MEASURING METHOD AND DEVICE FOR TRACE AND ULTRA-TRACE OIL CONTENT

    公开(公告)号:US20240035938A1

    公开(公告)日:2024-02-01

    申请号:US18325098

    申请日:2023-05-29

    摘要: The present disclosure relates to a measuring method and device for trace and ultra-trace oil content. The measuring device of the present disclosure includes a cryogenic enriching device, an extracting device and an infrared spectrometer; The cryogenic enriching device includes a Dewar container and a U-shaped pipe; The extracting device includes an extractant container, an input pipe, an outlet pipe and an extraction liquid quantitative pipe; A mass flowmeter is further disposed on the U-shaped pipe, the oil content in the gas is calculated according to the measured total mass of the gas and the oil concentration of the extraction liquid measured by the infrared spectrometer. The present disclosure further provides a measuring method, which converts the measurement of oil content in gas into the measurement of oil concentration in liquid extractant through effective extraction by liquid nitrogen cold trap enrichment mode, and adopts infrared spectrophotometry to accurately measure.

    Cryogenic liquid medium
    2.
    发明授权

    公开(公告)号:US10696884B2

    公开(公告)日:2020-06-30

    申请号:US16368000

    申请日:2019-03-28

    摘要: The cryogenic liquid medium provided by the present invention includes at least one of an alkane composition, an olefin composition, an alcohol composition and an ether composition, and each of the alkane composition, the olefin composition, the alcohol combination and the ether composition includes a corresponding non-toxic and harmless substance having a melting point lower than −110° C. and a standard boiling point higher than 50° C. Since the cryogenic liquid medium is formed by the non-toxic and harmless single substance having the melting point lower than −110° C. and the standard boiling point higher than 50° C. or a binary, ternary and multi-component mixture thereof, the cryogenic liquid medium has a lower atmospheric boiling point, and is difficult to volatilize. The eutectic crystal of the specific mixture can be used to achieve the liquid requirements of low temperature, especially the temperature below −110° C.

    Cesium-rubidium-borate nonlinear optical crystal and its growth method and applications
    5.
    发明申请
    Cesium-rubidium-borate nonlinear optical crystal and its growth method and applications 有权
    铷硼酸盐非线性光学晶体及其生长方法及应用

    公开(公告)号:US20050286572A1

    公开(公告)日:2005-12-29

    申请号:US11159143

    申请日:2005-06-23

    IPC分类号: C30B29/22 G02F1/355 H01S3/10

    CPC分类号: G02F1/3551

    摘要: The present invention provides a cesium-rubidium-borate nonlinear optical crystal, which is represented by the chemical formula CsxRb1-xB3O5 (0

    摘要翻译: 本发明提供一种由铯 - 硼酸铷硼酸盐非线性光学晶体,其由化学式Cs> Rb Rb>>>>>>>>>>>>>>>>>>>>>>>> O 0(0 2 <1> 2 <1> 空间组 单位电池参数在以下范围内:a = 8.202-8.514Å,b = 10.075-9.140Å,c = 5.375-6.207Å和Z = 4。 晶体的制备方法如下:将铯盐,铷盐和含硼化合物按比例混合,加热,保持在温度下,然后冷却,得到硼酸铯 - 硼酸铷。 将铯 - 硼酸铷和助熔剂混合并加热以形成熔体以获得混合熔体。 然后将连接到种棒的晶种浸入混合熔体中,同时旋转种子棒。 将熔体保持在620-780℃,然后以0-5℃/天的速度缓慢冷却。 将所得晶体从熔体表面拉出并冷却至室温。 由此得到硼酸铷硼酸盐非线性光学晶体。 该晶体可用于激光波长转换,光参量放大,电光调制,光波导等。

    BARIUM TETRABORATE COMPOUND AND BARIUM TETRABORATE NON-LINEAR OPTICAL CRYSTAL, AND PREPARATION METHOD AND USE THEREOF
    8.
    发明申请
    BARIUM TETRABORATE COMPOUND AND BARIUM TETRABORATE NON-LINEAR OPTICAL CRYSTAL, AND PREPARATION METHOD AND USE THEREOF 有权
    四硼酸钡化合物和四硼酸钡非线性光学晶体及其制备方法及其用途

    公开(公告)号:US20160130723A1

    公开(公告)日:2016-05-12

    申请号:US14891936

    申请日:2014-01-23

    摘要: The present invention relates to a barium tetraborate compound and a barium tetraborate non-linear optical crystal, and a preparation method and use thereof, wherein the chemical formulae of the barium tetraborate compound and the non-linear optical crystal thereof are both BaB4O7, with a molecular weight of 292.58; the barium tetraborate non-linear optical crystal has a non-centrosymmetric structure, which belongs to a hexagonal system, and has a space group P65 and lattice parameters of a=6.7233(6) Å, c=18.776(4) Å, V=735.01(17) Å3, and Z=6, wherein the powder frequency-doubled effect thereof is two times that of KDP (KH2PO4), and the ultraviolet cut-off edge is lower than 170 nm. The barium tetraborate compound is synthesised by a solid-phase reaction method; the barium tetraborate non-linear optical crystal is grown by a high-temperature molten solution method; and the crystal has a moderate mechanical hardness, is easy to cut, polish and store, and is widely applicable in the non-linear optics of a double-frequency doubling generator, an upper frequency converter, a lower frequency converter or an optical parameter oscillator etc.

    摘要翻译: 本发明涉及四硼酸钡化合物和四硼酸钡非线性光学晶体及其制备方法和用途,其中四硼酸钡化合物及其非线性光学晶体的化学式均为BaB4O7,其中 分子量292.58; 四硼酸钡非线性光学晶体具有属于六方晶系的非中心对称结构,具有空间群P65和晶格参数a = 6.7233(6),c = 18.776(4),V = 735.01(17)Å3和Z = 6,其中粉末倍频效应是KDP(KH 2 PO 4)的两倍,紫外线截止边缘低于170nm。 四硼酸钡化合物通过固相反应法合成; 通过高温熔融溶液法生长四硼酸钡非线性光学晶体; 并且晶体具有中等的机械硬度,易于切割,抛光和存储,并且广泛应用于双倍频发生器,上变频器,下变频器或光参数振荡器的非线性光学器件 等等

    Optical coupling device having KBBF group crystal coupled with prisms and method for manufacturing same
    9.
    发明授权
    Optical coupling device having KBBF group crystal coupled with prisms and method for manufacturing same 有权
    具有与棱镜耦合的KBBF组晶体的光耦合器件及其制造方法

    公开(公告)号:US08773750B2

    公开(公告)日:2014-07-08

    申请号:US14115261

    申请日:2012-03-21

    IPC分类号: G02F1/355

    摘要: The present invention relates to a KBBF family nonlinear optical crystal-prism coupler and its method of fabrication. The coupler comprises: a KBBF family crystal with two smooth surfaces; transition layers each of which is deposited on respective one of the two smooth surfaces of the KBBF family crystal; and a pair of prisms each of which optically contacts with respective one of the activated transition layers. The present invention further provides a KBBF family nonlinear optical crystal-prism coupler that comprises: a KBBF family crystal with two smooth surfaces; a pair of prisms each of which has a smooth surfaces; first transition layers each of which is deposited on respective one of the two smooth surfaces of the KBBF family crystal; and second transition layers each of which is deposited on a smooth surface of respective one of the pair of prisms, wherein the first and second transition layers are integral by optical contact. The coupling between the KBBF family crystal and the prisms is achieved by optical contact through transition layers to improve bonding strength.

    摘要翻译: 本发明涉及KBBF系列非线性光学晶体 - 棱镜耦合器及其制造方法。 耦合器包括:具有两个光滑表面的KBBF系列晶体; 过渡层各自沉积在KBBF族晶体的两个平滑表面的相应一个上; 以及一对棱镜,每个棱镜与相应的一个激活的过渡层光学接触。 本发明还提供一种KBBF系列非线性光学晶体 - 棱镜耦合器,其包括:具有两个平滑表面的KBBF族晶体; 一对棱镜具有光滑的表面; 第一过渡层分别沉积在KBBF族晶体的两个光滑表面的相应一个上; 以及第二过渡层,每个过渡层沉积在该对棱镜中的相应一个棱镜的光滑表面上,其中第一和第二过渡层通过光学接触而成一体。 KBBF系列晶体与棱镜之间的耦合是通过过渡层的光学接触来实现的,以提高结合强度。