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    Difunctional compound
    3.
    发明专利
    Difunctional compound 失效
    功能化合物

    公开(公告)号：JPS6110537A

    公开(公告)日：1986-01-18

    申请号：JP13140784

    申请日：1984-06-25

    申请人： Sumitomo Chem Co Ltd

    发明人： FUJII NOBUTAKA ,  AKAMICHI KENICHI ,  FUTAKI SHIROU

    IPC分类号： C07D207/46 ,  C07C67/00 ,  C07C201/00 ,  C07C205/54 ,  C07C313/00 ,  C07C323/60 ,  C07K16/00 ,  C07K17/06 ,  C07K19/00 ,  C12N11/06 ,  G01N33/531

    摘要： NEW MATERIAL:A compound of therformula [C(=O)-Z is reactive derivative of carboxyl group].
    EXAMPLE: N-Succinimidyl-p-(2-nitrovinyl)-benzoate.
    USE: Difunctional crosslinking agent: it is used to bind a compound bearing an amino group with another compound bearing a thiol group.
    PREPARATION: The reaction of p-(2-nitrovinyl)benzoic acid with 2,4-dinitrophenol derivative or N-hydroxysuccinimide derivative is carried out in a solvent such as THF or DMF in the presence of a dehydrating agent such as dicyclohexylcarbodiimide to give the compound of the formula. The compound of the formula is used to combine, e.g., peptides or steroids.
    COPYRIGHT: (C)1986,JPO&Japio

    摘要翻译： 新材料：化合物[C（= O）-Z是羧基的反应性衍生物]。 实施例：N-琥珀酰亚胺基 - 对 - （2-硝基乙烯基） - 苯甲酸酯。 用途：双功能交联剂：用于将带有氨基的化合物与带有硫醇基团的另一种化合物结合。 制备：对 - （2-硝基乙烯基）苯甲酸与2,4-二硝基苯酚衍生物或N-羟基琥珀酰亚胺衍生物的反应在溶剂如THF或DMF中，在脱水剂如二环己基碳二亚胺的存在下进行，得到 式的化合物。 式的化合物用于组合，例如肽或类固醇。

    Method for synthesizing compound and synthesis reaction catalyst
    7.
    发明专利
    Method for synthesizing compound and synthesis reaction catalyst 有权
    合成化合物和合成反应催化剂的方法

    公开(公告)号：JP2011046638A

    公开(公告)日：2011-03-10

    申请号：JP2009195760

    申请日：2009-08-26

    申请人： Daihatsu Motor Co Ltd ,  Hokko Chem Ind Co Ltd ,  ダイハツ工業株式会社 ,  北興化学工業株式会社

    发明人： KANEKO MASAYOSHI ,  YAMADA MITSUHIRO ,  TANAKA HIROHISA

    IPC分类号： C07C67/343 ,  B01J23/89 ,  B01J35/10 ,  C07B61/00 ,  C07C69/618 ,  C07C201/12 ,  C07C205/54

    CPC分类号： Y02P20/52

    摘要： PROBLEM TO BE SOLVED: To provide a synthesis reaction catalyst which effectively expresses the activity of palladium and can economically synthesize a compound, and a method for synthesizing a compound using the synthesis reaction catalyst. SOLUTION: In the Heck coupling reaction given by formula (8), a palladium-containing perovskite-type complex catalyst which is represented by formula (1): Ln 2 M y Cu 1-x-y Pd x O 4±δ and has a specific surface area of more than 0.5 m 2 /g and not more than 30 m 2 /g is used as a synthesis reaction catalyst. COPYRIGHT: (C)2011,JPO&INPIT

    摘要翻译： 待解决的问题：提供一种合成反应催化剂，其可以有效地表达钯的活性并可以经济合成化合物，以及使用合成反应催化剂合成化合物的方法。 解决方案：在由式（8）给出的Heck偶联反应中，由式（1）表示的含钯钙钛矿型络合物催化剂：Ln＆lt; SB＆gt; 2＆lt; / SB> Cu 1-xy 4 S> 4>δ，其比表面积大于0.5μm / SP> / g，不大于30m 2 / SP / g用作合成反应催化剂。 版权所有（C）2011，JPO＆INPIT

    PRODUCTION OF BETA-NITROSTYRENE COMPOUND
    9.
    发明专利
    PRODUCTION OF BETA-NITROSTYRENE COMPOUND 失效

    公开(公告)号：JPH04193850A

    公开(公告)日：1992-07-13

    申请号：JP32664390

    申请日：1990-11-27

    申请人： YOSHITOMI PHARMACEUTICAL

    发明人： SAEKI SUMI ,  USU TOSHIHIRO ,  MAUE MASATO ,  TSUINUKI KAZUTO

    IPC分类号： C07C201/12 ,  C07C205/04 ,  C07C205/09 ,  C07C205/11 ,  C07C205/17 ,  C07C205/32 ,  C07C205/54

    摘要： PURPOSE:To obtain the subject substance in high purity and yield with an inexpensive and safe process without producing polymer by-products by reacting a 2-nitro-1-nitrosoethylbenzene compound in a non-polar solvent such as chlorinated hydrocarbon or aromatic hydrocarbon. CONSTITUTION:The objective compound of formula II can be produced by dispersing or dissolving a compound of formula I (X is H, halogen, NO2, NH2, OH, lower alkyl, carboxy, benzyloxy, etc.; (n) is 1-3) in a non-polar solvent (e.g. chloroform or toluene) or in a mixture of water and a non-polar solvent and reacting the compound of formula I at 0-60 deg.C in the presence of 15/1000 to 1/10mol (based on 1mol of the compound of formula I) of an organic base (e.g. triethylamine) or inorganic base (e.g. NaOH) while adding a phase-transfer catalyst as necessary. The compound of formula II is useful as a synthetic intermediate for pharmaceuticals, agricultural chemicals, industrial materials, agricultural and horticultural fungicides, etc.