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    Co-crystallizable diacetylenic monomer compositions, crystal phases and mixtures, and related methods
    1.
    发明授权
    Co-crystallizable diacetylenic monomer compositions, crystal phases and mixtures, and related methods 有权
    可共结构的二炔单体组合物，结晶相和混合物及相关方法

    公开(公告)号：US08354486B2

    公开(公告)日：2013-01-15

    申请号：US12730835

    申请日：2010-03-24

    申请人： Elizabeth Castillo Martinez ,  Ray H. Baughman ,  Lee J. Hall ,  Mikhail Kozlov ,  Dawn E. Smith ,  Thaddeus Prusik ,  Carl M. Lentz

    发明人： Elizabeth Castillo Martinez ,  Ray H. Baughman ,  Lee J. Hall ,  Mikhail Kozlov ,  Dawn E. Smith ,  Thaddeus Prusik ,  Carl M. Lentz

    IPC分类号： C08F238/00 ,  G01D21/00 ,  C07C275/20 ,  C08F2/36

    CPC分类号： C07C275/20 ,  C08F238/02 ,  G01N31/229

    摘要： Solid polymerizable diacetylenic monomer compositions, including compositions co-crystallized from a diversity of solvent systems under diverse cooling conditions, can exhibit diffraction patterns associated with the color development reactivities of the compositions. High reactivity compositions are disclosed and high reactivity and low reactivity phases can be identified. A low angle powder X-ray diffraction peak can indicate the presence of one or more crystal phases in a composition. A fingerprint region can exhibit fingerprint patterns of diffraction peaks associated with different reactivities. Information about polymerization of the diacetylenic monomers is disclosed using 13C nuclear magnetic resonance (“NMR”) characterization. Diacetylenic monomer compositions useful in ambient condition indicators, for example time-temperature indicators are disclosed.

    摘要翻译： 固体可聚合二炔单体组合物，包括在不同冷却条件下从各种溶剂体系共结晶的组合物可以显示与组合物的显色反应性相关的衍射图。 公开了高反应性组合物，并且可以鉴定出高反应性和低反应性相。 低角度粉末X射线衍射峰可以指示组合物中存在一个或多个结晶相。 指纹区域可以显示与不同反应性相关的衍射峰的指纹图谱。 使用13C核磁共振（NMR）表征公开了关于二乙炔单体的聚合的信息。 公开了用于环境条件指示剂的二乙炔单体组合物，例如时间 - 温度指示剂。

    CO-CRYSTALLIZABLE DIACETYLENIC MONOMER COMPOSITIONS, CRYSTAL PHASES AND MIXTURES, AND RELATED METHODS
    4.
    发明申请
    CO-CRYSTALLIZABLE DIACETYLENIC MONOMER COMPOSITIONS, CRYSTAL PHASES AND MIXTURES, AND RELATED METHODS 有权
    可结晶的二乙烯单体组合物，晶体相和混合物及相关方法

    公开(公告)号：US20110086995A1

    公开(公告)日：2011-04-14

    申请号：US12730835

    申请日：2010-03-24

    申请人： Elizabeth CASTILLO MARTINEZ ,  Ray H. Baughman ,  Lee J. Hall ,  Mikhail Kozlov ,  Dawn E. Smith ,  Thaddeus Prusik ,  Carl M. Lentz

    发明人： Elizabeth CASTILLO MARTINEZ ,  Ray H. Baughman ,  Lee J. Hall ,  Mikhail Kozlov ,  Dawn E. Smith ,  Thaddeus Prusik ,  Carl M. Lentz

    IPC分类号： C08F238/00

    CPC分类号： C07C275/20 ,  C08F238/02 ,  G01N31/229

    摘要： Solid polymerizable diacetylenic monomer compositions, including compositions co-crystallized from a diversity of solvent systems under diverse cooling conditions, can exhibit diffraction patterns associated with the color development reactivities of the compositions. High reactivity compositions are disclosed and high reactivity and low reactivity phases can be identified. A low angle powder X-ray diffraction peak can indicate the presence of one or more crystal phases in a composition. A fingerprint region can exhibit fingerprint patterns of diffraction peaks associated with different reactivities. Information about polymerization of the diacetylenic monomers is disclosed using 13C nuclear magnetic resonance (“NMR”) characterization. Diacetylenic monomer compositions useful in ambient condition indicators, for example time-temperature indicators are disclosed.

    摘要翻译： 固体可聚合二炔单体组合物，包括在不同冷却条件下从多种溶剂体系共结晶的组合物可以显示与组合物的显色反应性相关的衍射图。 公开了高反应性组合物，并且可以鉴定出高反应性和低反应性相。 低角度粉末X射线衍射峰可以指示组合物中存在一个或多个结晶相。 指纹区域可以显示与不同反应性相关的衍射峰的指纹图谱。 使用13C核磁共振（“NMR”）表征公开了关于二乙炔单体的聚合的信息。 公开了用于环境条件指示剂的二乙炔单体组合物，例如时间 - 温度指示剂。