公开(公告)号：US10923662B2

公开(公告)日：2021-02-16

申请号：US15975224

申请日：2018-05-09

申请人： LOMOX LIMITED

发明人： Luke William Judd ,  Matthew Phillip Aldred ,  Gene Carl Koch

IPC分类号： H01L51/50 ,  H01L51/00 ,  C07C43/225 ,  C07D417/14 ,  C07D207/452 ,  C07D285/14 ,  C07C69/60 ,  C07C65/21 ,  C07C69/593 ,  C07C69/92 ,  C07D207/46 ,  C08G61/12 ,  C09K11/02 ,  C09K19/32 ,  H01L51/42 ,  H01L51/05

摘要： Compounds of the formula D-S1-A-S2—B1 wherein A comprises a 2,7-disubstituted 9,9-fluoroalkyl fluorene diradical of the formula wherein S1, S2, D and B1 have meanings given in the description that are useful as charge transport and emissive materials for the fabrication of electronic devices such as diodes, transistors, and photovoltaic devices.

公开(公告)号：US10807936B2

公开(公告)日：2020-10-20

申请号：US16711711

申请日：2019-12-12

申请人： Monsanto Technology LLC

发明人： Terri L. Boehm ,  Mangesh Bore ,  Jeffery N. Carroll ,  G. Davis Harris, Jr. ,  Matthew D. McReynolds ,  Justin R. Struble ,  Daniel P. Walker

IPC分类号： C07C51/363 ,  C07C67/035 ,  C07C51/377 ,  C07C69/88 ,  C07C51/367 ,  C07C67/317 ,  C07C67/307 ,  C07C51/29 ,  C07C69/92 ,  C07C69/84 ,  C07C65/05 ,  C07C65/21 ,  C07C47/565 ,  C07C47/56 ,  C07C47/575

摘要： The present disclosure relates, in general, to 5-halo-3,6-dichlorosalicylic acid compounds, 5-halo-3,6-dichlorosalicyaldehyde compounds, processes for preparing 5-halo-3,6-dichlorosalicylic acid compounds, processes for preparing 5-halo-3,6-dichlorosalicyaldehyde compounds, processes for preparing 3,6-dichlorosalicylic acid compounds, and processes that employ such compounds as intermediates in the preparation of the herbicide dicamba.

公开(公告)号：US10160712B2

公开(公告)日：2018-12-25

申请号：US15548100

申请日：2016-12-07

申请人： CHINA UNIVERSITY OF MINING AND TECHNOLOGY

发明人： Jing Liang ,  Huihui Yang ,  Xianyong Wei ,  Zhimin Zong

IPC分类号： C07C51/21 ,  C07C65/21 ,  C07C55/02 ,  C07C55/14 ,  C07C57/03 ,  C07C59/01 ,  C07C59/08 ,  C07C63/06 ,  C07C63/307 ,  B01J31/04 ,  B01J31/02

摘要： A method of catalytic oxidation of a lignite using oxygen as an oxidant at atmospheric pressure is provided. The method includes the following steps, pulverizing the lignite to 200-mesh or less; drying the pulverized lignite at a temperature of 80° C. in vacuum for 10 h; weighing 0.5 g of the dried lignite and sequentially adding 10 ml of acetic acid, 0.5 mmol of a catalyst and 0.15-0.25 mmol of a cocatalyst into a round-bottom flask filled with the oxygen, keeping oxygen pressure at 0.1 MPa, reacting at a temperature of 80-120° C. for 4-12 h; using oxygen as the oxidant to catalytically oxidize the reacted lignite at an atmospheric pressure of 0.1 MPa; filtering after the reaction is finished; decompressing the filtrate to remove the acetic acid, adding a small amount of ethyl acetate to dissolve, and using an excess CH2N2/ether solution to esterify for 10 h at room temperature; and analyzing the esterified product through a gas chromatography-mass spectrometer.

公开(公告)号：US20180261771A1

公开(公告)日：2018-09-13

申请号：US15975224

申请日：2018-05-09

申请人： LOMOX LIMITED

发明人： Luke William Judd ,  Matthew Phillip Aldred ,  Gene Carl Koch

IPC分类号： H01L51/00 ,  C07C43/225 ,  C07C69/593 ,  C07C69/60 ,  C07C69/92 ,  C07D207/452 ,  C07D207/46 ,  C07D285/14 ,  C07D417/14 ,  C08G61/12 ,  C09K11/02 ,  C09K19/32 ,  C07C65/21 ,  H01L51/05 ,  H01L51/42 ,  H01L51/50

CPC分类号： H01L51/0039 ,  C07C43/225 ,  C07C65/21 ,  C07C69/593 ,  C07C69/60 ,  C07C69/92 ,  C07C2603/18 ,  C07D207/452 ,  C07D207/46 ,  C07D285/14 ,  C07D417/14 ,  C08G61/121 ,  C08G2261/146 ,  C08G2261/228 ,  C08G2261/312 ,  C08G2261/3142 ,  C08G2261/3221 ,  C08G2261/3223 ,  C08G2261/3246 ,  C08G2261/512 ,  C08G2261/53 ,  C08G2261/76 ,  C08G2261/91 ,  C08G2261/92 ,  C08G2261/95 ,  C09K11/025 ,  C09K19/32 ,  H01L51/0035 ,  H01L51/0036 ,  H01L51/005 ,  H01L51/0052 ,  H01L51/0068 ,  H01L51/0071 ,  H01L51/0076 ,  H01L51/0512 ,  H01L51/42 ,  H01L51/5012 ,  H01L51/5056 ,  Y02E10/549

摘要： Compounds of the formula D-S1-A-S2—B1 wherein A comprises a 2,7-disubstituted 9,9-fluoroalkyl fluorene diradical of the formula wherein S1, S2, D and B1 have meanings given in the description that are useful as charge transport and emissive materials for the fabrication of electronic devices such as diodes, transistors, and photovoltaic devices.

公开(公告)号：US09988344B2

公开(公告)日：2018-06-05

申请号：US14890053

申请日：2014-05-19

申请人： Covestro Deutschland AG

发明人： Thorsten Dreier ,  Stefan Wershofen ,  Anton Vidal ,  Robert Haak

IPC分类号： C07F3/00 ,  C07C269/04 ,  B01J31/22 ,  C07C51/41 ,  C07C65/21

CPC分类号： C07C269/04 ,  B01J31/2208 ,  B01J2231/34 ,  B01J2531/26 ,  C07C51/418 ,  C07C65/21 ,  C07C271/26 ,  C07C271/24 ,  C07C271/12

摘要： The present invention relates to metallic zinc cluster compounds which are suitable as catalysts in the reaction of amines with dialkyl carbonates to produce carbamates. The invention is also directed towards a method for the alkoxycarbonylation of amines. The cluster compound has a general formula which may be written as [M(O2C—R)2]x.[MO]y.[H2O]z, wherein M is Zn, R is an unsubstituted or substituted aromatic, cycloaliphatic, linear aliphatic, or other organic rest, x is 1, y is ≥x is 1, y is ≥0.03 to ≤26.0 and z is >0.00 to ≤17.0.

公开(公告)号：US09662606B2

公开(公告)日：2017-05-30

申请号：US14238662

申请日：2012-08-08

申请人： Yasutaka Inubushi ,  Chikako Ikeda ,  Takashi Hori

发明人： Yasutaka Inubushi ,  Chikako Ikeda ,  Takashi Hori

IPC分类号： B01D53/04 ,  B01D53/02 ,  C07C63/28 ,  B01J20/22 ,  B01J20/30 ,  B01J20/34 ,  B01D53/047 ,  C01B3/56 ,  C07C65/21 ,  C07F3/00

CPC分类号： B01D53/0462 ,  B01D53/02 ,  B01D53/047 ,  B01D2253/204 ,  B01D2256/18 ,  B01D2257/102 ,  B01D2257/104 ,  B01D2257/304 ,  B01D2257/406 ,  B01D2257/502 ,  B01D2257/504 ,  B01D2257/702 ,  B01D2257/80 ,  B01J20/223 ,  B01J20/226 ,  B01J20/3085 ,  B01J20/3425 ,  B01J20/3483 ,  B01J20/3491 ,  C01B3/56 ,  C01B2203/042 ,  C01B2203/043 ,  C01B2203/0475 ,  C07C63/28 ,  C07C65/21 ,  C07F3/003 ,  Y02C10/08 ,  Y02P20/152 ,  Y02P20/51 ,  Y02P30/30

摘要： The problem of providing a metal complex having excellent gas adsorption performance, gas storage performance, and gas separation performance is solved by a metal complex comprising a dicarboxylic acid compound (I) including 20 to 99 mole % of a dicarboxylic acid compound (I-1) selected from terephthalic acid derivatives having an electron-donating group in the 2nd position such as 2-methoxyterephthalic acid, 2-methylterephthalic acid, and terephthalic acid, and 80 to 1 mole % of a dicarboxylic acid compound (I-2) selected from terephthalic acid derivatives having an electron-withdrawing group in the 2nd position such as 2-nitroterephthalic acid, 2-fluoroterephthalic acid, 2-chloroterephthalic acid, 2-bromoterephthalic acid, and 2-iodoterephthalic acid; at least one kind of metal ion selected from metal ions belonging to Group 2 and Groups 7 to 12 of the periodic table; and an organic ligand capable of bidentate binding to the metal ion.

公开(公告)号：US09573876B2

公开(公告)日：2017-02-21

申请号：US14773372

申请日：2014-03-07

申请人： UNIVERSITY OF CENTRAL FLORIDA RESEARCH FOUNDATION

发明人： Richard Blair

IPC分类号： C07C51/16 ,  C07C45/00 ,  C07C65/21 ,  B01J23/10 ,  C07C45/60 ,  C07C47/58

CPC分类号： C07C65/21 ,  B01J23/10 ,  C07C45/60 ,  C07C47/58 ,  C07C51/16 ,  C07C47/19 ,  C07C49/17

摘要： The presently disclosed and/or claimed inventive concept(s) relates generally to retro-aldol reaction products and methods of making and using same. More particularly, but without limitation, the methods disclosed herein for producing the retro-aldol reaction products are performed in a non-aqueous/solvent-free based process. The reaction products obtained from the process include, for example, dihydroxyacetone, glyceraldehyde, glycolaldehyde, and combinations thereof. In one particular embodiment, the process of making such retro-aldol reaction products includes, without limitation, the step of mechanocatalytically reacting a heterogeneous catalyst with one or more sugar reactants.

摘要翻译： 本公开和/或要求保护的发明构思一般涉及反醛醇醛反应产物及其制备和使用方法。 更具体地，但不限于本文公开的用于生产反醛醇醇反应产物的方法在非水/无溶剂的方法中进行。 从该方法获得的反应产物包括例如二羟基丙酮，甘油醛，乙二醇及其组合。 在一个具体实施方案中，制备这种反醛醇醛反应产物的方法包括但不限于使非均相催化剂与一种或多种糖反应物机械偶联反应的步骤。

公开(公告)号：US20170029355A1

公开(公告)日：2017-02-02

申请号：US15225396

申请日：2016-08-01

申请人： Monsanto Technology LLC

发明人： David A. Morgenstern

IPC分类号： C07C65/21 ,  A01N37/38 ,  C07C205/42 ,  C07C69/92 ,  C07D237/26 ,  A01N43/60 ,  C07D213/64 ,  A01N43/40 ,  C07D237/16 ,  A01N43/58 ,  A01N37/40 ,  C07D241/44

CPC分类号： C07C65/21 ,  A01N37/38 ,  A01N37/40 ,  A01N39/04 ,  A01N43/40 ,  A01N43/42 ,  A01N43/58 ,  A01N43/60 ,  C07C69/712 ,  C07C69/92 ,  C07C205/34 ,  C07C205/37 ,  C07C205/42 ,  C07C205/43 ,  C07C205/56 ,  C07C255/55 ,  C07D213/63 ,  C07D213/64 ,  C07D213/69 ,  C07D213/84 ,  C07D213/85 ,  C07D215/32 ,  C07D237/16 ,  C07D237/26 ,  C07D237/32 ,  C07D241/18 ,  C07D241/44 ,  Y02P20/55 ,  Y02P20/582

摘要： The present invention relates to esters of carboxylic acid agrochemicals comprising a labile protecting group and having formula (I). Certain of the esters of carboxylic acid agrochemicals do not undergo hydrolysis to a significant degree in the dark, but are cleaved to regenerate the parent carboxylic acid agrochemical when exposed to light. Others of the esters of carboxylic acid agrochemicals undergo hydrolysis under both light and dark conditions. The present invention further relates to methods for the controlled release of a carboxylic acid agrochemicals, and to methods of controlling unwanted plants comprising applying to the unwanted plants an ester of a carboxylic acid agrochemical.

摘要翻译： 本发明涉及包含不稳定保护基并具有式（I）的羧酸农药的酯。 某些羧酸农药的酯类在黑暗中不会发生显着程度的水解，但当暴露于光时，它们被切割以再生母体羧酸农药。 羧酸农药的其他酯在光和黑条件下都经历水解。 本发明还涉及羧酸农药的控制释放方法，以及控制不想要的植物的方法，包括向不想要的植物施用羧酸农药的酯。

公开(公告)号：US09464232B2

公开(公告)日：2016-10-11

申请号：US14450533

申请日：2014-08-04

申请人： FUJIFILM Corporation

发明人： Shunya Katoh ,  Masaru Yoshikawa

IPC分类号： C09K19/56 ,  C07C65/21 ,  C07C275/10 ,  C07C309/42 ,  C08K5/107 ,  C09K19/06 ,  C09K19/20 ,  C09K19/22 ,  C09K19/24 ,  C09K19/32 ,  C09K19/34 ,  C07C69/63 ,  C07C69/86 ,  C09K19/36 ,  C08K5/11 ,  C09K19/04 ,  C09K19/18

CPC分类号： C09K19/56 ,  C07C65/21 ,  C07C69/63 ,  C07C69/86 ,  C07C275/10 ,  C07C309/42 ,  C08K5/107 ,  C08K5/11 ,  C09K19/062 ,  C09K19/063 ,  C09K19/2014 ,  C09K19/22 ,  C09K19/24 ,  C09K19/32 ,  C09K19/3405 ,  C09K19/3444 ,  C09K19/3455 ,  C09K19/3477 ,  C09K19/3491 ,  C09K19/36 ,  C09K2019/044 ,  C09K2019/0448 ,  C09K2019/181 ,  C09K2019/2078 ,  C09K2019/3422 ,  C09K2219/03

摘要： A liquid crystal composition containing a liquid crystal molecule, a compound represented by the formula (1), and a compound represented by the formula (2) can provide a film with a reduced haze.

公开(公告)号：US20150361030A1

公开(公告)日：2015-12-17

申请号：US14834935

申请日：2015-08-25

申请人： E I DU PONT DE NEMOURS AND COMPANY

发明人： NEVILLE EVERTON DRYSDALE

IPC分类号： C07C235/48 ,  C07C43/23 ,  C07C67/347 ,  C07C69/92 ,  C07C43/225 ,  C07C231/12 ,  C07C47/575 ,  C07C49/84 ,  C07C51/367 ,  C07C65/21 ,  C07C51/62 ,  C07C41/06 ,  C07C45/70

CPC分类号： C07C235/48 ,  C07C41/06 ,  C07C41/48 ,  C07C43/205 ,  C07C43/225 ,  C07C43/23 ,  C07C43/313 ,  C07C43/315 ,  C07C45/64 ,  C07C45/70 ,  C07C47/575 ,  C07C49/84 ,  C07C51/367 ,  C07C51/62 ,  C07C65/21 ,  C07C67/31 ,  C07C67/347 ,  C07C69/92 ,  C07C231/12

摘要： A compound of formula (I) wherein Rf is —CF3, —C2F5, or —CF2CFXCF3; X is —F, or —OC3F7; Y is —H, —Cl, or —Br; R is —OH, —(CH2)nOH, —(OCH2CH2)mOH, —(CH2)n(OCH2CH2)mOH, —O—C(O)—R1, —(CH2)nO—C(O)—R1, —(OCH2CH2)mOC(O)—R1, —C(O)NHw(CH2CH2OH)2-w, —C≡N, —C≡CH, or —C(O)R2; n is 1 to 10; m is 1 to 10; R1 is C1 to C10 alkyl; R2 is —H, C1 to C10 alkyl, —Cl, or —OCH2CH2OH; a is 1 to 5; b is 1 to 5; and w is 0, 1 or 2.

摘要翻译： 式（I）的化合物，其中R f为-CF 3，-C 2 F 5或-CF 2 CFXCF 3; X为-F或-OC 3 F 7; Y是-H，-Cl或-Br; R 2是-OH， - （CH 2）n OH， - （OCH 2 CH 2）m OH， - （CH 2）n（OCH 2 CH 2）mOH，-O-C（O）-R 1， - （CH 2）n O -C（O） - （OCH2CH2）mOC（O）-R1，-C（O）NHw（CH2CH2OH）2-w，-C≡N，-C≡CH或-C（O） n为1〜10; m为1〜10; R1是C1-C10烷基; R2是-H，C1-C10烷基，-Cl或-OCH2CH2OH; a是1到5; b为1〜5; w为0,1或2。