CAST MOLDED ARTICLE MADE OF POLYURETHANE POROUS SUBSTANCE AND METHOD FOR PRODUCING THE SAME
    131.
    发明申请
    CAST MOLDED ARTICLE MADE OF POLYURETHANE POROUS SUBSTANCE AND METHOD FOR PRODUCING THE SAME 审中-公开
    聚氨酯多孔物质的铸模制品及其制造方法

    公开(公告)号:US20090312444A1

    公开(公告)日:2009-12-17

    申请号:US12350046

    申请日:2009-01-07

    Abstract: An object of the invention is, in producing a cast molded article by crosslinking a water-dispersed urethane prepolymer with a polyamine compound, providing a method for producing a cast molded article made of a polyurethane porous substance in which a cured reactant has good demolding properties and a cast molded article with a fine structure can be easily produced, and a cast molded article having a fine structure with high dimensional accuracy. The cast molded article of this invention is produced by reacting polyol, a chain length regulator, isocyanate and 0.1 through 4 wt % of a hydrophilic chain length regulator to one another, allowing a resultant urethane prepolymer having a terminal isocyanate group to be mixed with and dispersed in water, mixing a resultant water-dispersed urethane prepolymer with 1,4-diaminobutane and injecting a resultant mixture into a die for crosslinkage, and demolding a resultant cured reactant and removing moisture from the cured reactant.

    Abstract translation: 本发明的目的在于,通过使水分散的氨基甲酸酯预聚物与多胺化合物交联来制造模制品,提供一种制备由聚氨酯多孔物质制成的模制品的方法,其中固化的反应物具有良好的脱模性能 并且可以容易地制造具有精细结构的铸模制品,以及具有高尺寸精度的精细结构的铸塑制品。 本发明的铸塑制品通过使多元醇,链长调节剂,异氰酸酯和0.1至4重量%的亲水链长调节剂彼此反应制备,使得得到的具有末端异氰酸酯基团的所得氨基甲酸酯预聚物与 分散在水中,将得到的水分散的氨基甲酸酯预聚物与1,4-二氨基丁烷混合,并将所得混合物注入模具中进行交联,并将所得固化的反应物脱模并从固化的反应物中除去水分。

    High strength air-dried aerogels
    139.
    发明申请
    High strength air-dried aerogels 有权
    高强度风干气凝胶

    公开(公告)号:US20070167534A1

    公开(公告)日:2007-07-19

    申请号:US11335297

    申请日:2006-01-18

    Abstract: A method for the preparation of high strength air-dried organic aerogels. The method involves the sol-gel polymerization of organic gel precursors, such as resorcinol with formaldehyde (RF) in aqueous solvents with R/C ratios greater than about 1000 and R/F ratios less than about 1:2.1. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogeis, this approach generates wet gels that can be air dried at ambient temperatures and pressures. The method significantly reduces the time and/or energy required to produce a dried aerogel compared to conventional methods using either supercritical solvent extraction. The air dried gel exhibits typically less than 5% shrinkage.

    Abstract translation: 一种制备高强度空气干燥有机气凝胶的方法。 该方法包括在R / C比大于约1000且R / F比小于约1:2.1的水性溶剂中有机凝胶前体如间苯二酚与甲醛(RF)的溶胶 - 凝胶聚合。 使用类似于间苯二酚 - 甲醛(RF)气动制剂的方法,该方法产生可在环境温度和压力下风干的湿凝胶。 与使用超临界溶剂萃取的常规方法相比,该方法显着降低了产生干燥气凝胶所需的时间和/或能量。 空气干燥凝胶的收缩率通常小于5%。

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