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    POLYESTER RESIN AND METHOD FOR PREPARING THE SAME
    1.
    发明申请
    POLYESTER RESIN AND METHOD FOR PREPARING THE SAME 审中-公开
    聚酯树脂及其制备方法

    公开(公告)号：US20120177854A1

    公开(公告)日：2012-07-12

    申请号：US13394805

    申请日：2010-09-13

    申请人： Roy Lee ,  Jong-Ryang Kim ,  Jae-Bong Lim ,  Won-Jae Yoon ,  Dong-Jin Kim ,  Jyu-Tae Park ,  Yoo-Jin Lee

    发明人： Roy Lee ,  Jong-Ryang Kim ,  Jae-Bong Lim ,  Won-Jae Yoon ,  Dong-Jin Kim ,  Jyu-Tae Park ,  Yoo-Jin Lee

    IPC分类号： C08G63/672 ,  B32B1/02

    CPC分类号： C08G63/672 ,  C08G63/78 ,  G06F8/65 ,  Y10T428/1352

    摘要： A polyester resin copolymerized with isosorbide and 1,4-cyclohexane dimethanol and having an improved impact strength, and a method for preparing the same are disclosed. The copolymerized polyester resin has an alternating structure of acid moieties which are derived from acid components and diol moieties which are derived from diol components, wherein the acid components comprise terephthalic acid, and the diol components comprise (i) 5˜99 mol % of 1,4-cyclohexanedimethanol and (ii) 1˜60 mol % of isosorbide with respect to the total diol components.

    摘要翻译： 与异山梨醇和1,4-环己烷二甲醇共聚并具有改善的冲击强度的聚酯树脂及其制备方法。 共聚聚酯树脂具有衍生自酸组分的酸性部分和衍生自二醇组分的二醇部分的交替结构，其中酸组分包括对苯二甲酸，并且二醇组分包含（i）5〜99mol％的1 ，4-环己烷二甲醇和（ii）1至60摩尔％的异山梨醇相对于总二醇组分。

    Method for preparing polyarylene sulfide with reduced free iodine content
    2.
    发明授权
    Method for preparing polyarylene sulfide with reduced free iodine content 有权
    制备具有降低游离碘含量的聚芳硫醚的方法

    公开(公告)号：US09163119B2

    公开(公告)日：2015-10-20

    申请号：US13142932

    申请日：2009-12-28

    申请人： Yong-Jun Shin ,  Sung-Gi Kim ,  Jae-Bong Lim ,  Joon-Sang Cho ,  Il-Hoon Cha

    发明人： Yong-Jun Shin ,  Sung-Gi Kim ,  Jae-Bong Lim ,  Joon-Sang Cho ,  Il-Hoon Cha

    IPC分类号： C08G75/14 ,  C08G75/02 ,  C08G75/00

    CPC分类号： C08G75/16 ,  C08G75/0213 ,  C08G75/0263 ,  C08G75/0268

    摘要： The present invention relates to a method for preparing polyarylene sulfide with a reduced free iodine content. More specifically, the method for preparing polyarylene sulfide includes: (a) polymerizing reactants including a diiodo aromatic compound and a sulfur compound to form a polyarylene sulfide; and (b) maintaining the polyarylene sulfide product at 100 to 260° C. for heat-setting. The preparation method of the present invention effectively reduces the free iodine content of the polyarylene sulfide to prevent potential corrosion of facilities for the subsequent process and improves the properties of the polyarylene sulfide product such as thermal stability, so the method can be usefully applied to industrial fields in regard to the preparation of polyarylene sulfide.

    摘要翻译： 本发明涉及一种具有降低游离碘含量的聚芳硫醚的制备方法。 更具体地说，制备聚芳硫醚的方法包括：（a）使包含二碘芳族化合物和硫化合物的反应物聚合以形成聚芳硫醚; 和（b）将聚芳硫醚产物保持在100-260℃以进行热定型。 本发明的制备方法有效地降低了聚芳硫醚的游离碘含量，以防止随后工艺的设备的潜在腐蚀，提高聚芳硫醚产品的性能，如热稳定性，因此该方法可有效应用于工业 关于制备聚芳硫醚的领域。

    POLYARYLENE SULFIDE HAVING EXCELLENT PROCESSABILITY AND PREPARATION METHOD THEREOF
    3.
    发明申请
    POLYARYLENE SULFIDE HAVING EXCELLENT PROCESSABILITY AND PREPARATION METHOD THEREOF 有权
    具有优异处理性的聚亚烷基硫化物及其制备方法

    公开(公告)号：US20130115438A1

    公开(公告)日：2013-05-09

    申请号：US13697282

    申请日：2011-05-06

    申请人： Kyu-Tae Park ,  Sung-Gi Kim ,  Jae-Bong Lim ,  Il-Hoon Cha ,  Se-Ho Lee

    发明人： Kyu-Tae Park ,  Sung-Gi Kim ,  Jae-Bong Lim ,  Il-Hoon Cha ,  Se-Ho Lee

    IPC分类号： C08G75/14

    CPC分类号： C08G75/14 ,  C08G75/0204 ,  C08L81/02 ,  Y10T428/249921

    摘要： The present invention relates to polyarylene sulfide, in which a ratio of a peak area of a polymer chain of a second polyarylene sulfide having a lower molecular weight than the maximum peak molecular weight to a peak area of a polymer chain of a first polyarylene sulfide having a higher molecular weight than the maximum peak molecular weight is 1.3 or less in the molecular weight distribution of the polyarylene sulfide, as measured by gel permeation chromatography using polystyrene as a standard, and a preparation method thereof. This polyarylene sulfide exhibits excellent processability and generates no burrs (flashes) or the like, and can satisfactorily mold a product requiring high molding precision.

    摘要翻译： 本发明涉及聚芳硫醚，其中具有比最大峰分子量低的分子量的第二聚芳硫醚的聚合物链的峰面积与具有第一聚亚芳基硫醚的聚合物链的峰面积的比率 通过使用聚苯乙烯作为标准物的凝胶渗透色谱法测定，聚亚芳基硫醚的分子量分布中的分子量比最大峰分子量高的分子量为1.3以下，及其制备方法。 该聚亚芳基硫醚显示出优异的加工性，不产生毛刺（闪光）等，能够令人满意地成型需要高成型精度的产品。

    METHOD FOR PREPARING POLYARYLENE SULFIDE WITH REDUCED FREE IODINE CONTENT
    4.
    发明申请
    METHOD FOR PREPARING POLYARYLENE SULFIDE WITH REDUCED FREE IODINE CONTENT 有权
    制备具有降低免费碘含量的聚亚锡硫化物的方法

    公开(公告)号：US20110269935A1

    公开(公告)日：2011-11-03

    申请号：US13142932

    申请日：2009-12-28

    申请人： Yong-Jun Shin ,  Sung-gi Kim ,  Jae-Bong Lim ,  Joon-Sang Cho ,  II-Hoon Cha

    发明人： Yong-Jun Shin ,  Sung-gi Kim ,  Jae-Bong Lim ,  Joon-Sang Cho ,  II-Hoon Cha

    IPC分类号： C08G75/14

    CPC分类号： C08G75/16 ,  C08G75/0213 ,  C08G75/0263 ,  C08G75/0268

    摘要： The present invention relates to a method for preparing polyarylene sulfide with a reduced free iodine content. More specifically, the method for preparing polyarylene sulfide includes: (a) polymerizing reactants including a diiodo aromatic compound and a sulfur compound to form a polyarylene sulfide; and (b) maintaining the polyarylene sulfide product at 100 to 260° C. for heat-setting. The preparation method of the present invention effectively reduces the free iodine content of the polyarylene sulfide to prevent potential corrosion of facilities for the subsequent process and improves the properties of the polyarylene sulfide product such as thermal stability, so the method can be usefully applied to industrial fields in regard to the preparation of polyarylene sulfide.

    摘要翻译： 本发明涉及一种具有降低游离碘含量的聚芳硫醚的制备方法。 更具体地说，制备聚芳硫醚的方法包括：（a）使包含二碘芳族化合物和硫化合物的反应物聚合以形成聚芳硫醚; 和（b）将聚芳硫醚产物保持在100-260℃以进行热定型。 本发明的制备方法有效地降低了聚芳硫醚的游离碘含量，以防止随后工艺的设备的潜在腐蚀，提高聚芳硫醚产品的性能，如热稳定性，因此该方法可有效应用于工业 关于制备聚芳硫醚的领域。

    METHOD OF PREPARING IODINATED AROMATIC COMPOUNDS
    6.
    发明申请
    METHOD OF PREPARING IODINATED AROMATIC COMPOUNDS 有权
    制备芳族化合物的方法

    公开(公告)号：US20100222617A1

    公开(公告)日：2010-09-02

    申请号：US12599400

    申请日：2008-12-17

    申请人： Han-Seok Kim ,  Jae-Bong Lim ,  Il-Hoon Cha

    发明人： Han-Seok Kim ,  Jae-Bong Lim ,  Il-Hoon Cha

    IPC分类号： C07C17/06 ,  C07C17/392

    CPC分类号： C07C17/12 ,  C07C17/383 ,  C07C17/392 ,  C07C25/02

    摘要： The present invention relates to a method of preparing iodinated aromatic compounds, and more preferably a method of preparing iodinated aromatic compounds comprising a step of iodinating a reactant including an aromatic compound, a di-iodo aromatic compound or water, and iodine (I2) in the presence of a zeolite catalyst and oxygen. The method of the present invention has an advantage that by iodination of a reactant including the aromatic compound, and the di-iodo aromatic compound or water in the presence of the zeolite catalyst and oxygen, the temperature of the iodinating reactor can be controlled reliably and constantly, thereby resulting in improved productivity per unit weight of catalyst and inhibition of a side reaction in accordance with suppression of producing impurities. In addition, the productivity of the iodinated aromatic compound, preferably the di-iodo aromatic compound, more preferably a p-di-iodo aromatic compound can be improved, and thus can be widely used in the preparation of a di-iodo aromatic compound such as a p-di-iodo aromatic compound.

    摘要翻译： 本发明涉及一种制备碘化芳族化合物的方法，更优选的是制备碘化芳族化合物的方法，其包括将包含芳族化合物，二碘芳族化合物或水的反应物和碘（I 2）碘化的步骤 存在沸石催化剂和氧气。 本发明的方法具有的优点是，通过在沸石催化剂和氧气的存在下，通过碘化包含芳族化合物和二碘芳族化合物或水的反应物，可以可靠地控制碘化反应器的温度， 从而导致每单位重量催化剂的生产率提高，并且抑制副产物产生杂质。 此外，可以提高碘化芳香族化合物，优选二碘芳香族化合物，更优选对二碘芳香族化合物的生产率，因此可以广泛用于制备二碘芳族化合物，例如 作为对二碘芳族化合物。

    Polyarylene sulfide having excellent processability and preparation method thereof
    7.
    发明授权
    Polyarylene sulfide having excellent processability and preparation method thereof 有权
    具有优异加工性能的聚芳硫醚及其制备方法

    公开(公告)号：US09546248B2

    公开(公告)日：2017-01-17

    申请号：US13697282

    申请日：2011-05-06

    申请人： Kyu-Tae Park ,  Sung-Gi Kim ,  Jae-Bong Lim ,  Il-Hoon Cha ,  Se-Ho Lee

    发明人： Kyu-Tae Park ,  Sung-Gi Kim ,  Jae-Bong Lim ,  Il-Hoon Cha ,  Se-Ho Lee

    IPC分类号： C08G75/00 ,  C08G75/14 ,  C08G75/02 ,  C08L81/02

    CPC分类号： C08G75/14 ,  C08G75/0204 ,  C08L81/02 ,  Y10T428/249921

    摘要： The present invention relates to polyarylene sulfide, in which a ratio of a peak area of a polymer chain of a second polyarylene sulfide having a lower molecular weight than the maximum peak molecular weight to a peak area of a polymer chain of a first polyarylene sulfide having a higher molecular weight than the maximum peak molecular weight is 1.3 or less in the molecular weight distribution of the polyarylene sulfide, as measured by gel permeation chromatography using polystyrene as a standard, and a preparation method thereof. This polyarylene sulfide exhibits excellent processability and generates no burrs (flashes) or the like, and can satisfactorily mold a product requiring high molding precision.

    摘要翻译： 本发明涉及聚芳硫醚，其中具有比最大峰分子量低的分子量的第二聚芳硫醚的聚合物链的峰面积与具有第一聚亚芳基硫醚的聚合物链的峰面积的比率 通过使用聚苯乙烯作为标准物的凝胶渗透色谱法测定，聚亚芳基硫醚的分子量分布中的分子量比最大峰分子量高的分子量为1.3以下，及其制备方法。 该聚亚芳基硫醚显示出优异的加工性，不产生毛刺（闪光）等，能够令人满意地成型需要高成型精度的产品。

    Method for preparing polyarylene sulfide
    8.
    发明授权
    Method for preparing polyarylene sulfide 有权
    聚芳硫醚的制备方法

    公开(公告)号：US08859720B2

    公开(公告)日：2014-10-14

    申请号：US13141822

    申请日：2009-12-22

    申请人： Yong-Jun Shin ,  Jae-Bong Lim ,  Joon-Sang Cho ,  Il-Hoon Cha ,  Sung-Gi Kim

    发明人： Yong-Jun Shin ,  Jae-Bong Lim ,  Joon-Sang Cho ,  Il-Hoon Cha ,  Sung-Gi Kim

    IPC分类号： C08G75/14 ,  C08G75/02 ,  C08G75/16

    CPC分类号： C08G75/0209 ,  C08G75/0268

    摘要： The present invention relates to a method for preparing polyarylene sulfide, in which the polyarylene sulfide is prepared by a polymerization reaction of reactants including a diiodo aromatic compound and a sulfur compound, the method including: further adding 0.01 to 10.0 wt. % of diphenyl disulfide with respect to the weight of the polyarylene sulfide to the reactants to form the polyarylene sulfide having a melting point of 265 to 320° C.The diphenyl disulfide included in the reactants according to the present invention costs far less than other conventional polymerization inhibitors to dramatically lower the production cost, and the polyarylene sulfide prepared using the diphenyl disulfide exhibits low iodine content and very excellence in thermal stability.

    摘要翻译： 本发明涉及一种聚芳硫醚的制备方法，其中聚芳硫醚通过包括二碘芳族化合物和硫化合物的反应物的聚合反应制备，所述方法包括：进一步加入0.01至10.0wt。 相对于聚芳硫醚相对于反应物的重量的二苯基二硫化物的％为二苯醚，以形成熔点为265至320℃的聚芳硫醚。根据本发明的反应物中包含的二苯基二硫醚的成本远低于其它常规 聚合抑制剂大大降低生产成本，并且使用二苯基二硫化物制备的聚芳硫醚表现出低碘含量和非常优异的热稳定性。

    Method and apparatus for preparing alkyl ester fatty acid using fatty acid
    10.
    发明授权
    Method and apparatus for preparing alkyl ester fatty acid using fatty acid 有权
    使用脂肪酸制备烷基酯脂肪酸的方法和设备

    公开(公告)号：US08895765B2

    公开(公告)日：2014-11-25

    申请号：US13128171

    申请日：2009-09-22

    申请人： Soo-Hyun Kim ,  Hyun-Jun Cho ,  Chan-Woo Moon ,  Byoung-Kyung Ham ,  Jae-Bong Lim

    发明人： Soo-Hyun Kim ,  Hyun-Jun Cho ,  Chan-Woo Moon ,  Byoung-Kyung Ham ,  Jae-Bong Lim

    IPC分类号： C11C3/04 ,  B01J8/00 ,  C07C67/08 ,  C11C1/08 ,  C11C3/00 ,  B01J8/04

    CPC分类号： C07C67/08 ,  B01J8/0492 ,  C11C1/08 ,  C11C3/003 ,  Y02E50/13 ,  C07C69/52 ,  C07C69/24

    摘要： A method for preparing fatty acid alkyl ester for bio-diesel fuel is disclosed wherein fatty acid, specifically fatty acid distillate reacts with alcohol. The method does not require the glycerin purification process, and has the superior conversion ratio of fatty acid. The method for preparing fatty acid alkyl ester for bio-diesel fuel comprises the step of carrying out a counter current type esterification reaction of fatty acid and alcohol in each tray of a counter current column reactor at a temperature of 200 to 350° C. and a pressure of 1 to 35 bar. Here the raw material of the fatty acid is fed to an upper part of the counter current column reactor and the alcohol is fed to a lower part of the counter current column reactor. The counter current column reactor has a number of trays which are installed horizontally to have a number of vertical compartments. Each of the number of trays has an opening part at one end thereof to communicate one compartment with an adjoining compartment. The opening parts of two adjoining trays are alternately installed with each other.

    摘要翻译： 公开了一种制备用于生物柴油燃料的脂肪酸烷基酯的方法，其中脂肪酸特别是脂肪酸馏出物与醇反应。 该方法不需要甘油纯化方法，具有优异的脂肪酸转化率。 制备用于生物柴油燃料的脂肪酸烷基酯的方法包括在200-350℃的温度下在逆流塔式反应器的每个托盘中进行脂肪酸和醇的逆流型酯化反应的步骤，以及 压力为1至35巴。 这里，将该脂肪酸的原料送入逆流塔式反应器的上部，将该醇进料到逆流塔式反应器的下部。 逆流塔式反应器具有水平安装以具有多个垂直隔间的多个托盘。 多个托盘中的每一个在其一端具有开口部分，以将一个隔室与相邻的隔间连通。 两个相邻的托盘的开口部分彼此交替地安装。