Method for particle size distribution control in a bayer circuit decomposition chain, comprising an agglomeration phase
    6.
    发明授权
    Method for particle size distribution control in a bayer circuit decomposition chain, comprising an agglomeration phase 失效
    在拜尔电路分解链中的粒度分布控制方法,包括凝聚相

    公开(公告)号:US06878357B1

    公开(公告)日:2005-04-12

    申请号:US09744237

    申请日:1999-08-12

    申请人: Benoit Cristol

    发明人: Benoit Cristol

    IPC分类号: C01F7/14 C01F7/00

    摘要: In a BAYER circuit, a process for controlling precipitation in which particle size quality of alumina hydrate produced in the circuit and circulating in feed tanks is monitored utilizing a calibration step and a control step. In the calibration step, cumulative percentage of alumina hydrate particles circulating in the feed tanks in the circuit that are finer than X2 μm, defined as CPFT X2, is measured vs. time and cumulative percentage of alumina hydrate particles circulating in the feed tanks in the circuit that are finer that X1 μm, defined as CPFT X1 vs. time, is measured, where X1 and X2 are predetermined particles sizes and X1 is smaller than X2. A relationship R between CPFT X1 and later changes in CPFT X2, is determined and upper and lower trigger thresholds of CPFT X1 which correspond to maximum permissible variation in CPFT X2 are defined. In the control step, CPFT X1 and CPFT X2 are regularly measured, and R and the correlation between CPFT X2 and the particle size of hydrate produced are updated. Corrective action is taken at the beginning of precipitation when the measured value of CPFT X1 reaches one of the trigger thresholds.

    摘要翻译: 在BAYER电路中,使用校准步骤和控制步骤来监测用于控制沉淀的方法,其中在电路中产生的水合氧化铝的粒度质量和在进料罐中循环。 在校准步骤中,测定在循环中进料池中循环的氧化铝水合物颗粒的累积百分比,其比X2妈妈定义为CPFT X2,相对于在进料罐中循环的水合氧化铝颗粒的时间和累积百分比 测量X1 mum,定义为CPFT X1与时间相比更精细的电路,其中X1和X2是预定的粒径,X1小于X2。 确定CPFT X1与CPFT X2之间的更改之间的关系R,并且定义与CPFT X2中的最大允许变化对应的CPFT X1的上下触发阈值。 在控制步骤中,定期测量CPFT X1和CPFT X2,并更新R和CPFT X2与产生的水合物粒径之间的相关性。 当CPFT X1的测量值达到触发阈值之一时,在降水开始时采取纠正措施。

    Small sized alpha alumina particles and platelets
    7.
    发明授权
    Small sized alpha alumina particles and platelets 失效
    小尺寸的α氧化铝颗粒和血小板

    公开(公告)号:US5149520A

    公开(公告)日:1992-09-22

    申请号:US460844

    申请日:1990-01-31

    IPC分类号: C01F7/14 C01F7/44

    摘要: A process for producing alpha alumina particles includes steps of precipitating alumina hydrate from an aqueous sodium aluminate solution by treatment with alumina hydrate seed material and alpha alumina promoter particles; and calcining the precipitated alumina hydrate in the presence of a mineralizer. A preferred mineralizer is aluminum fluoride. The process produces alpha alumina particles having a plate-like shape and an average size of less than about 1.5 microns.

    摘要翻译: PCT No.PCT / US89 / 02659 Sec。 371日期1990年1月31日第 102(e)日期1990年1月31日PCT 1989年6月19日PCT。一种生产α氧化铝颗粒的方法包括通过用氧化铝水合物种子材料和α氧化铝促进剂颗粒处理从铝酸钠水溶液中沉淀氧化铝水合物的步骤; 并在矿化剂存在下煅烧沉淀的氧化铝水合物。 优选的矿化剂是氟化铝。 该方法产生具有板状形状和平均尺寸小于约1.5微米的α氧化铝颗粒。

    Economical process for alpha alumina production
    10.
    发明授权
    Economical process for alpha alumina production 失效
    α氧化铝生产的经济工艺

    公开(公告)号:US4847064A

    公开(公告)日:1989-07-11

    申请号:US137159

    申请日:1987-12-23

    申请人: Alan Pearson

    发明人: Alan Pearson

    摘要: A process for making alpha alumina particles wherein a Bayer process caustic aluminate solution is treated with both alumina hydrate seed material and alpha alumina promoter particles to precipitate alumina hydrate particles. The precipitated particles are separated from the solution and then dried and calcined to produced alpha alumina particles. Addition of promoter particles in the precipitation step lowers the calcination temperture necessary to produce alpha alumina and results in smaller sized crystallites in the product.

    摘要翻译: 制备α氧化铝颗粒的方法,其中用氧化铝水合物种子材料和α氧化铝促进剂颗粒处理拜耳法苛性铝酸盐溶液以沉淀氧化铝水合物颗粒。 将沉淀的颗粒与溶液分离,然后干燥并煅烧以产生α氧化铝颗粒。 在沉淀步骤中加入助催化剂颗粒降低产生α氧化铝所需的煅烧温度,并在产品中产生较小尺寸的微晶。