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    Process for the preparation of anhydrous solutions of alkaline phenates in organic solvents
    3.
    发明授权
    Process for the preparation of anhydrous solutions of alkaline phenates in organic solvents 失效
    在有机溶剂中制备碱性磷酸盐的无水溶液的方法

    公开(公告)号：US4113973A

    公开(公告)日：1978-09-12

    申请号：US816919

    申请日：1977-07-19

    申请人： Enzo Alneri ,  Giorgio Bottaccio ,  Stefano Campolmi ,  Luigi Cassar

    发明人： Enzo Alneri ,  Giorgio Bottaccio ,  Stefano Campolmi ,  Luigi Cassar

    IPC分类号： C07C37/60 ,  C07C27/00 ,  C07C37/66 ,  C07C37/72 ,  C07C39/235 ,  C07C39/44 ,  C07C67/00 ,  C07C39/04

    CPC分类号： C07C37/66 ,  C07C37/72

    摘要： A process is disclosed for the preparation of anhydrous solutions of alkaline phenates in organic solvents, comprising the steps:(a) synthesis in water of alkaline phenates by the reaction of sodium sulphate or potassium sulphate with calcium hydroxide and a phenol of the general formula: ##STR1## wherein R and R', which may be the same or different from each other, are hydrogen atoms or linear alkyl groups having up to 4 carbon atoms, at a temperature substantially lower than 30.degree. C;(b) filtering the calcium sulphate;(c) quantitatively decalcifying the residual aqueous solution by the addition of an aqueous solution of NaOH or KOH, until a total concentration is reached which is at least equal to about 30% by weight of the total solution;(d) filtering the precipitated calcium hydroxide and alkaline sulphate;(e) extracting in countercurrent, at a temperature between 50.degree. and about 90.degree. C, the residual aqueous solution with at least one aprotic polar organic solvent; and(f) dehydrating the organic solution of the alkaline phenates.For the extraction in countercurrent of the aqueous residual solution, preferred organic solvents include .beta.-picoline, dimethylether of diethylene glycol, quinoline, tetrahydrofuran, dimethylsulphoxide, sulpholane and N-methyl-morpholine. If desired, a non-polar diluent (e.g., toluene) may also be present.

    Ionic liquids containing a sulfonate anion
    9.
    发明申请
    Ionic liquids containing a sulfonate anion 失效
    含有磺酸根离子的离子液体

    公开(公告)号：US20050131118A1

    公开(公告)日：2005-06-16

    申请号：US10642438

    申请日：2003-08-15

    申请人： Roger Moulton ,  James Davis

    发明人： Roger Moulton ,  James Davis

    IPC分类号： C07C39/44 ,  C07C211/63 ,  C07C309/17 ,  C07D295/088

    CPC分类号： C07D295/088 ,  C07C211/63 ,  C07C309/17 ,  C07C2601/14 ,  Y02P20/544

    摘要： The present invention relates to novel ionic liquids comprising a docusate, docusate variant, or other sulfonate anion. The ionic liquids may be conveniently made via, for example, metathesis. The ionic liquids are often hydrophobic and useful in many hydrocarbon compositions, polymer compositions, and in supercritical carbon dioxide applications. The ionic liquids are capable of hindering static electricity buildup in the hydrocarbon compositions and can therefore minimize flammability and/or explosiveness.

    摘要翻译： 本发明涉及包含多库酯，多库酯变体或其它磺酸根阴离子的新型离子液体。 离子液体可以通过例如复分解方便地制备。 离子液体通常是疏水性的，可用于许多烃组合物，聚合物组合物和超临界二氧化碳应用中。 离子液体能够阻碍烃组合物中的静电积累，因此可以使可燃性和/或爆炸性最小化。