公开(公告)号：US09505620B2

公开(公告)日：2016-11-29

申请号：US14395442

申请日：2013-04-10

Applicant: ExxonMobil Upstream Research Company ,  Solid Carbon Products LLC

Inventor： Robert D. Denton ,  Dallas B. Noyes ,  Russell J. Koveal, Jr. ,  Terry A. Ring

IPC: C01B31/02 ,  D01F9/12 ,  D01F9/127 ,  B01J8/18

CPC classification number: C01B31/0226 ,  B01J8/1836 ,  B01J2208/00876 ,  C01B32/152 ,  C01B32/16 ,  D01F9/12 ,  D01F9/127 ,  Y02P20/129

Abstract: Methods and systems are provided for forming carbon allotropes. An exemplary method includes treating a carbonaceous compound to form a feedstock that includes at least about 10 mol % oxygen, at least about 10 mol % carbon, and at least about 20 mol % hydrogen. Carbon allotropes are formed from the feedstock in a reactor in a Bosch reaction at a temperature of at least about 500° C. The carbon allotropes are separated from a reactor effluent stream.

Abstract translation: 提供了形成碳同素异形体的方法和系统。 示例性的方法包括处理含碳化合物以形成包含至少约10mol％的氧，至少约10mol％的碳和至少约20mol％的氢的原料。 在博世反应中的反应器中，在至少约500℃的温度下，由原料形成碳同素异形体。将碳同素异形体与反应器流出物流分离。

公开(公告)号：US20160121290A1

公开(公告)日：2016-05-05

申请号：US14931403

申请日：2015-11-03

Applicant: Singh Instrument LLC

Inventor： Robbie Singh Sidhu

IPC: B01J8/10 ,  G01N31/10 ,  B01L3/00

CPC classification number: B01J8/10 ,  B01F11/0054 ,  B01J19/0066 ,  B01J2208/00814 ,  B01J2208/00858 ,  B01J2208/00876 ,  B01J2208/00911 ,  B01J2208/028 ,  B01J2219/00011 ,  B01J2219/00779 ,  G01N31/10

Abstract: a reactor for conducting laboratory reactions comprises includes reaction vessel, a catalyst holder in the reaction vessel, and a drive system configured to drive reciprocating linear movement of the catalyst basket. The catalyst holder can be configured to hold a plurality of catalyst particles so the catalyst particles remain spaced apart from one another. A reactor for conducting laboratory reactions can also include a reaction vessel, an impeller in the reaction vessel, and a drive system configured to drive reciprocating linear movement of the impeller.

Abstract translation: 用于进行实验室反应的反应器包括反应容器，反应容器中的催化剂保持器和构造成驱动催化剂篮的往复线性运动的驱动系统。 催化剂保持器可以构造成保持多个催化剂颗粒，使得催化剂颗粒保持彼此间隔开。 用于进行实验室反应的反应器还可以包括反应容器，反应容器中的叶轮和构造成驱动叶轮的往复线性运动的驱动系统。

公开(公告)号：US20150071848A1

公开(公告)日：2015-03-12

申请号：US14395434

申请日：2013-04-10

Applicant: ExxonMobil Upstream Research Company ,  Solid Carbon Products LLC

Inventor： Robert D. Denton ,  Dallas B. Noyes ,  Russell J. Koveal, JR. ,  Terry A. Ring

IPC: C01B31/02 ,  B01J8/18

CPC classification number: D01F9/12 ,  B01J8/1836 ,  B01J2208/00876 ,  C01B32/152 ,  C01B32/16 ,  D01F9/127 ,  Y02P20/129

Abstract: Methods and systems are provided for forming carbon allotropes. An exemplary method includes forming a feedstock that includes at least about 10 mol % oxygen, at least about 10 mol % carbon, and at least about 20 mol % hydrogen. Carbon allotropes are formed from the feedstock in a reactor in a Bosch reaction at a temperature of at least about 500° C., and the carbon allotropes are separated from a reactor effluent stream.

Abstract translation: 提供了形成碳同素异形体的方法和系统。 示例性的方法包括形成包含至少约10mol％的氧，至少约10mol％的碳和至少约20mol％的氢的原料。 在博世反应中的反应器中，在至少约500℃的温度下由原料形成碳同素异形体，并将碳同素异形体与反应器流出物流分离。

公开(公告)号：US08241492B1

公开(公告)日：2012-08-14

申请号：US13330716

申请日：2011-12-20

Applicant: Leon Yuan

Inventor： Leon Yuan

IPC: B01D15/08

CPC classification number: B01D15/1842 ,  B01J8/0214 ,  B01J8/0278 ,  B01J2208/00814 ,  B01J2208/00876 ,  G01N30/38 ,  G01N2030/386

Abstract: Disclosed herein is a simulated moving bed chromatography device comprises a minimum of one stationary pipe with a plurality of inlet/outlet channels, a rotary device next to the stationary pipes, a stationary radial flow segmented vessel communicates with the rotary device, a fluid moving device and a drive means to rotate the rotary device. The counter movement of the stationary phase and the fluid is simulated by rotating the rotary device in the same direction as the circulating fluid flow, and the fluid flows through the flow distribution segments, the stationary phase segments, the outer fluid transfer segments, holes or by passes of the improved partition plates in the flow distribution segments/compartments and outer fluid transfer segments.

Abstract translation: 本文公开了一种模拟移动床层析装置，其包括具有多个入口/出口通道的至少一个固定管，邻近固定管的旋转装置，固定径向流分段容器与旋转装置连通，流体移动装置 以及用于旋转旋转装置的驱动装置。 通过沿与循环流体流相同的方向旋转旋转装置来模拟固定相和流体的相对运动，并且流体流过流量分配段，固定相段，外部流体传递段，孔或 通过流量分配段/隔室中的改进的隔板和外部流体转移段。

公开(公告)号：US20100329949A1

公开(公告)日：2010-12-30

申请号：US12790941

申请日：2010-05-31

Applicant: Leon Yuan

Inventor： Leon Yuan

IPC: B01J19/00 ,  B01J38/00

CPC classification number: B01J8/0214 ,  B01D53/0431 ,  B01D53/0462 ,  B01D53/047 ,  B01D53/06 ,  B01J8/0278 ,  B01J2208/00814 ,  B01J2208/00876

Abstract: This specification discloses a radial flow continuous reaction/regeneration apparatus. Through employing a rotary device to individually and annularly distributing process fluid and regeneration fluid into a stationary segmented reaction/regeneration box and receiving effluents individually and annularly from the same stationary reaction/regeneration box, the mentioned radial flow continuous reaction/regeneration apparatus can be operated continuously and efficiently without the need for shutting down for regeneration. This radial flow continuous reaction/regeneration apparatus is not only used to separate components by adsorption, such as dehumidification, but also is used in chemical processes to carry out catalytic reaction, regenerate catalyst and used as filtration device to trap particles by changing the filler in the stationary reaction/regeneration box.

Abstract translation: 本说明书公开了径向流动连续反应/再生装置。 通过采用旋转装置将过程流体和再生流体单独地和环形地分配到静止分段的反应/再生箱中并且从相同的固定反应/再生箱单独地和环形地接收流出物，所述径向流动连续反应/再生装置可以被操作 连续而有效地进行，不需要关闭再生。 这种径向流动连续反应/再生装置不仅用于通过除湿等吸附分离组分，而且还用于化学过程中进行催化反应，再生催化剂并用作过滤装置以通过改变填料来捕获颗粒 静止反应/再生箱。

公开(公告)号：US07642365B2

公开(公告)日：2010-01-05

申请号：US11890183

申请日：2007-08-03

Applicant: Prakash G. Balan

Inventor： Prakash G. Balan

IPC: C07D301/06 ,  B01J8/02

CPC classification number: B01J23/38 ,  B01D29/018 ,  B01D29/58 ,  B01J8/009 ,  B01J8/0257 ,  B01J29/89 ,  B01J2208/00814 ,  B01J2208/00849 ,  B01J2208/00876 ,  B01J2208/00884 ,  B01J2229/186 ,  B01J2229/42 ,  Y02P20/582

Abstract: A unique reactor configuration especially suitable for interphase mass transfer and mixing of multiple phases, i.e. gas(es), liquid(s), and solid(s) where reaction is catalyzed by a solid catalyst comprises a draught tube reactor wherein the solid catalyst particles are maintained in an annular space between the draught tube of the reactor and an annulus-defining wall by means of filter elements positioned downstream and optionally also upstream from the catalyst bed.

Abstract translation: 特别适用于反应由固体催化剂催化的多相（即气体，液体和固体）的相间传质和混合的独特的反应器构型包括引流管反应器，其中固体催化剂颗粒 通过位于下游和任选地也位于催化剂床上游的过滤元件保持在反应器的引流管和环形壁之间的环形空间中。

公开(公告)号：US20040179983A1

公开(公告)日：2004-09-16

申请号：US10385180

申请日：2003-03-10

Inventor： Prakash G. Balan

IPC: B01F007/00 ,  B01F007/16

CPC classification number: B01J23/38 ,  B01D29/018 ,  B01D29/58 ,  B01J8/009 ,  B01J8/0257 ,  B01J29/89 ,  B01J2208/00814 ,  B01J2208/00849 ,  B01J2208/00876 ,  B01J2208/00884 ,  B01J2229/186 ,  B01J2229/42 ,  Y02P20/582

Abstract: A unique reactor configuration especially suitable for interphase mass transfer and mixing of multiple phases, i.e. gas(es), liquid(s), and solid(s) where reaction is catalyzed by a solid catalyst comprises a draught tube reactor wherein the solid catalyst particles are maintained in an annular space between the draught tube of the reactor and an annulus-defining wall by means of filter elements positioned downstream and optionally also upstream from the catalyst bed.

Abstract translation: 特别适用于反应由固体催化剂催化的多相（即气体，液体和固体）的相间传质和混合的独特的反应器构型包括引流管反应器，其中固体催化剂颗粒 通过位于下游和任选地也位于催化剂床上游的过滤元件保持在反应器的引流管和环形壁之间的环形空间中。

公开(公告)号：US20040116626A1

公开(公告)日：2004-06-17

申请号：US10662249

申请日：2003-09-15

Inventor： David H. Burns ,  Donald W. Verser

IPC: C08F002/00

CPC classification number: C08F6/003 ,  B01J8/0015 ,  B01J8/222 ,  B01J19/1837 ,  B01J2208/00176 ,  B01J2208/00212 ,  B01J2208/00274 ,  B01J2208/00876 ,  B01J2219/00006 ,  B01J2219/00094 ,  B01J2219/00191 ,  B01J2219/00252 ,  B01J2219/182 ,  B01J2219/185 ,  C08F10/02 ,  C08F110/02 ,  C08F210/16 ,  C08L23/00 ,  C08F2/01 ,  C08F210/14

Abstract: A recycling and recovery system and process comprising a flash gas separator that receives a slurry comprising liquid medium and solid polymer particles. The flash gas separator separates the diluent from the solid polymer particles as a vapor stream comprising at least diluent and heavies. A line receives the vapor stream from the flash gas separator. The line leads to a heavies removal system that yields a liquid that is relatively concentrated in heavies and a diluent vapor that is relatively free of heavies. The liquid is passed to a heavies column, while the diluent vapor is passed to a diluent recycle chamber and then recycled to a slurry polymerization reactor without additional treatment to remove heavies.

Abstract translation: 回收和回收系统和方法，其包括接收包含液体介质和固体聚合物颗粒的浆料的闪蒸气分离器。 闪蒸气分离器将稀释剂与固体聚合物颗粒分离，作为至少包含稀释剂和重质物的蒸气流。 线路接收来自闪蒸气体分离器的蒸汽流。 该线通向重质的除去系统，其产生相对集中在重质物中的液体和相对不含重质的稀释剂蒸汽。 将液体通入重质柱，同时将稀释剂蒸气通入稀释剂再循环室，然后再循环至淤浆聚合反应器，无需另外处理以除去重质物。

公开(公告)号：US20040083028A1

公开(公告)日：2004-04-29

申请号：US10281624

申请日：2002-10-28

Inventor： Ramaswamy Vaidyanathan ,  Ronald S. Hurlbut ,  William D. Stephens ,  David R. Van Hare

IPC: G05B021/00

CPC classification number: B01J19/0006 ,  B01J8/10 ,  B01J8/36 ,  B01J19/0033 ,  B01J2208/00168 ,  B01J2208/00274 ,  B01J2208/00362 ,  B01J2208/00876 ,  B01J2219/00006 ,  B01J2219/002 ,  B01J2219/00209 ,  B01J2219/00229 ,  B01J2219/182 ,  B01J2219/185 ,  Y10T436/24

Abstract: A method for providing improved estimates of properties of a chemical manufacturing process is disclosed. The method employs a process model that includes, or is modified by, scores or other gains obtained from the mathematical transformation of data obtained from an on-line analyzer. Chemical manufacturing processes using the method also are disclosed.

Abstract translation: 公开了一种用于提供改进的化学制造工艺性能估计的方法。 该方法采用由从在线分析器获得的数据的数学变换获得的评分或其他增益包括或修改的过程模型。 使用该方法的化学制造方法也被公开。

公开(公告)号：US5102628A

公开(公告)日：1992-04-07

申请号：US196288

申请日：1988-05-20

Applicant: Hugo I. De Lasa

Inventor： Hugo I. De Lasa

IPC: B01J8/24 ,  G01N31/10

CPC classification number: G01N31/10 ,  B01J8/24 ,  B01J2208/00407 ,  B01J2208/00522 ,  B01J2208/00876 ,  B01J2208/00884

Abstract: An apparatus for testing performance of a catalyst in a gaseous phase catalytic reaction for a given reactant comprises a reactor receiving a predetermined quantity of fluid reactant discharging the reaction mixture, including reaction products, from the reactor after a predetermined residence time. The reactor comprises a confined reactor volume with an upflow zone and a downflow zone. A device circulates fluids upwardly through the upflow zone and downwardly through the downflow zone where particulate catalysts in the upflow zone are fluidized by the upward flow of the fluid. The circulating device is adapted to circulate the fluid about the reactor volume at a rate which provides at any moment during the residence time for the reactants an essentially uniform concentration of reactants throughout the reactor volume to simulate conditions in a catalytic riser reactor.

Abstract translation: 用于测试给定反应物的气相催化反应中的催化剂性能的装置包括在预定的停留时间之后从反应器接收预定量的流体反应物的反应器，该反应器从反应器排出包括反应产物。 反应器包括具有上流区和下流区的约束反应器体积。 装置将液体向上循环通过上流区并向下通过下流区，其中上流区中的颗粒催化剂被流体的向上流动流化。 循环装置适于以围绕反应器体积的流体循环流体，该速率在反应物的停留时间的任何时刻提供整个反应器体积中的基本均匀浓度的反应物，以模拟催化提升管反应器中的条件。