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公开(公告)号:US20240351889A1
公开(公告)日:2024-10-24
申请号:US18684228
申请日:2022-08-10
申请人: MERCK PATENT GMBH
发明人: Eric JACQUINOT , Leo HANUS , Geary GRAHAM
IPC分类号: C01B33/158 , C01B33/141 , C01B33/152
CPC分类号: C01B33/158 , C01B33/1415 , C01B33/152 , C01P2006/80
摘要: The present application relates to a method for producing silica particles, and to the silica particles produced by such method. The present application further relates to compositions comprising the silica particles produced by such method as well as to uses of such silica particles and compositions comprising such silica particles.
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公开(公告)号:US11691885B2
公开(公告)日:2023-07-04
申请号:US16644583
申请日:2018-09-05
发明人: Kazui Omokawa , Hirokazu Yokota , Kenichi Takeuchi , Yuma Negishi , Tomoko Kiseki , Munenori Komoto
IPC分类号: C01B33/159 , C01B33/152 , G03G9/097
CPC分类号: C01B33/159 , C01B33/152 , G03G9/09725 , C01P2002/86 , C01P2006/82
摘要: Provided is a hydrophobic silica powder that can be obtained by the sol-gel process, and that is excellent in charge properties. The hydrophobic silica powder has a hydrophobicity of 50% or more, a saturated water content of 4% or less, and a nitrogen content of 0.05% or more.
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公开(公告)号:US20180179075A1
公开(公告)日:2018-06-28
申请号:US15738516
申请日:2017-02-07
申请人: LG CHEM, LTD.
发明人: Ye Hon KIM , Je Kyun LEE , Kyoung Shil OH
IPC分类号: C01B33/158 , C01B33/145 , C01B33/155 , B05C5/02 , B05C9/12 , B05C11/02 , B05D1/26 , B05D3/02
CPC分类号: C01B33/1585 , B05C5/0245 , B05C9/12 , B05C11/028 , B05D1/26 , B05D3/0254 , B65H35/06 , B65H37/00 , C01B33/14 , C01B33/145 , C01B33/152 , C01B33/155 , C01P2006/32
摘要: The present invention relates to a method for manufacturing an aerogel sheet and comprises: a step (a) of preparing silica sol and a surface modifying agent to prepare a silica precursor; a step (b) of preparing a gelling catalyst; a step (c) of injecting the silica precursor prepared in the step (a) to a surface of a blanket to impregnate the silica precursor; and a step (d) of injecting the gelling catalyst prepared in the step (b) to the surface of the blanket in which the silica precursor is impregnated to gelate the silica precursor.
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公开(公告)号:US20180044188A1
公开(公告)日:2018-02-15
申请号:US15552443
申请日:2016-04-21
申请人: Wacker Chemie AG
IPC分类号: C01B33/158 , C01B33/155 , C01B33/152
CPC分类号: C01B33/1585 , C01B33/152 , C01B33/155
摘要: The invention relates to a method for producing organically modified aerogels. The problem addressed by the invention is that of providing an economical method for producing hydrophobic aerogels which can be implemented cost-effectively, simply, and safely, and which operates to save on resources. This problem is solved by the provision of a method for producing organically modified aerogels, wherein a sol containing [SiO4,2] units is produced, and the sol obtained is dispersed in a continuous phase. The sol forms a separate phase and the continuous phase contains at least 20 wt % organosiloxane, a gel is formed from the sol in the continuous phase, and the gel obtained is surface-modified in the presence of a phase mediator in the continuous phase, wherein acids or chlorosilanes or mixtures thereof are added as initiator and the gels obtained are dried. The aerogels provided can be used as insulating materials, in particular in thermal insulation.
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公开(公告)号:US4576921A
公开(公告)日:1986-03-18
申请号:US522695
申请日:1983-08-12
申请人: Edward S. Lane
发明人: Edward S. Lane
CPC分类号: C01G19/02 , B01J13/0034 , B01J13/0047 , C01B33/152 , C03C1/008
摘要: The present invention relates to the preparation of materials and finds application in the preparation of dispersions and gels.The invention provides, in one aspect, a process for the preparation of a dispersion which comprises treating a chemical compound with a quaternary ammonium hydroxide so as to peptize the chemical compound to form a dispersion.The dispersion may be, for example, a suspension or a sol (i.e. a colloidal solution). The chemical compound may be, for example, a hydrous metal oxide (e.g. hydrous stannic oxide).Mixed dispersions may be formed in accordance with the present invention.
摘要翻译: 本发明涉及材料的制备和应用于分散体和凝胶的制备。 本发明一方面提供一种制备分散体的方法,该方法包括用氢氧化季铵处理化合物,以使该化合物胶溶以形成分散体。 分散体可以是例如悬浮液或溶胶(即胶体溶液)。 化合物可以是例如含水金属氧化物(例如,含水锡氧化物)。 可以根据本发明形成混合分散体。
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公开(公告)号:US1539342A
公开(公告)日:1925-05-26
申请号:US67949923
申请日:1923-12-08
申请人: NAT BENZOLE ASS
发明人: WILLIAMS EVAN C
IPC分类号: C01B33/152
CPC分类号: C01B33/152
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公开(公告)号:US20230348285A1
公开(公告)日:2023-11-02
申请号:US17922203
申请日:2021-04-20
发明人: Uwe NUMRICH , Stefan BADE , Nicolas MARION , Matthias KOEBEL , Wim MALFAIT , Stefanie HAUSER , Nicolas VOGEL
IPC分类号: C01B33/158 , C01B33/159 , C01B33/152
CPC分类号: C01B33/1585 , C01B33/159 , C01B33/152
摘要: The present invention relates to a process for producing a hydrophobized silica aerogel, comprising the following steps: a) preparing a hydrophobized silica gel comprising alkoxy groups; b) drying of the hydrophobized silica gel obtained in step a); c) treatment of the product obtained in step b) with a gas mixture comprising water and a base or an acid. A hydrophobized silica aerogel with a reduced alkoxy group content, suitable for thermal insulation applications, is also provided.
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公开(公告)号:US09969867B2
公开(公告)日:2018-05-15
申请号:US14785739
申请日:2014-05-14
IPC分类号: C08G59/18 , C08L63/00 , C08K3/36 , C08K9/06 , C01B33/14 , C01B33/141 , C01B33/142 , C01B33/143 , C01B33/146 , C01B33/149 , C01B33/12 , C01B33/148 , C01B33/152
CPC分类号: C08K9/06 , C01B33/128 , C01B33/142 , C01B33/146 , C01B33/148 , C01B33/152 , C08K3/36 , C08L63/00
摘要: The silica sol of the invention contains silica particles having a mean primary particle size of 20 to 100 nm and which has a silica particle size/mean primary particle size ratio, determined through dynamic light scattering, of 3.0 or less, wherein the silica particles are surface-treated with an organic silane compound and have an α-ray emission rate of 0.005 counts/cm2·hr or less and a moisture absorption coefficient, determined after allowing the silica particles to stand for 48 hours at 23° C. and a relative humidity of 50 RH %, of 0.5 mass % or lower.
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公开(公告)号:US20090074655A1
公开(公告)日:2009-03-19
申请号:US12085974
申请日:2006-12-01
申请人: Crina Silvia Suciu
发明人: Crina Silvia Suciu
IPC分类号: C01G25/02 , C01B33/141 , B01J13/00
CPC分类号: C01B13/32 , B82Y30/00 , C01B33/152 , C01G1/02 , C01G17/02 , C01G25/02 , C01G27/02 , C01G35/00 , C01G53/04 , C01P2002/60 , C01P2002/72 , C01P2002/88 , C01P2004/04 , C01P2004/64 , C01P2006/12
摘要: Methods of sol-gel processing for preparing of gels and nanoparticles are described. The invention also relates to gels and nanoparticles prepared by the described methods. A preferable embodiment describes ZrO2 nanoparticles produced by sol gel processing by using sucrose and pectin as polymerization agents.
摘要翻译: 描述了制备凝胶和纳米颗粒的溶胶 - 凝胶加工方法。 本发明还涉及通过所述方法制备的凝胶和纳米颗粒。 优选的实施方案描述了通过使用蔗糖和果胶作为聚合剂通过溶胶凝胶加工制备的ZrO 2纳米颗粒。
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公开(公告)号:US5158758A
公开(公告)日:1992-10-27
申请号:US342547
申请日:1989-04-24
IPC分类号: B01J20/10 , B01J20/283 , B01J20/287 , C01B33/152
CPC分类号: B01J20/287 , B01J20/103 , B01J20/283 , C01B33/152
摘要: A method for production of high specific surface area silica gel by hydrolysis of silicon tetrahalide, wherein a solution of silicon tetrahalide in a non-reactive solvent such as alcohol is mixed with water to produce silica gel having a high surface area and narrow pore diameter distribution especially suited for use as normal phase packing material in high performance chromatography columns. The water contains fluoride ions if the halide is chloride. Reverse phase packing material can be prepared by reacting the normal phase silica gel with organochlorosilanes to prepare bonded reverse phase material for use in high performance liquid chromotagraphy systems.
摘要翻译: 一种通过水解四卤化硅生产高比表面积硅胶的方法,其中将四卤化硅在无反应性溶剂如醇中的溶液与水混合,生产具有高表面积和窄孔径分布的硅胶 特别适用于高性能色谱柱中的正相填充材料。 如果卤化物是氯化物,水就含有氟离子。 反相包装材料可以通过正相硅胶与有机氯硅烷反应制备用于高性能液体色谱系统的粘结反相材料。
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