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    6,6-difluoro-5-hexene-1-amine derivative and agricultural and horticultural pest controlling agent
    6.
    发明专利
    6,6-difluoro-5-hexene-1-amine derivative and agricultural and horticultural pest controlling agent 审中-公开
    6,6-二氟-5-HEXENE-1-胺衍生物和农业和农业害虫控制剂

    公开(公告)号：JP2006056813A

    公开(公告)日：2006-03-02

    申请号：JP2004239336

    申请日：2004-08-19

    Applicant: Ube Ind Ltd ,  宇部興産株式会社

    Inventor： FUJII KATSUTOSHI ,  NAKAMOTO YASUSHI ,  HATANO KOJI ,  KANATSUKI YU

    IPC: C07C211/15 ,  A01N25/04 ,  A01N25/12 ,  A01N25/14 ,  A01N33/04 ,  A01N37/18 ,  A01N43/40 ,  A01N43/54 ,  A01N43/56 ,  A01N47/12 ,  A01N47/22 ,  A01N47/30 ,  A01N47/34 ,  C07C233/13 ,  C07C271/46 ,  C07C275/30 ,  C07D213/74 ,  C07D213/81 ,  C07D231/16 ,  C07D239/42

    Abstract: PROBLEM TO BE SOLVED: To provide a novel 6,6-difluoro-5-hexene-1-amine derivative and an agricultural horticultural pest controlling agent comprising the same as an active ingredient. SOLUTION: The agricultural and horticultural pest controlling agent comprises a new 6,6-difluoro-5-hexene-1-amine derivative (formula I) (wherein Q is a substituent shown in figure B (I-a, I-b, I-c, I-d, I-e, I-f, I-g, I-h, I-i or I-j, provided that R 1 is a lower alkyl group, R 2 is a hydrogen atom or a halogen atom, R 3 is a lower alkyl group, R 4 is a halogen atom, R 5 is a halogen atom, R 6 is a lower alkyl group or a lower haloalkyl group, R 7 is a halogen atom, and X is an oxygen atom or a sulfur atom)) shown in figure A and/or its synthetic intermediate, 6,6-difluoro-5-hexene-1-amine (formula II) shown in figure A as an active ingredient. COPYRIGHT: (C)2006,JPO&NCIPI

    Abstract translation: 待解决的问题：提供新的6,6-二氟-5-己烯-1-胺衍生物和包含其作为活性成分的农业园艺害虫控制剂。 解决方案：农业和园艺害虫控制剂包括新的6,6-二氟-5-己烯-1-胺衍生物（式I）（其中Q是图B所示的取代基（Ia，Ib，Ic， Id，Ie，If，Ig，Ih，Ii或Ij，条件是R 1 为低级烷基，R SP 2为氢原子或卤素原子，R 3 是低级烷基，R 4是卤素原子，R 6是卤原子，R SP 6 >为低级烷基或低级卤代烷基，R A为卤素原子，X为氧原子或硫原子））和/或其合成中间体6 ，6-二氟-5-己烯-1-胺（式II）作为活性成分。 版权所有（C）2006，JPO＆NCIPI

    PURIFICATION OF CARBAMIC ESTER
    9.
    发明专利
    PURIFICATION OF CARBAMIC ESTER 失效

    公开(公告)号：JPH03184947A

    公开(公告)日：1991-08-12

    申请号：JP32391689

    申请日：1989-12-15

    Applicant: ASAHI CHEMICAL IND

    Inventor： YOKOTA MASAHISA ,  ONISHI KAZUHIRO

    IPC: C07C269/08 ,  C07C271/40 ,  C07C271/44 ,  C07C271/46 ,  C07C271/52

    Abstract: PURPOSE:To obtain the title high-purity compound in an industrially advantageous manner through crystallization of its crude form by using a mixed solvent containing an aromatic hydroxyl compound and an organic solvent soluble for this compound at a specified ratio. CONSTITUTION:In purifying a compound, in a crude form, of the formula {R is [substituted (halogen, NO2 or NO)] 2-20C aliphatic or alicyclic hydrocarbon group; Ar is [substituted (one of the above-mentioned groups)]6-20C aromatic hydrocarbon group; n is integer 1-10} through crystallization, using a mixed solvent containing (a) an aromatic hydroxyl compound (pref.

    CARBAMATE DERIVATIVE, PRODUCTION THEREOF AND INDUSTRIAL GERMICIDE CONTAINING THE SAME DERIVATIVE AS ACTIVE INGREDIENT
    10.
    发明专利
    CARBAMATE DERIVATIVE, PRODUCTION THEREOF AND INDUSTRIAL GERMICIDE CONTAINING THE SAME DERIVATIVE AS ACTIVE INGREDIENT 失效

    公开(公告)号：JPH0262855A

    公开(公告)日：1990-03-02

    申请号：JP21270688

    申请日：1988-08-26

    Applicant: SUMITOMO CHEMICAL CO

    Inventor： TAKAHASHI JUNYA ,  YAMAMOTO SHIGEO ,  TERAMAE TOMOHIRO

    IPC: A01N47/22 ,  C07C269/02 ,  C07C271/46

    Abstract: NEW MATERIAL:A carbamate derivative expressed by formula I (X is H or Cl; R is >=3C lower alkyl or hydroxy group). EXAMPLE:3,4,5-Trichlorophenyl N-isopropylcarbamate. USE:Useful as an insecticide for industry capable using as an exterminator of harmful germ against industrial product of wood, bamboo product, textile product, paper product, cosmetics, glass products, paint, synthetic resins, etc., hygienic processing agent, cleaning agent, antiseptics, slime controlling agent, food controlling agent, etc. PREPARATION:A compound expressed by formula Il is reacted with an alkylisocyante expressed by formula III (R' is >=3C lower alkyl) in a solvent such as toluene at ambient temperature to 100 deg.C to provide the compound expressed by formula I or as other method, a compound expressed by formula IV is reacted with a compound expressed by formula V to provide the compound expressed by formula I.

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