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    Organic microporous materials
    2.
    发明申请
    Organic microporous materials 审中-公开
    有机微孔材料

    公开(公告)号：US20040198587A1

    公开(公告)日：2004-10-07

    申请号：US10481434

    申请日：2004-05-20

    Inventor： Neil B McKeown ,  Saad Maksheed

    IPC: B01J021/00 ,  B01J023/00 ,  B01J025/00 ,  B01J029/00 ,  B32B003/26 ,  B01J020/26

    CPC classification number: C08G73/06 ,  C08G73/0672

    Abstract: A microporous network material comprises a rigid 3-dimensional network of planer porphyrinic macrocycles in which pyrrole residues of adjacent macrocycles are connected by rigid linkers which restrain these adjacent macrocycles such that their porphyrinic planes are in a non-co-planar orientation. Material in accordance with the invention generally have a surface area of at least 300M2 gnull1, e.g. in the range of 100-1000 m2 gnull1. Preferred materials in accordance with the invention are phthalocyanine networks.

    Abstract translation: 微孔网络材料包括平面卟啉大环的刚性三维网络，其中相邻大环的吡咯残基通过刚性连接体连接，其限制这些相邻的大环，使得它们的卟啉平面处于非共平面取向。 根据本发明的材料通常具有至少300M 2 g -1的表面积，例如 在100-1000m 2 -1的范围内。 根据本发明的优选材料是酞菁网络。

    Olefin polymerization catalyst, process for polymerizing olefins, ethylene polymer obtained by said process and use thereof
    3.
    发明申请
    Olefin polymerization catalyst, process for polymerizing olefins, ethylene polymer obtained by said process and use thereof 有权
    烯烃聚合催化剂，烯烃聚合方法，所述方法得到的乙烯聚合物及其用途

    公开(公告)号：US20030027955A1

    公开(公告)日：2003-02-06

    申请号：US10174959

    申请日：2002-06-20

    Inventor： Seiichi Ishii ,  Makoto Mitani ,  Junji Saito ,  Sadahiko Matsuura ,  Naoto Matsukawa ,  Kazutaka Tsuru ,  Terunori Fujita

    IPC: C08F004/44 ,  C08F004/06 ,  B01J021/00 ,  B01J023/00 ,  B01J025/00 ,  B01J029/00 ,  C08F004/40 ,  C08F004/42

    CPC classification number: C08F290/042 ,  C08F8/00 ,  C08F8/36 ,  C08F8/46 ,  C08F110/02 ,  C08F2810/40 ,  C08F4/64048 ,  C08F2500/03 ,  C08F2500/02 ,  C08F2500/17

    Abstract: The present invention provides a novel olefin polymerization catalyst having excellent olefin polymerization activity and, in polymerization with the catalyst comprising a transition metal compound, a polymerization process for preparing a polymer having a low molecular weight with high polymerization activity. The process comprises polymerizing olefin in the presence of an olefin polymerization catalyst comprising (A) a transition metal compound represented by the following 1 nullM: a Group 4 or 5 transition metal atom in the Periodic Table, m: 1-4, R1: H, a C1-C5 linear hydrocarbon group, 3- to 5-membered alicyclic hydrocarbon group, bicycloaliphatic hydrocarbon group wherein two alicyclic rings share one or more carbon atoms, R2 to R6: H, a halogen atom, hydrocarbon group etc, X: H, a halogen atom etc, and n is a valence of Mnull, and (B) at least one compound selected from (B-1) an organometallic compound, (B-2) an organoaluminum oxy compound and (B-3) an ionizing ionic compound.

    Abstract translation: 本发明提供了具有优异的烯烃聚合活性的新型烯烃聚合催化剂，并且在与包含过渡金属化合物的催化剂的聚合中，制备具有高聚合活性的低分子量聚合物的聚合方法。 该方法包括在烯烃聚合催化剂存在下聚合烯烃，所述烯烃聚合催化剂包含（A）由以下[M：元素周期表中第4或5族过渡金属原子表示的过渡金属化合物，m：1-4，R1：H ，C 1 -C 5直链烃基，3〜5元脂环族烃基，2个脂环族共有1个以上碳原子的双环脂族烃基，R 2〜R 6 :H，卤原子，烃基等，X：H 卤素原子等，n为M价），（B）选自（B-1）有机金属化合物，（B-2）有机铝氧化合物和（B-3） 电离离子化合物。

    Synergistic, layered, precious metal-base metal hydrogenation catalysts
    5.
    发明申请
    Synergistic, layered, precious metal-base metal hydrogenation catalysts 审中-公开
    协同，分层，贵金属 - 碱金属加氢催化剂

    公开(公告)号：US20030040433A1

    公开(公告)日：2003-02-27

    申请号：US09939862

    申请日：2001-08-27

    Inventor： Leslie C. Case

    IPC: B01J025/00 ,  B01J023/00

    CPC classification number: B01J25/02 ,  B01J23/8906 ,  B01J23/892 ,  B01J25/00 ,  H01M4/921 ,  H01M4/94 ,  H01M4/98

    Abstract: This invention is the new and useful embodiment of a long-recongized principlenullthat heterogeneous catalysis takes place in at least two steps, (1) hydrogen is taken up (absorbed) by the catalyst, and (2) that absorbed hydrogen that undergoes the further catalytic reaction. The instant invention divides the two steps between two cooperative and intimately connected layersnull(b) a substantial layer of base metal, which absorbs the hydrogen, and then supplies it rapidly to (2) a much less massive layer of precious metal capable of effecting the desired catalysis. The unexpected and very useful advantage of this invention is that it provides very useful rates of heterogeneous catalytic hydrogenation at far lower requirement of precious metal compared to a catalyst body employing precious metal alone.

    Abstract translation: 本发明是长期以来的重要原理的新的有用的实施例，即至少两个步骤进行非均相催化，（1）氢被催化剂吸收（吸收），和（2）吸收氢 进一步催化反应。 本发明将两个合作和紧密连接的层之间的两个步骤分开 - （b）基本金属的基本层，其吸收氢，然后迅速地将其提供给（2）能够实现的少量的贵重金属层 所需的催化。 本发明的意想不到的和非常有用的优点是，与仅使用贵金属的催化剂体相比，其提供了非常有用的非均相催化氢化速率，贵于贵金属的要求低得多。

    Raney catalyst preparation by gas atomisation of molten alloy
    6.
    发明申请
    Raney catalyst preparation by gas atomisation of molten alloy 失效
    通过熔融合金的气体雾化制备阮内催化剂

    公开(公告)号：US20040074571A1

    公开(公告)日：2004-04-22

    申请号：US10240955

    申请日：2002-10-04

    Inventor： Nicholas John Elsworth Adkins ,  Stephen Michael Andrew Sillitto ,  George Paul Yiasemides

    IPC: B01J025/00

    CPC classification number: B01J37/0232 ,  B01J25/00 ,  B01J35/06 ,  B01J37/0225 ,  B01J37/023 ,  C23C4/123

    Abstract: A method of producing a Raney type catalyst, the method comprising melting together a Raney metal and aluminium to form an alloy mixture, pouring the mixture through a nozzle, directing a gas jet on to the mixture to form a spray of droplets, which droplets are directed on to a metallic substrate, the substrate material and thickness and latent heat and superheat of the sprayed material upon initial contact with the substrate being such that the temperature is sufficiently high for an exothermic reaction to take place between the alloy mixture and the substrate such that intermetallic bonds are formed therebetween, and subsequently chemically removing at least some of the aluminium from the sprayed material.

    Abstract translation: 一种制造阮内型催化剂的方法，该方法包括将阮内金属和铝熔融在一起以形成合金混合物，将混合物通过喷嘴浇注，将气体射流引导到混合物上以形成液滴喷雾，该液滴为 指向金属基板时，基板材料和初始接触基板时喷涂材料的厚度和厚度以及潜热和过热使得温度足够高以使合金混合物和基板之间发生放热反应，例如 在其间形成金属间键，随后从喷涂材料中化学除去至少一些铝。

    Skeletal iron catalyst and its preparation for fischer-tropsch synthesis processes
    7.
    发明申请
    Skeletal iron catalyst and its preparation for fischer-tropsch synthesis processes 审中-公开
    骨架铁催化剂及其制备费托合成法

    公开(公告)号：US20020010087A1

    公开(公告)日：2002-01-24

    申请号：US09895540

    申请日：2001-07-02

    Inventor： Jinglai Zhou ,  Yijun Lu ,  Zhixin Zhang ,  Guohui Li ,  Linyao Dong ,  Hairong Wang ,  Peizheng Zhou ,  Lap-Keung Lee

    IPC: B01J025/00 ,  B01J023/00

    CPC classification number: C10G2/332 ,  B01J23/745 ,  B01J25/00 ,  B01J37/0018 ,  B01J37/0036 ,  B01J37/06 ,  B22F9/16 ,  C07C1/0445 ,  C07C1/046 ,  C07C2521/02 ,  C07C2521/06 ,  C07C2523/06 ,  C07C2523/14 ,  C07C2523/745 ,  C07C2523/78 ,  C07C2523/843 ,  C22C38/06 ,  C22C38/16

    Abstract: Skeletal iron catalysts are prepared and utilized for producing synthetic hydrocarbon products from CO and H2 feeds by Fischer-Tropsch synthesis process. Iron powder is mixed with aluminum, antimony, silicon, tin or zinc powder and 0.01-5 wt. % metal promotor powder to provide 20-80 wt. % iron content, then melted together, cooled to room temperature and pulverized to provide 0.1-10 mm iron alloy catalyst precursor particles. The iron alloy precursor particles are treated with NaOH or KOH caustic solution at 30-95null C. to extract or leach out a major portion of the non-ferrous metal portion from the iron and provide the skeletal iron catalyst material. Such skeletal iron catalyst is utilized with COnullH2 feedstream in either fixed bed or slurry bed type reactor at 200-350null C. temperature, 1.0-3.0 mPa pressure and gas hourly space velocity of 0.5-3.0 L/g Fe/h to produce desired hydrocarbon products.

    Abstract translation: 制备骨架铁催化剂，并用于通过费 - 托合成方法从CO和H 2进料生产合成烃产物。 铁粉与铝，锑，硅，锡或锌粉末和0.01-5重量％ ％的金属促进剂粉末提供20-80wt。 铁含量，然后熔化在一起，冷却至室温并粉碎，得到0.1-10mm铁合金催化剂前体颗粒。 铁水合物前体颗粒在30-95℃下用NaOH或KOH苛性碱溶液处理，以从铁中提取或浸出大部分有色金属部分并提供骨架铁催化剂材料。 在200-350℃温度，1.0-3.0mPa压力和0.5-3.0L / g Fe / h的气时空速下，这种骨架铁催化剂与CO + H 2进料流一起用于固定床或浆床型反应器中， 产生所需的烃产物。

    Method for low temperature preparation of a noble metal alloy
    10.
    发明申请
    Method for low temperature preparation of a noble metal alloy 审中-公开
    低温制备贵金属合金的方法

    公开(公告)号：US20020137628A1

    公开(公告)日：2002-09-26

    申请号：US10020073

    申请日：2001-12-14

    Inventor： William R. Even JR.

    IPC: B01J031/00 ,  B01J025/00

    CPC classification number: B01J37/031 ,  B01J23/40

    Abstract: A method for producing fine, essentially contamination free, noble metal alloys is disclosed. The alloys comprise particles in a size range of 5 to 500 nm. The method comprises 1. A method for preparing a noble metal alloy at low temperature, the method comprising the steps of forming solution of organometallic compounds by dissolving the compounds into a quantity of a compatible solvent medium capable of solvating the organometallic, mixing a portion of each solution to provide a desired molarity ratio of ions in the mixed solution, rapidly quenching droplets of the mixed solution to initiate a solute-solvent phase separation as the solvent freezes, removing said liquid cryogen, collecting and freezing drying the frozen droplets to produce a dry powder, and finally reducing the powder to a metal by flowing dry hydrogen over the powder while warming the powder to a temperature of about 150null C.

    Abstract translation: 公开了一种生产精细，基本上无污染的贵金属合金的方法。 该合金包括尺寸范围为5至500nm的颗粒。 该方法包括1.一种低温制备贵金属合金的方法，所述方法包括以下步骤：通过将化合物溶解到一定量的能够溶剂化有机金属的相容溶剂介质中，混合一部分 每个溶液提供混合溶液中所需的离子的摩尔比，快速淬灭混合溶液的液滴，以在溶剂冻结时引发溶质 - 溶剂相分离，除去所述液体冷冻剂，收集并冷冻干燥冷冻液滴以产生 干粉末，最后通过将干燥氢气流过粉末将粉末还原成金属，同时将粉末加热至约150℃的温度。

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