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    Polymer membranes
    1.
    发明授权
    Polymer membranes 有权
    聚合物膜

    公开(公告)号：US08168705B2

    公开(公告)日：2012-05-01

    申请号：US12850530

    申请日：2010-08-04

    申请人： Jochen Kerres

    发明人： Jochen Kerres

    IPC分类号： C08K5/41

    CPC分类号： B01D67/0093 ,  B01D67/0011 ,  B01D67/0048 ,  B01D69/141 ,  B01D71/00 ,  B01D71/52 ,  B01D71/68 ,  B01D71/80 ,  B01D71/82 ,  B01D2323/08 ,  B01D2323/12 ,  B01D2323/26 ,  C08J5/2275 ,  C08J2379/06 ,  C25B13/04 ,  H01M8/1025 ,  H01M8/1027 ,  H01M8/103 ,  H01M8/1032 ,  H01M8/1041 ,  H01M8/1048 ,  H01M8/1074 ,  H01M8/1081 ,  H01M8/1088 ,  Y02P70/56

    摘要： The invention relates to novel organic/inorganic hybrid membranes which have the following composition: a polymer acid containing —SO3H, PO3H2, —COOH or B(OH)2 groups, a polymeric ease (optional), which contains primary, secondary or tertiary amino groups, pyridine groups, imidazole, benzimidazole, triazole, benzotriazole, pyrazole or benzopyrazole groups, either in the side chain or in the main chain; an additional polymeric base (optional) containing the aforementioned basic groups; an element or metal oxide or hydroxide, which has been obtained by hydrolysis and/or sol-gel reaction of an elementalorganic and/or metalorganic compound during the membrane forming process and/or by a re-treatment of the membrane in aqueous acidic, alkaline or neutral electrolytes. The invention also relates to methods for producing said membranes and to various uses for membranes of this type.

    摘要翻译： 本发明涉及具有以下组成的新型有机/无机杂化膜：含有-SO 3 H，PO 3 H 2，-COOH或B（OH）2基团的聚合酸，聚合物易于（任选的），其含有伯，仲或叔氨基 基团，吡啶基，咪唑，苯并咪唑，三唑，苯并三唑，吡唑或苯并吡唑基团，在侧链或主链中; 含有上述碱性基团的另外的聚合物基（任选的） 通过元素或金属氧化物或氢氧化物，其通过在成膜过程中元素有机和/或金属有机化合物的水解和/或溶胶 - 凝胶反应和/或通过在酸性，碱性水溶液中再次处理而获得 或中性电解质。 本发明还涉及生产所述膜的方法和用于这种类型的膜的各种用途。

    Solid state proton conductor system derived from hybrid composite inorganic-organic multicomponent material
    3.
    发明授权
    Solid state proton conductor system derived from hybrid composite inorganic-organic multicomponent material 有权
    衍生自混合复合无机 - 有机多组分材料的固态质子导体系统

    公开(公告)号：US07563828B2

    公开(公告)日：2009-07-21

    申请号：US10892979

    申请日：2004-07-16

    申请人： Ralph Taylor-Smith

    发明人： Ralph Taylor-Smith

    IPC分类号： B01J41/12 ,  H01M4/86

    CPC分类号： C08G77/04 ,  C08J5/2256 ,  C08J2383/04 ,  C08K3/08 ,  H01M8/1037 ,  H01M8/1039 ,  H01M8/1044 ,  H01M8/1048 ,  H01M8/1074 ,  H01M2300/0082 ,  H01M2300/0091 ,  Y02P70/56

    摘要： A polysesquioxane composition, comprising (i) a polysesquioxane matrix comprising sesquioxane moieties comprising a metallic element; (ii) a hydrophilic component; and (iii) a proton-conducting component, is provided. The metallic element can be silicon, aluminum, titanium, zirconium, germanium, or a mixture of two or more thereof. The hydrophilic component can comprise an imidazole moiety, a pyrazole moiety, a benzimidazole moiety, a silanol moiety, a cyclodextrin, or two or more thereof, and the hydrophilic component can be covalently bonded to the polysesquioxane matrix. The proton-conducting component can comprise an inorganic Brønsted acid moiety. The polysesquioxane composition can be used as a proton exchange membrane in a fuel cell; as a component of a membrane electrode assembly; or as a sensor assembly in a potentiometric sensor.

    摘要翻译： 一种聚倍半硅氧烷组合物，其包含（i）包含倍半硅氧烷部分的聚倍半硅氧烷基体，其包含金属元素; （ii）亲水组分; 和（iii）质子传导组分。 金属元素可以是硅，铝，钛，锆，锗或其两种或更多种的混合物。 亲水性组分可以包含咪唑部分，吡唑部分，苯并咪唑部分，硅烷醇部分，环糊精或其两种或更多种，并且亲水性组分可以共价键合到聚倍半硅氧烷基质上。 质子传导组分可以包含无机布朗斯台德酸部分。 聚倍半硅氧烷组合物可以用作燃料电池中的质子交换膜; 作为膜电极组件的组件; 或作为电位传感器中的传感器组件。

    Polymer Membranes
    4.
    发明申请
    Polymer Membranes 审中-公开
    聚合物膜

    公开(公告)号：US20080318134A1

    公开(公告)日：2008-12-25

    申请号：US12102776

    申请日：2008-04-14

    申请人： Jochen Kerres

    发明人： Jochen Kerres

    IPC分类号： H01M10/04 ,  B01D61/00 ,  B01D67/00 ,  B01D71/00 ,  C08J5/22

    CPC分类号： B01D67/0093 ,  B01D67/0011 ,  B01D67/0048 ,  B01D69/141 ,  B01D71/00 ,  B01D71/52 ,  B01D71/68 ,  B01D71/80 ,  B01D71/82 ,  B01D2323/08 ,  B01D2323/12 ,  B01D2323/26 ,  C08J5/2275 ,  C08J2379/06 ,  C25B13/04 ,  H01M8/1025 ,  H01M8/1027 ,  H01M8/103 ,  H01M8/1032 ,  H01M8/1041 ,  H01M8/1048 ,  H01M8/1074 ,  H01M8/1081 ,  H01M8/1088 ,  Y02P70/56

    摘要： The invention relates to novel organic/inorganic hybrid membranes which have the following composition: a polymer acid containing —SO3H, —PO3H2, —COOH or B(OH)2 groups, a polymeric base (optional), which contains primary, secondary or tertiary amino groups, pyridine groups, imidazole, benzimidazole, triazole, benzotriazole, pyrazole or benzopyrazole groups, either in the side chain or in the main chain; an additional polymeric base (optional) containing the aforementioned basic groups; an element or metal oxide or hydroxide, which has been obtained by hydrolysis and/or sol-gel reaction of an elementalorganic and/or metalorganic compound during the membrane forming process and/or by a re-treatment of the membrane in aqueous acidic, alkaline or neutral electrolytes. The invention also relates to methods for producing said membranes and to various uses for membranes of this type.

    摘要翻译： 本发明涉及具有以下组成的新型有机/无机杂化膜：含有-SO 3 H，-PO 3 H 2，-COOH或B（OH）2基团的聚合酸，聚合碱（任选的），其含有伯，仲或叔 氨基，吡啶基，咪唑，苯并咪唑，三唑，苯并三唑，吡唑或苯并吡唑基团，在侧链或主链中; 含有上述碱性基团的另外的聚合物基（任选的） 通过元素或金属氧化物或氢氧化物，其通过在成膜过程中元素有机和/或金属有机化合物的水解和/或溶胶 - 凝胶反应和/或通过在酸性，碱性水溶液中再次处理而获得 或中性电解质。 本发明还涉及生产所述膜的方法和用于这种类型的膜的各种用途。

    Proton conducting membrane, method for producing the same, and fuel cell using the same
    5.
    发明申请
    Proton conducting membrane, method for producing the same, and fuel cell using the same 审中-公开
    质子导电膜及其制造方法以及使用其的燃料电池

    公开(公告)号：US20070213495A1

    公开(公告)日：2007-09-13

    申请号：US11727036

    申请日：2007-03-23

    申请人： Shigeki Nomura ,  Toshiya Sugimoto ,  Masanori Nakamura ,  Kenji Yamauchi

    发明人： Shigeki Nomura ,  Toshiya Sugimoto ,  Masanori Nakamura ,  Kenji Yamauchi

    IPC分类号： C08G77/04

    CPC分类号： C08G77/28 ,  C08G77/50 ,  C08J5/2275 ,  C08J2383/06 ,  H01B1/122 ,  H01M4/8605 ,  H01M8/1037 ,  H01M8/1051 ,  H01M8/1074 ,  H01M2300/0082 ,  H01M2300/0091 ,  Y02P70/56 ,  Y10T442/2467

    摘要： The present invention provides relates to a crosslinkable, proton-conducting membrane having a crosslinked structure, excellent in heat resistance, durability, dimensional stability and fuel barrier characteristics, and showing excellent proton conductivity at high temperature, characterized by comprising (a) an organic/inorganic hybrid structure (A) covalently bonded to 2 or more silicon-oxygen crosslinks and, at the same time, having a carbon atom, and (b) an acid containing structure (B) having an acid group, covalently bonded to a silicon-oxygen crosslink and having an acidic group; and provides a fuel cell using the same membrane. The present invention also provides a method for producing the proton-conducting membrane, comprising steps of preparing a mixture containing an organic/inorganic hybrid, crosslinkable compound (C) and compound (D), the former having 2 or more crosslinkable silyl groups and carbon atoms each being bonded to the silyl group via the covalent bond and the latter having a crosslinkable silyl group and acid group, as the first step; forming the above mixture into a film as the second step; and hydrolyzing/condensing or only condensing the hydrolyzable silyl group contained in the mixture formed into the film to form a crosslinked structure as the third step.

    摘要翻译： 本发明涉及具有交联结构，耐热性，耐久性，尺寸稳定性和燃料阻隔特性优异的交联性质子传导膜，并且在高温下显示出优异的质子传导性，其特征在于包括（a）有机/ 共价结合到2个以上的硅 - 氧交联基团，同时具有碳原子的无机杂化结构（A），和（b）具有酸基的含酸结构体（B），共价键合到硅 - 氧交联并具有酸性基团; 并提供使用相同膜的燃料电池。 本发明还提供一种生产质子传导膜的方法，包括以下步骤：制备含有有机/无机杂化物，可交联化合物（C）和化合物（D）的混合物，前者具有2个或更多个可交联甲硅烷基和碳 作为第一步，各自通过共价键与甲硅烷基键合的原子，后者具有交联性甲硅烷基和酸基; 将上述混合物形成为第二步骤的膜; 并将形成的混合物中所含的可水解甲硅烷基水解/缩合或缩合形成第三步的交联结构。

    Method for producing a membrane for a fuel cell
    6.
    发明申请
    Method for producing a membrane for a fuel cell 失效
    燃料电池用膜的制造方法

    公开(公告)号：US20060194089A1

    公开(公告)日：2006-08-31

    申请号：US11351697

    申请日：2006-02-10

    申请人： Hubertus Biegert ,  Peter Britz ,  Gabor Toth ,  Peter Urban

    发明人： Hubertus Biegert ,  Peter Britz ,  Gabor Toth ,  Peter Urban

    IPC分类号： H01M8/10 ,  C08J5/22

    CPC分类号： C08J5/2218 ,  H01M8/1023 ,  H01M8/1037 ,  H01M8/1039 ,  H01M8/1044 ,  H01M8/1074 ,  Y02P70/56 ,  Y10T29/49115

    摘要： The invention relates to an ion-conductive polymer membrane for a fuel cell, whereby the polymer membrane is configured from a polymer-forming hydrocarbon material and to a method for producing the same. The membrane also has a metal-containing gel which has been hydrolysed and/or condensed from a metal alkoxide starting material and which is deposited in the polymer and/or is chemically bonded to the polymer. The proportion of metal alkoxide by weight, in relation to the membrane, lies between 25% and 1%.

    摘要翻译： 本发明涉及一种用于燃料电池的离子导电聚合物膜，其中聚合物膜由形成聚合物的烃材料构成，并且涉及其制造方法。 膜还具有已经从金属醇盐起始材料水解和/或冷凝并且沉积在聚合物中和/或化学键合到聚合物上的含金属凝胶。 相对于膜，金属醇盐的重量比例在25％至1％之间。

    Organic-inorganic membranes
    10.
    发明申请
    Organic-inorganic membranes 审中-公开
    有机无机膜

    公开(公告)号：US20040101760A1

    公开(公告)日：2004-05-27

    申请号：US10275113

    申请日：2002-12-12

    发明人： Jochen Kerres ,  Thomas Haring

    IPC分类号： H01M010/40 ,  H01M008/10 ,  C08J005/22

    CPC分类号： B01D67/0093 ,  B01D67/0011 ,  B01D67/0048 ,  B01D69/12 ,  B01D69/141 ,  B01D71/00 ,  B01D71/52 ,  B01D71/68 ,  B01D71/82 ,  B01D2325/26 ,  C08J5/2275 ,  C08J2357/08 ,  H01M8/1011 ,  H01M8/1025 ,  H01M8/1027 ,  H01M8/1032 ,  H01M8/1044 ,  H01M8/1072 ,  H01M8/1074 ,  H01M8/1081 ,  H01M2300/0068 ,  H01M2300/0082 ,  H01M2300/0091 ,  Y02E60/523 ,  Y02P70/56

    摘要： The invention relates to organic/inorganic hybrid polymer blends and hybrid polymer blend membranes that are composed of: one polymer acid halide containing SO2X, POX2 or COX groups (XnullF, Cl, Br, I); one elemental or metallic oxide or hydroxide, obtained by the hydrolysis and/or the sol/gel reaction of an elemental and/or organometallic compound during the membrane forming process and/or by subsequently treating the membrane in aqueous acidic, alkaline or neutral electrolytes. The invention further relates to hybrid blends and hybrid blend membranes containing polymers that carry SO3H, PO3H2 and/or COOH groups, obtained by aqueous, alkaline or acidic hydrolysis of the polymer acid halides contained in the polymer blend or the polymer blend membrane. The invention also relates to methods for producing the inventive hybrid blends and hybrid blend membranes.

    摘要翻译： 本发明涉及由以下组成的有机/无机杂化聚合物共混物和混合聚合物共混物膜：含有SO 2 X，POX 2或COX基团的一种聚合物酰卤（X = F，Cl，Br，I）; 通过元素和/或有机金属化合物在膜形成过程中的水解和/或溶胶/凝胶反应获得的一种元素或金属氧化物或氢氧化物和/或通过随后在酸性，碱性或中性电解质水溶液中处理该膜而得到。 本发明还涉及含有通过聚合物共混物或聚合物共混物膜中所含的聚合物酰卤的水性，碱性或酸性水解得到的SO 3 H，PO 3 H 2和/或COOH基团的聚合物的混合共混物和混合共混膜。 本发明还涉及制备本发明的混合共混物和混合共混膜的方法。