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    Polymer dispersion with a colour effect
    1.
    发明授权
    Polymer dispersion with a colour effect 有权
    聚合物色散具有色彩效果

    公开(公告)号：US07776237B2

    公开(公告)日：2010-08-17

    申请号：US10553793

    申请日：2004-05-04

    申请人： Xu He ,  Reinhold J. Leyrer ,  Holger Schöpke

    发明人： Xu He ,  Reinhold J. Leyrer ,  Holger Schöpke

    IPC分类号： B05D5/06 ,  C09D5/36 ,  C09D7/14 ,  C09D5/02 ,  C09D151/10 ,  C08F2/22 ,  C08F265/00

    CPC分类号： C08L51/003 ,  B05D3/0254 ,  B05D5/06 ,  C08F257/02 ,  C08F265/00 ,  C08F265/04 ,  C08F265/06 ,  C08F291/00 ,  C09D151/003 ,  Y10S525/902 ,  C08L2666/02

    摘要： Process for improving the brilliance of color and the stability of a colored polymer system, which is composed of a matrix and of discrete polymer particles distributed in accordance with a defined spatial lattice structure in the matrix, and which is obtained by filming of an emulsion polymer with core/shell structure, which comprises using an emulsion polymer obtainable by polymerizing monomers in at least one first stage (core monomers), then polymerizing monomers in at least one further, second stage (transition stage), and finally polymerizing monomers in a third stage (shell monomers), where, based on the percentage constitution of the monomer mixtures of the three stages, at most 30% by weight of the monomers of the first stage are identical with those of the third stage, and 5% of the monomers of the second stage are identical with, respectively, those of the first and those of the third stage, and not more than 60% by weight of the monomers of the 2nd stage here are monomers absent in the 1st stage and also absent in the 3rd stage.

    摘要翻译： 用于提高颜色亮度和着色聚合物体系的稳定性的方法，其由基质和根据基质中限定的空间格子结构分布的离散聚合物颗粒组成，并且其通过将乳液聚合物 具有核/壳结构，其包括使用可通过在至少一个第一阶段（核心单体）中聚合单体获得的乳液聚合物，然后在至少一个第二阶段（过渡阶段）中聚合单体，最后在第三阶段中聚合单体 阶段（壳单体），其中基于三个阶段的单体混合物的百分比构成，至多30重量％的第一阶段的单体与第三阶段的单体相同，并且5％的单体 第二阶段的单体分别与第一阶段和第三阶段的相同，并且不超过60重量％的第二阶段的单体是单体a 在第一阶段也没有在第三阶段。

    Preparation of emulsion homo- and copolymers and device therefore
    4.
    发明授权
    Preparation of emulsion homo- and copolymers and device therefore 失效
    因此制备乳液均聚物和共聚物和装置

    公开(公告)号：US06660814B1

    公开(公告)日：2003-12-09

    申请号：US08940996

    申请日：1997-09-30

    申请人： Huberrus Kröner ,  Wolfgang Klanig ,  Bradley Ronald Morrison ,  Rainer Klostermann ,  Holger Schöpke ,  Walter Kastenhuber

    发明人： Huberrus Kröner ,  Wolfgang Klanig ,  Bradley Ronald Morrison ,  Rainer Klostermann ,  Holger Schöpke ,  Walter Kastenhuber

    IPC分类号： C08F200

    CPC分类号： B01J19/1881 ,  C08F2/22 ,  Y10S526/92 ,  Y10S526/922

    摘要： In the process and a correspondingly appropriate device for preparing homo- or copolymers of at least one of the, polymerizable monomers of the group consisting of styrene, butadiene, vinyl chloride, vinyl acetate, vinylidene chloride, alkyl (meth)acrylatc (meth)acrylic acid, (meth)acrylonitrile and (meth)acrylamide reaction is carried out at at least 40° C. in the presence of a dispersing auxiliary and of a free-radical polymerization initiator such that at least 85% by weight of the polymer is formed from these monomers. In the multistage process the procedure is such that a) in a first stage water is added as a solvent which is inert in the reaction and dispersing auxiliaries, seed and a first portion of monomer(s) are added if desired, b) in a second stage initiator is added, and c) in a third stage the remainder or all of the monomer(s) is added directly or in emulsion form and in the presence of further water and, if desired, further dispersing auxiliary or other auxiliaries, it also being possible to operate any two of the stages as a single stage. The reaction mixture, which is in emulsion form, is moved in all or some stages through an external circuit which leads from and back to the reaction vessel (2) and comprises at least one low-shear pump (7) and at least one heat exchanger (8) having an essentially laminar flow profile. The products prepared by this process, which involves short preparation times, have good performance properties (for adhesive bonds, for example).

    摘要翻译： 在该方法中以及用于制备苯乙烯，丁二烯，氯乙烯，乙酸乙烯酯，偏二氯乙烯，（甲基）丙烯酸（甲基）丙烯酸烷基酯，（甲基）丙烯酸烷基酯（甲基）丙烯酸烷基酯中的至少一种可聚合单体的均聚物或共聚物的相应适当的装置 酸，（甲基）丙烯腈和（甲基）丙烯酰胺反应在分散助剂和自由基聚合引发剂的存在下在至少40℃下进行，使得形成至少85重量％的聚合物 来自这些单体。 在多级方法中，a）在第一阶段中加入水作为在反应中为惰性的溶剂，并且分散助剂，如果需要，加入种子和第一部分单体，b）在第二阶段 并且c）在第三阶段中，剩余或全部单体直接或以乳液形式加入，并且在另外的水的存在下，如果需要，还可以分散辅助剂或其它助剂，它也是 可以将任何两个阶段操作为单一阶段。乳液形式的反应混合物通过从反应容器（2）引出并返回到反应容器（2）的外部回路在所有或某些阶段中移动，并且至少包括 一个低剪切泵（7）和至少一个具有基本层流轮廓的热交换器（8）。 通过该方法制备的产品，其制备时间短，具有良好的性能（例如粘合剂粘合）。

    Method for producing aqueous active substance compositions of active substances that are hardly soluble in water
    5.
    发明授权
    Method for producing aqueous active substance compositions of active substances that are hardly soluble in water 有权
    生成难溶于水的活性物质的水性活性物质组合物的制造方法

    公开(公告)号：US08974806B2

    公开(公告)日：2015-03-10

    申请号：US11658472

    申请日：2005-08-03

    申请人： Patrick Amrhein ,  Holger Schöpke ,  Gunnar Kleist ,  Michael Kluge

    发明人： Patrick Amrhein ,  Holger Schöpke ,  Gunnar Kleist ,  Michael Kluge

    IPC分类号： A01N25/12 ,  A01P15/00 ,  A01P3/00 ,  A01P13/00 ,  A01N43/36 ,  A01N25/04 ,  A01N25/26 ,  A01N25/28 ,  A01N43/653 ,  A01N53/00 ,  C08L97/02 ,  B27K3/00 ,  B27K3/15 ,  C08L33/08 ,  C08L35/02

    CPC分类号： A01N43/36 ,  A01N25/04 ,  A01N25/26 ,  A01N25/28 ,  A01N43/653 ,  A01N53/00 ,  B27K3/007 ,  B27K3/15 ,  C08L33/08 ,  C08L35/02 ,  C08L97/02 ,  A01N2300/00

    摘要： The present invention relates to a process for preparing aqueous active compound compositions of active compounds which are poorly soluble in water, in particular of active compounds for the protection of crops and materials. Moreover, the invention relates to the active compound compositions obtainable by the process and to their use for controlling harmful organisms in plants and in the protection of materials.The process comprises the following steps: a) provision of an aqueous suspension of solid active compound particles of at least one active compound having a solubility in water of not more than 5 g/l at 25° C./1013 mbar, comprising, for stabilizing the active compound particles, at least one surfactant, where the active compound particles in the suspension have a mean particle size, determined by dynamic light scattering, of not more than 1200 nm, b) emulsion polymerization of a first monomer composition M1 in the aqueous suspension of the active compound, where the monomer composition M1 comprises at least 95% by weight, based on its total weight, of at least one neutral, monoethylenically unsaturated monomer M1.1 having a solubility in water of not more than 30 g/l at 25° C./1013 mbar, giving an aqueous dispersion of polymer/active compound particles, and c) emulsion polymerization of a second monomer composition M2 in an aqueous dispersion of the polymer/active compound particles obtained in step b), where the monomer composition M2 comprises at least 60% by weight, based on its total weight, of at least one neutral, monoethylenically unsaturated monomer M2.1 having a solubility in water of not more than 30 g/l at 25° C./1013 mbar.

    摘要翻译： 本发明涉及一种制备水溶性较差的活性化合物的水性活性化合物组合物的方法，特别是用于保护作物和材料的活性化合物。 此外，本发明涉及通过该方法获得的活性化合物组合物及其用于控制​​植物中的有害生物和保护材料的用途。 该方法包括以下步骤：a）提供至少一种在25℃下在水中具有不超过5克/升溶解度的活性化合物的固体活性化合物颗粒的水性悬浮液。1013毫巴， 稳定活性化合物颗粒，至少一种表面活性剂，其中悬浮液中的活性化合物颗粒具有不超过1200nm的动态光散射测定的平均粒径，b）第一单体组合物M1在 活性化合物的水性悬浮液，其中单体组合物M1占总重量的至少95重量％至少一种在水中的溶解度不超过30g / m 2的中性单烯属不饱和单体M1.1， l在25℃/ 1013毫巴下，得到聚合物/活性化合物颗粒的水分散体，和c）第二单体组合物M2在聚合物/活性化合物颗粒的水分散体中的乳液聚合 其中单体组合物M2占其总重量至少为60重量％，至少一种在水中的溶解度不超过30g / l的至少一种中性单烯属不饱和单体M2.1 在25℃/ 1013毫巴。

    Aqueous fungicidal composition and use thereof for combating harmful microorganisms
    6.
    发明授权
    Aqueous fungicidal composition and use thereof for combating harmful microorganisms 有权
    杀真菌组合物及其用于防治有害微生物的用途

    公开(公告)号：US08741968B2

    公开(公告)日：2014-06-03

    申请号：US12831055

    申请日：2010-07-06

    申请人： Gunnar Kleist ,  Joerg Habicht ,  Holger Schöpke ,  Patrick Amrhein ,  Helga Göttsche

    发明人： Reimer Göttsche ,  Gunnar Kleist ,  Joerg Habicht ,  Holger Schöpke ,  Patrick Amrhein

    IPC分类号： A01N25/04 ,  A01N43/653 ,  A01N43/36 ,  A01N47/12 ,  A01P3/00 ,  C08L33/14 ,  C08L25/06

    CPC分类号： A01N25/02 ,  A01N25/04 ,  A01N43/36 ,  A01N43/653 ,  A01N47/12 ,  B27K3/007 ,  B27K3/15 ,  C08L25/06 ,  C08L33/14 ,  C08L97/02 ,  A01N25/30 ,  A01N2300/00

    摘要： The invention relates to aqueous fungicidal active substance compositions and to their use in the control of harmful microorganisms and in particular in the protection of cellulose-comprising materials, particularly wood, from infection by microorganisms, in particular those harmful fungi which can damage wood or cellulose.The active substance composition according to the invention comprises: a) at least one fungicidal organic active substance with a solubility in water of not more than 5 g/l at 25° C./1013 mbar, and b) a finely-divided polymer with an average particle size, determined by dynamic light scattering, of not more than 300 nm, in which the polymer particles comprise the active substance, the polymer being formed from ethylenically unsaturated monomers M comprising: at least 60% by weight, based on the total amount of the monomers M, of at least one neutral monoethylenically unsaturated monomer M1 with a solubility in water of not more than 30 g/l at 25° C., and up to 40% by weight, based on the total amount of the monomers M, of one or more ethylenically unsaturated monomers M2 other than the monomers M1.

    摘要翻译： 本发明涉及含水杀真菌活性物质组合物及其在控制有害微生物中的用途，特别是用于保护由微生物感染的纤维素材料特别是木材，特别是可损害木材或纤维素的那些有害真菌 。 根据本发明的活性物质组合物包含：a）至少一种在25℃，1013毫巴下在水中溶解度不超过5克/升的杀真菌有机活性物质，和b） 通过动态光散射确定的不大于300nm的平均粒度，其中聚合物颗粒包含活性物质，聚合物由烯键式不饱和单体M形成，包括：至少60重量％，基于总计 至少一种在25℃下在水中的溶解度不超过30g / l的至少一种中性单烯键式不饱和单体M1的单体量，和基于单体总量的至多40重量％ M，除了单体M1之外的一种或多种烯属不饱和单体M2。

    AQUEOUS FUNGICIDAL COMPOSITION AND USE THEREOF FOR COMBATING HARMFUL MICROORGANISMS
    7.
    发明申请
    AQUEOUS FUNGICIDAL COMPOSITION AND USE THEREOF FOR COMBATING HARMFUL MICROORGANISMS 有权
    水质防霉组合物及其用于组合有害微生物的用途

    公开(公告)号：US20100273897A1

    公开(公告)日：2010-10-28

    申请号：US12831055

    申请日：2010-07-06

    申请人： Reimer GÖTTSCHE ,  Heir Helga Göttsche ,  Gunnar Kleist ,  Joerg Habicht ,  Holger Schöpke ,  Patrick Amrhein

    发明人： Reimer GÖTTSCHE ,  Heir Helga Göttsche ,  Gunnar Kleist ,  Joerg Habicht ,  Holger Schöpke ,  Patrick Amrhein

    IPC分类号： A01N25/02

    CPC分类号： A01N25/02 ,  A01N25/04 ,  A01N43/36 ,  A01N43/653 ,  A01N47/12 ,  B27K3/007 ,  B27K3/15 ,  C08L25/06 ,  C08L33/14 ,  C08L97/02 ,  A01N25/30 ,  A01N2300/00

    摘要： The invention relates to aqueous fungicidal active substance compositions and to their use in the control of harmful microorganisms and in particular in the protection of cellulose-comprising materials, particularly wood, from infection by microorganisms, in particular those harmful fungi which can damage wood or cellulose.The active substance composition according to the invention comprises: a) at least one fungicidal organic active substance with a solubility in water of not more than 5 g/l at 25° C./1013 mbar, and b) a finely-divided polymer with an average particle size, determined by dynamic light scattering, of not more than 300 nm, in which the polymer particles comprise the active substance, the polymer being formed from ethylenically unsaturated monomers M comprising: at least 60% by weight, based on the total amount of the monomers M, of at least one neutral monoethylenically unsaturated monomer M1 with a solubility in water of not more than 30 g/l at 25° C., and up to 40% by weight, based on the total amount of the monomers M, of one or more ethylenically unsaturated monomers M2 other than the monomers M1.

    摘要翻译： 本发明涉及含水杀真菌活性物质组合物及其在控制有害微生物中的用途，特别是用于保护由微生物感染的纤维素材料特别是木材，特别是可损害木材或纤维素的那些有害真菌 。 根据本发明的活性物质组合物包含：a）至少一种在25℃，1013毫巴下在水中溶解度不超过5克/升的杀真菌有机活性物质，和b） 通过动态光散射确定的不大于300nm的平均粒度，其中聚合物颗粒包含活性物质，聚合物由烯键式不饱和单体M形成，包括：至少60重量％，基于总计 至少一种在25℃下在水中的溶解度不超过30g / l的至少一种中性单烯键式不饱和单体M1的单体量，和基于单体总量的至多40重量％ M，除了单体M1之外的一种或多种烯属不饱和单体M2。

    Aqueous insecticidal compositions and the use thereof for protecting lignocellulose-containing materials
    8.
    发明授权
    Aqueous insecticidal compositions and the use thereof for protecting lignocellulose-containing materials 有权
    水性杀虫组合物及其用于保护含木素纤维素的材料的用途

    公开(公告)号：US08999358B2

    公开(公告)日：2015-04-07

    申请号：US11885799

    申请日：2006-03-08

    申请人： Patrick Amrhein ,  Gunnar Kleist ,  Dirk Haentzschel ,  Joerg Habicht ,  Holger Schöpke

    发明人： Patrick Amrhein ,  Gunnar Kleist ,  Dirk Haentzschel ,  Joerg Habicht ,  Holger Schöpke

    IPC分类号： A01N25/04 ,  A01N53/02 ,  A01N47/10 ,  A01N57/10 ,  A01N43/36 ,  A01P7/04 ,  A01N25/26 ,  A01N25/28 ,  A01N53/00 ,  B27K3/00 ,  B27K3/15

    CPC分类号： A01N43/36 ,  A01N25/04 ,  A01N25/26 ,  A01N25/28 ,  A01N53/00 ,  B27K3/007 ,  B27K3/15 ,  A01N2300/00

    摘要： The present invention relates to aqueous insecticidal preparations in the form of an aqueous dispersion of finely divided polymer particles which comprise at least one insecticidal organic active ingredient with a solubility in water of not more than 5 g/l at 25° C. at 1013 mbar and which have a mean particle size, determined by dynamic light scattering, of not more than 300 nm, where the polymer particles which comprise the at least one insecticidal active ingredient of a cationic surface charge and where the aqueous dispersion of the active-ingredient-comprising polymer particles is obtainable by subjecting a monomer composition of ethylenically unsaturated monomers M, in which the ethylenically unsaturated monomers M comprise the at least one insecticidal active ingredient in dissolved form, to radical aqueous emulsion polymerization. The invention also related to the use of such aqueous insecticide compositions for protecting lignocellulosic materials, in particular timber, against attack by harmful insects.

    摘要翻译： 本发明涉及细分散的聚合物颗粒的水性分散体形式的含水杀虫剂，其含有至少一种在25℃，1013毫巴下在水中的溶解度不超过5克/升的杀虫有机活性成分 并且其具有不大于300nm的由动态光散射确定的平均粒度，其中包含至少一种阳离子表面活性成分的聚合物颗粒进料，并且其中活性成分 - 包含聚合物颗粒的方法可通过将烯键式不饱和单体M的单体组合物（其中烯键式不饱和单体M包含至少一种溶解形式的杀虫活性成分）进行自由基水性乳液聚合而获得。 本发明还涉及这种水性杀虫剂组合物用于保护木质纤维素材料，特别是木材，防止有害昆虫袭击的用途。