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    Methods for identifying and utilizing rubber compositions with good wet traction performance
    1.
    发明授权
    Methods for identifying and utilizing rubber compositions with good wet traction performance 有权
    用于识别和利用具有良好湿牵引性能的橡胶组合物的方法

    公开(公告)号：US08841376B2

    公开(公告)日：2014-09-23

    申请号：US11967829

    申请日：2007-12-31

    申请人： Xiao-Dong Pan ,  Pat Sadhukhan ,  Hiroshi Mouri ,  Michael W. Hayes ,  Dennis R. Brumbaugh

    发明人： Xiao-Dong Pan ,  Pat Sadhukhan ,  Hiroshi Mouri ,  Michael W. Hayes ,  Dennis R. Brumbaugh

    IPC分类号： C08C19/00 ,  C08K3/22 ,  C08K3/00 ,  B82Y30/00

    CPC分类号： B82Y30/00 ,  C08K3/013 ,  C08K3/22 ,  C08K2201/011 ,  C08L21/00

    摘要： A rubber formulation with good wet traction properties includes one or more elastomers and at least two types of particulate filler materials including at least one of which has a relatively high free surface energy in water (i.e., a supplemental filler). The formulation containing the supplemental filler(s) can provide a vulcanizate that has a British pendulum (skid) number that is at least ˜5% greater than that of a vulcanizate made from an essentially identical formulation that does not contain the supplemental filler(s). Also provided is a method for providing such a formulation which involves identifying one or more supplemental fillers having relatively high free surface energies in water, replacing at least 15% (by wt.) of one or more of the conventional particulate fillers in the formulation with an approximately equivalent volume of supplemental filler particles, and providing the modified formulation.

    摘要翻译： 具有良好湿牵引性能的橡胶制剂包括一种或多种弹性体和至少两种类型的颗粒填料，包括其中至少一种在水中具有相对高的游离表面能（即，补充填料）。 含有补充填料的制剂可以提供一种硫化橡胶，其具有比不含补充填料的基本相同的制剂制成的硫化橡胶的至少约5％的英制摆（滑动）数量 ）。 还提供了一种用于提供这种制剂的方法，其包括鉴定一种或多种在水中具有相对高的游离表面能的补充填料，用制剂中至少15％（重量）的一种或多种常规颗粒填料替代， 约等量的补充填料颗粒，并提供改性制剂。

    METHODS FOR IDENTIFYING AND UTILIZING RUBBER COMPOSITIONS WITH GOOD WET TRACTION PERFORMANCE
    2.
    发明申请
    METHODS FOR IDENTIFYING AND UTILIZING RUBBER COMPOSITIONS WITH GOOD WET TRACTION PERFORMANCE 有权
    用于识别和利用具有良好湿度牵引性能的橡胶组合物的方法

    公开(公告)号：US20080161467A1

    公开(公告)日：2008-07-03

    申请号：US11967829

    申请日：2007-12-31

    申请人： Xiao-Dong Pan ,  Pat Sadhukhan ,  Hiroshi Mouri ,  Michael W. Hayes ,  Dennis R. Brumbaugh

    发明人： Xiao-Dong Pan ,  Pat Sadhukhan ,  Hiroshi Mouri ,  Michael W. Hayes ,  Dennis R. Brumbaugh

    IPC分类号： C08C19/00 ,  C08K3/22

    CPC分类号： B82Y30/00 ,  C08K3/013 ,  C08K3/22 ,  C08K2201/011 ,  C08L21/00

    摘要： A rubber formulation with good wet traction properties includes one or more elastomers and at least two types of particulate filler materials including at least one of which has a relatively high free surface energy in water (i.e., a supplemental filler). The formulation containing the supplemental filler(s) can provide a vulcanizate that has a British pendulum (skid) number that is at least ˜5% greater than that of a vulcanizate made from an essentially identical formulation that does not contain the supplemental filler(s). Also provided is a method for providing such a formulation which involves identifying one or more supplemental fillers having relatively high free surface energies in water, replacing at least 15% (by wt.) of one or more of the conventional particulate fillers in the formulation with an approximately equivalent volume of supplemental filler particles, and providing the modified formulation.

    摘要翻译： 具有良好湿牵引性能的橡胶制剂包括一种或多种弹性体和至少两种类型的颗粒填料，包括其中至少一种在水中具有相对高的游离表面能（即，补充填料）。 含有补充填料的制剂可以提供一种硫化橡胶，其具有比不含补充填料基本上相同的制剂制成的硫化橡胶的至少约5％的英制摆（滑动）数量 ）。 还提供了一种用于提供这种制剂的方法，其包括鉴定一种或多种在水中具有相对高的游离表面能的补充填料，用制剂中至少15％（重量）的一种或多种常规颗粒填料替代， 约等量的补充填料颗粒，并提供改性制剂。

    Method of preparing syndiotactic 1,2-polybutadiene with a chromium-based catalyst system
    6.
    发明授权
    Method of preparing syndiotactic 1,2-polybutadiene with a chromium-based catalyst system 失效
    用铬基催化剂体系制备间同立构1,2-聚丁二烯的方法

    公开(公告)号：US5919875A

    公开(公告)日：1999-07-06

    申请号：US173254

    申请日：1998-10-14

    申请人： Steven Luo ,  Michael W. Hayes ,  Dennis R. Brumbaugh

    发明人： Steven Luo ,  Michael W. Hayes ,  Dennis R. Brumbaugh

    IPC分类号： C08F2/38 ,  C08F4/69 ,  C08F136/06

    CPC分类号： C08F136/06 ,  C08F2410/01

    摘要： A process for polymerizing 1,3-butadiene into syndiotactic 1,2-polybutadiene is described using a catalyst system comprising (a) a chromium-containing compound, (b) an organoaluminum hydride, and (c) a hydrogen phosphite. The use of the catalyst system avoids the use of environmentally detrimental components such as carbon disulfide and halogenated solvents. The syndiotactic 1,2-polybutadiene can be used as a plastic or as an additive for rubber compositions wherein it can crosslink with conventional rubbers using conventional crosslinking agents.

    摘要翻译： 使用包含（a）含铬化合物，（b）有机铝氢化物和（c）亚磷酸氢盐的催化剂体系描述了将1,3-丁二烯聚合成间规1,2-聚丁二烯的方法。 催化剂体系的使用避免使用环境有害组分如二硫化碳和卤化溶剂。 间规1,2-聚丁二烯可以用作塑料或作为橡胶组合物的添加剂，其中它可以使用常规的交联剂与常规橡胶交联。

    FUNCTIONALIZED POLYMER AND METHODS FOR MAKING AND USING
    8.
    发明申请
    FUNCTIONALIZED POLYMER AND METHODS FOR MAKING AND USING 有权
    功能化聚合物及其制备和使用方法

    公开(公告)号：US20100311899A1

    公开(公告)日：2010-12-09

    申请号：US12810845

    申请日：2008-12-26

    申请人： Steven Luo ,  Dennis R. Brumbaugh ,  Michael W. Hayes ,  Yoichi Ozawa ,  Jason T. Poulton

    发明人： Steven Luo ,  Dennis R. Brumbaugh ,  Michael W. Hayes ,  Yoichi Ozawa ,  Jason T. Poulton

    IPC分类号： C08C19/25 ,  C08F8/30

    CPC分类号： C08F8/42 ,  C08C19/44 ,  C08F8/30 ,  C08K3/04 ,  C08L9/00 ,  C08L15/00 ,  C08L2666/08

    摘要： A functionalized polymer includes a polymer chain and a terminal functionality that includes at least one disilylamino group. The polymer can be the reaction product of a terminally active polymer chain and a compound that includes at least one disilylamino group and a group capable of reacting with terminally active polymers. Methods for making and using such polymers also are provided, as are compositions containing the polymer and one or more types of filler particles as well as vulcanizates provided from such compositions.

    摘要翻译： 官能化聚合物包括聚合物链和包括至少一个二甲硅烷基氨基的末端官能团。 聚合物可以是末端活性聚合物链和包含至少一个二甲硅烷基氨基和能够与末端活性聚合物反应的基团的化合物的反应产物。 还提供了制备和使用这些聚合物的方法，以及含有聚合物和一种或多种类型的填料颗粒的组合物以及由这种组合物提供的硫化橡胶。

    Method for quantitative analysis of styrene microblock content
    10.
    发明授权
    Method for quantitative analysis of styrene microblock content 有权
    苯乙烯微块含量定量分析方法

    公开(公告)号：US08618226B2

    公开(公告)日：2013-12-31

    申请号：US13476387

    申请日：2012-05-21

    申请人： Waruna Chethiya Bandara Kiridena ,  Mindaugas Rackaitis ,  Terrence Eugene Hogan ,  Dennis R. Brumbaugh ,  William L. Hergenrother

    发明人： Waruna Chethiya Bandara Kiridena ,  Mindaugas Rackaitis ,  Terrence Eugene Hogan ,  Dennis R. Brumbaugh ,  William L. Hergenrother

    IPC分类号： G01N3/44 ,  C08F6/00 ,  G01N1/22 ,  C08F236/10

    CPC分类号： C08F236/10 ,  G01N31/12 ,  G01N33/442

    摘要： A method for determining the styrene microblock content of a copolymer sample, the method comprising: (i) pyrolyzing the copolymer sample to form polymer fragments of the polymer sample; (ii) analyzing the fragments to determine the relative amounts of styrene monomer fragments, styrene dimer fragments, and styrene trimer fragments, where the relative amounts of the fragments include the amount of any given fragment relative to the total of the monomer fragments, dimer fragments, and trimer fragments; and (iii) using the relative amounts of the styrene monomer fragments, styrene dimer fragments, and styrene trimer fragments to predict the polystyrene microblock content from a mathematical model that is based upon the relative styrene monomer fragments, relative styrene dimer fragments, relative styrene trimer fragments, and microblock content of a copolymer having known microblock content.

    摘要翻译： 一种用于测定共聚物样品的苯乙烯微团含量的方法，所述方法包括：（i）热解共聚物样品以形成聚合物样品的聚合物片段; （ii）分析片段以确定苯乙烯单体片段，苯乙烯二聚体片段和苯乙烯三聚体片段的相对量，其中片段的相对量包括相对于单体片段总数的任何给定片段的量，二聚体片段 ，和三聚体片段; 和（iii）使用苯乙烯单体片段，苯乙烯二聚体片段和苯乙烯三聚物片段的相对量从基于相对苯乙烯单体片段，相对苯乙烯二聚体片段，相对苯乙烯三聚物的数学模型预测聚苯乙烯微块含量 具有已知微块含量的共聚物的片段和微嵌段含量。