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    Process for producing aliphatic amine derivative
    1.
    发明授权
    Process for producing aliphatic amine derivative 有权
    脂肪族胺衍生物的制造方法

    公开(公告)号：US6117948A

    公开(公告)日：2000-09-12

    申请号：US192385

    申请日：1998-11-16

    申请人： Tetsuaki Fukushima ,  Wataru Yoshida ,  Hiroshi Abe

    发明人： Tetsuaki Fukushima ,  Wataru Yoshida ,  Hiroshi Abe

    IPC分类号： C07C213/04 ,  C07C217/08 ,  C07C217/50 ,  C08G65/32 ,  C08L71/02

    CPC分类号： C07C213/04

    摘要： The present invention provides a process for easily producing an alkylene oxide adduct to an aliphatic amine compound which has a fully excellent color, is not turbid, and does not deteriorate in color even through long-term storage. That is, the present invention provides a process for producing an alkylene oxide adduct to a primary or secondary amine compound having an aliphatic, saturated or unsaturated, hydrocarbon radical having 8 to 22 carbon atoms, having an excellent color, by reacting an alkyene oxide to the amine compound, characterized by comprising the step of adding a base or an aqueous solution thereof to the amine compound and then heating the mixture.

    摘要翻译： 本发明提供一种容易地制备脂肪族胺化合物的烯化氧加合物的方法，其具有完全优异的颜色，不混浊，即使长期保存也不会劣化颜色。 也就是说，本发明提供了通过使氧化烯与氧化烯反应生成具有碳原子数为8〜22的脂肪族，饱和或不饱和的烃基的伯或仲胺化合物的烯化氧加合物，具有优异的颜色的方法 所述胺化合物的特征在于包括将碱或其水溶液加入到所述胺化合物中，然后加热所述混合物的步骤。

    Process for producing aliphatic nitrile
    2.
    发明授权
    Process for producing aliphatic nitrile 失效
    生产脂族腈的方法

    公开(公告)号：US5703264A

    公开(公告)日：1997-12-30

    申请号：US670787

    申请日：1996-06-24

    申请人： Wataru Yoshida ,  Tetsuaki Fukushima ,  Hideki Taniguchi ,  Hiroshi Abe

    发明人： Wataru Yoshida ,  Tetsuaki Fukushima ,  Hideki Taniguchi ,  Hiroshi Abe

    IPC分类号： B01J23/89 ,  C07B61/00 ,  C07C253/00 ,  C07C255/03

    CPC分类号： B01J23/8933 ,  B01J23/8926 ,  C07C253/00

    摘要： The process for producing an aliphatic nitrile comprising reacting an aliphatic alcohol having 6 to 40 carbon atoms with ammonia (a) in the presence of a copper/transition metal element in the fourth period other than Cr/platinum group element in the eighth group catalyst, (b) under a reaction system pressure in the range of from atmospheric pressure to 100 atm, (c) at a reaction system temperature in the range of from 100.degree. to 250.degree. C., (d) while introducing at least one gas selected from the group consisting of inert gases and hydrogen gas into the reaction system, (e) removing water formed by the reaction out of the reaction system, and (f) controlling the amount of the ammonia contained in the gas (exclusive of the water formed by the reaction) discharged out of the reaction system to 5 to 50% by volume based on the volume of the gas discharged (exclusive of the water formed by the reaction) makes it possible to produce various kinds of aliphatic nitriles.

    摘要翻译： 在第八组催化剂中除了Cr /铂族元素以外的第四期间，在铜/过渡金属元素的存在下，使具有6〜40个碳原子的脂肪醇与氨（a）反应的方法， （b）在大气压至100大气压范围内的反应体系压力下，（c）反应体系温度为100-250℃，（d）同时引入至少一种选择的气体 从由惰性气体和氢气组成的组中进入反应体系，（e）将由反应形成的水除去反应体系，和（f）控制气体中所含的氨的量（不包括形成的水 通过反应）从排出的气体的体积（不包括由反应形成的水）排出反应体系的5〜50体积％使得可以生产各种脂族腈。

    Process for producing a primary amine compound
    3.
    发明授权
    Process for producing a primary amine compound 有权
    伯胺化合物的制造方法

    公开(公告)号：US06307104B1

    公开(公告)日：2001-10-23

    申请号：US09552659

    申请日：2000-04-19

    申请人： Wataru Yoshida ,  Tetsuaki Fukushima

    发明人： Wataru Yoshida ,  Tetsuaki Fukushima

    IPC分类号： C07C20948

    CPC分类号： C07C209/48

    摘要： The present invention relates to a process for producing both of a primary amine compound and an alkylene oxide adduct thereto, given that the both are excellent in color, with high yield. That is, the process comprises hydrogenating a nitrile compound in the presence of a Raney catalyst comprising 90 to 96% by weight of Ni, 3 to 9% by weight of Al and 0.5 to 3% by weight of Mo being based on the total of the atoms of Ni, Al and Mo to obtain the primary amine compound. Further, an alkylene oxide may be added thereto to obtain an alkylene oxide adduct to the primary amine compound.

    摘要翻译： 本发明涉及一种制备伯胺化合物和其氧化烯加成物的方法，只要它们的颜色都优异，产率高。 也就是说，该方法包括在阮内催化剂存在下氢化腈化合物，该催化剂包含90至96重量％的Ni，3至9重量％的Al和0.5至3重量％的Mo，基于 Ni，Al和Mo的原子以获得伯胺化合物。 此外，可以向其中加入环氧烷以获得与伯胺化合物的烯化氧加合物。

    Polyamine
    4.
    发明授权
    Polyamine 有权
    多胺

    公开(公告)号：US06667382B1

    公开(公告)日：2003-12-23

    申请号：US09674410

    申请日：2000-11-01

    申请人： Kazuo Isobe ,  Ryoichi Tamaki ,  Keiichiro Tomioka ,  Wataru Yoshida ,  Tetsuaki Fukushima ,  Uichiro Nishimoto

    发明人： Kazuo Isobe ,  Ryoichi Tamaki ,  Keiichiro Tomioka ,  Wataru Yoshida ,  Tetsuaki Fukushima ,  Uichiro Nishimoto

    IPC分类号： C08G802

    CPC分类号： C08L95/005 ,  C07C211/14 ,  C08K5/17

    摘要： The present invention provides an amine or polyamine, which has a surface activity not inferior to a solid tallow-based amine and an excellent workability. A salt of the amine is suited for emulsifying asphalt and the like, and also provides an asphalt emulsion composition which is obtained by using the salt and which has a quick setting property. Namely, the prevent invention provides a polyamine represented by the formula (1), a process for producing the amine, and an asphalt emulsion composition containing a water-soluble salt of the amine. wherein R is a straight or branched hydrocarbon group having 8 to 22 carbon atoms; x is a number of 1 to 5; and each of y and z is a number of 0 to 5 with the proviso that both of y and z are not 0 at the same time.

    摘要翻译： 本发明提供一种胺或多胺，其具有不劣于固体牛脂基胺的表面活性和优异的可加工性。 胺的盐适于乳化沥青等，并且还提供了通过使用盐获得并且具有快速固化性能的沥青乳液组合物。 即，本发明提供由式（1）表示的多胺，胺的制造方法和含有胺的水溶性盐的沥青乳液组合物。其中R为直链或支链的烃基，其具有8〜 22个碳原子; x是1到5的数字; 并且y和z中的每一个是0至5的数，条件是y和z两者同时不为0。

    Process for production of ether amine
    6.
    发明授权
    Process for production of ether amine 有权
    醚胺生产工艺

    公开(公告)号：US06576794B2

    公开(公告)日：2003-06-10

    申请号：US10015657

    申请日：2001-12-17

    申请人： Tetsuaki Fukushima ,  Hiroyuki Masuda ,  Uichiro Nishimoto ,  Hiroshi Abe

    发明人： Tetsuaki Fukushima ,  Hiroyuki Masuda ,  Uichiro Nishimoto ,  Hiroshi Abe

    IPC分类号： C07C25330

    CPC分类号： C07C253/30 ,  C07C213/02 ,  C07C255/13 ,  C07C217/08

    摘要： A process for producing an ether amine (3), which comprises reacting a primary or secondary alcohol (1), ROH, with acrylonitrile in an amount of 0.8 to 1.2 equivalents of the alcohol (1) in the presence of an alkali metal hydroxide in an amount of not less than 0.01 part by weight, but less than 0.05 part by weight per 100 parts by weight of the alcohol (1) to obtain an alkyloxypropionitrile (2), and then adding water to the reaction system without removing the alkali metal hydroxide therefrom and effecting hydrogenation using a hydrogenation catalyst: ROH(1)+CH2=CHCN→ROCH2CH2CN(2)→ROCH2CH2CH2NH2(3) wherein R denotes a linear or branched alkyl or alkenyl group having 6 to 24 carbon atoms. Also disclosed are a process for producing an ether tertiary amine (5), R—O—CH2—CH2—CH2—N(CH2R1)2, which comprises adding an aldehyde to the resulting ether amine (3) in the presence of a metal catalyst or a Raney nickel catalyst, and a process for producing an ether quaternary ammonium salt (6), R—O—CH2—CH2—CH2—N(CH2R1)2(R2), which comprises reacting a quaternizing agent with the ether tertiary amine (5).

    摘要翻译： 一种制备醚胺（3）的方法，其包括在碱金属氢氧化物存在下，将伯醇或仲醇（1），ROH与丙烯腈的量为0.8至1.2当量的醇（1） 相对于每100重量份的醇（1），不少于0.01重量份，但小于0.05重量份，得到烷氧基丙腈（2），然后向反应体系中加入水而不除去碱金属 使用氢化催化剂氢化，其中R表示碳原子数为6〜24的直链或支链烷基或链烯基。 还公开了制备醚叔胺（5），RO-CH2-CH2-CH2-N（CH2R1）2的方法，其包括在金属催化剂存在下将醛加到得到的醚胺（3）中，或 阮内镍催化剂和制备醚季铵盐（6），RO-CH2-CH2-CH2-N（CH2R1）2（R2）的方法，其包括使季铵化剂与醚叔胺（5）反应， 。

    Hair cosmetic compositions
    9.
    发明授权
    Hair cosmetic compositions 有权
    头发化妆品组合物

    公开(公告)号：US06737050B2

    公开(公告)日：2004-05-18

    申请号：US10026641

    申请日：2001-12-27

    申请人： Yasuhiro Doi ,  Keiko Hasebe ,  Hiroyuki Masuda ,  Tetsuaki Fukushima ,  Uichiro Nishimoto ,  Hiroshi Abe

    发明人： Yasuhiro Doi ,  Keiko Hasebe ,  Hiroyuki Masuda ,  Tetsuaki Fukushima ,  Uichiro Nishimoto ,  Hiroshi Abe

    IPC分类号： A61K7075

    CPC分类号： A61K8/898 ,  A61K8/416 ,  A61K8/44 ,  A61K8/463 ,  A61K8/60 ,  A61K8/73 ,  A61K8/891 ,  A61Q5/00 ,  A61Q5/02 ,  A61Q5/12

    摘要： Provided are a hair cosmetic composition comprising an ether type cationic surfactant represented by the following formula (1): wherein, R1 represents a linear or branched C6-24 alkyl or alkenyl group, R2 and R4 each represents a C1-6 alkyl group or —(AO)nH (A: a C2-4 alkylene group, n: a number of from 1 to 6 with the proviso that n pieces of A may be the same or different and their sequence is optional), R3 represents a C1-6 alkyl group or —(A′O)mH (A′: a C2-4 alkylene group, m: a number of from 1 to 6 with the proviso that m pieces of A may be the same or different and their sequence is optional), and X− represents an anion; a hair cleansing composition containing the cationic surfactant(1); and a method of treating hair with these compositions. The hair cosmetic composition of the present invention can impart good flexibility and smoothness to hair not only when it is wetted but also after drying. When used as a hair cleansing composition, it provides excellent quality of foam and feeling upon use and exhibits good low-temperature stability.

    摘要翻译： 提供一种包含由下式（1）表示的醚型阳离子表面活性剂的毛发化妆品组合物：其中，R 1表示直链或支链的C 6-24烷基或链烯基，R 2和R 4各自 表示C 1-6烷基或 - （AO）n H（A：C 2-4亚烷基，n：1至6的数，条件是n个A可以相同或不同，它们的顺序为 可选），R 3表示C 1-6烷基或 - （A'O）m H（A'：C 2-4亚烷基，m：1至6的数，条件是m个A 可以相同或不同，它们的顺序是任选的），而X“表示阴离子; 含有阳离子表面活性剂（1）的毛发清洁组合物; 以及使用这些组合物处理毛发的方法。本发明的毛发化妆品组合物可以赋予头发良好的柔韧性和光滑性，不仅当其被润湿时，而且在干燥之后。 当用作头发清洁组合物时，它提供优异的泡沫质量和使用感，并表现出良好的低温稳定性。