbons and especially of hydrotreating, in their sulfide state, process in which the sulfurized catalyst is brought into contact with an oxidizing gas flow that can be dry or wet, during heat treatment at more than 50° C. This invention, for passivation of sulfide phases, can be equally well implemented for a process that takes place in a fixed bed or a fluidized bed, for example a moving bed.

    摘要翻译： 本发明涉及一种用于烃的加氢转化的催化剂的非原位氧化钝化方法，特别是在其硫化物状态下加氢处理，其中使硫化催化剂与可干燥或潮湿的氧化气流接触的方法， 在超过50℃的热处理期间。本发明用于钝化硫化物相，对于在固定床或流化床（例如移动床）中发生的方法同样可以很好地实施。