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    Use of indole derivative for dyeing keratin materials, tinctorial compositions, new compounds and dyeing process
    164.
    发明授权
    Use of indole derivative for dyeing keratin materials, tinctorial compositions, new compounds and dyeing process 失效
    用于染色材料，化学成分，新化合物和染色工艺的染料衍生用途

    公开(公告)号：US5131911A

    公开(公告)日：1992-07-21

    申请号：US769811

    申请日：1991-10-02

    Applicant: Gerard Lang ,  Serge Forestier ,  Alex Junino ,  Herve Richard ,  Jean Jacques Van den Bossche

    Inventor： Gerard Lang ,  Serge Forestier ,  Alex Junino ,  Herve Richard ,  Jean Jacques Van den Bossche

    IPC: A61K8/00 ,  A61K8/34 ,  A61K8/37 ,  A61K8/39 ,  A61K8/49 ,  A61K8/58 ,  A61Q1/00 ,  A61Q5/10 ,  C07D209/08

    CPC classification number: A61Q5/10 ,  A61K8/492 ,  C07D209/08

    Abstract: Process for dyeing keratin fibers by using derivatives of formula: ##STR1## where: R.sub.1 =H, lower alkyl or SiR.sub.11 R.sub.12 R.sub.13 ;R.sub.2 and R.sub.3, which may be identical or different, =H, alkyl, carboxyl, alkoxycarbonyl or --COOSiR.sub.11 R.sub.12 R.sub.13 ;R.sub.4 to R.sub.7, which may be identical or different, =H or an O--Z group, where Z=H, C.sub.1 -C.sub.20 alkyl, aralkyl, formyl, C.sub.2 -C.sub.20 acyl, C.sub.3 -C.sub.20 alkenyl, --SiR.sub.11 R.sub.12 R.sub.13, --P(O)(OR.sub.8).sub.2, R.sub.8 OSO.sub.2 ;or a heterocycle which may contain a P(O)(OR.sub.8) or CR.sub.9 R.sub.10 group;with the reservation that at least two of R.sub.4 to R.sub.7 denotes OZ or form a ring, and that at least one of R.sub.4 or R.sub.7 represents OZ;R.sub.8 and R.sub.9 =H, lower alkyl;R.sub.10 =alkoxy, mono- or dialkylamino;R.sub.11, R.sub.12 and R.sub.13, which may be identical or different, are alkyl groups;or their alkali metal, alkaline-earth metal, ammonium and amine salts.

    Abstract translation: 通过使用下式的衍生物染色角蛋白纤维的方法：其中：R1 = H，低级烷基或SiR11R12R13; R2和R3可以相同或不同，= H，烷基，羧基，烷氧基羰基或-COOSiR11R12R13; 其中Z = H，C 1 -C 20烷基，芳烷基，甲酰基，C 2 -C 20酰基，C 3 -C 20链烯基，-SiR 11 R 12 R 13，-P（O）（OR 8），R 4至R 7可以相同或不同， 2，R8OSO2; 或可含有P（O）（OR 8）或CR 9 R 10基团的杂环; 保留R4至R7中的至少两个表示OZ或形成环，并且R4或R7中的至少一个表示OZ; R8和R9 = H，低级烷基; R10 =烷氧基，单或二烷基氨基; R 11，R 12和R 13可以相同或不同，是烷基; 或它们的碱金属，碱土金属，铵和胺盐。

    Process for the preparation of 6-piperidino-2,4-diamino pyrimidine-3-oxide and novel compounds
    165.
    发明授权
    Process for the preparation of 6-piperidino-2,4-diamino pyrimidine-3-oxide and novel compounds 失效
    制备6-哌啶基-2,4-二氨基嘧啶-3-氧化物和新化合物的方法

    公开(公告)号：US5126453A

    公开(公告)日：1992-06-30

    申请号：US636126

    申请日：1990-12-31

    Applicant: Jean Maignan ,  Serge Restle ,  Gerard Lang

    Inventor： Jean Maignan ,  Serge Restle ,  Gerard Lang

    IPC: A61K8/00 ,  A61K8/49 ,  A61Q5/00 ,  C07D239/48 ,  C07D239/50 ,  C07D239/52

    CPC classification number: C07D239/48 ,  C07D239/50 ,  Y02P20/55

    Abstract: In a first stage of a process for the preparation of 6-piperidino-2,4-diaminopyrimidine-3-oxide at least one of the two amino groups of a compound having formula (1): ##STR1## where X represents a halogen atom or OH group, is protected by an addition reaction with an isocyanate having formula:R--N=C=OIn this formula R represents an alkyl group, or one of the amino groups. The resulting urea derivative is then oxidized to produce the corresponding N-oxide which is then reacted with piperidine. The protective group(s) are then eliminated by reaction with an organic or inorganic base.

    Abstract translation: 在具有式（1）的化合物的两个氨基中的至少一个中制备6-哌啶子基-2,4-二氨基嘧啶-3-氧化物的方法的第一阶段：其中X表示 通过与具有下式的异氰酸酯的加成反应来保护卤素原子或OH基团：RN = C = O在该式中，R表示烷基或氨基之一。 然后将所得的脲衍生物氧化以产生相应的N-氧化物，然后与哌啶反应。 然后通过与有机或无机碱反应除去保护基。

    Meta-phenylenediamines, process for preparation thereof, intermediate compounds and use of these meta-phenylenediamines as couplers for the oxidation dyeing of keratinous fibres and especially human hair
    170.
    发明授权
    Meta-phenylenediamines, process for preparation thereof, intermediate compounds and use of these meta-phenylenediamines as couplers for the oxidation dyeing of keratinous fibres and especially human hair 失效
    间苯二胺，其制备方法，中间体化合物和这些间苯二胺作为角质纤维，特别是人发的氧化染色的成色剂的用途

    公开(公告)号：US4960432A

    公开(公告)日：1990-10-02

    申请号：US200170

    申请日：1988-05-31

    Applicant: Alex Junino ,  Jean J. Vandenbossche ,  Herve Borowiak ,  Gerard Lang

    Inventor： Alex Junino ,  Jean J. Vandenbossche ,  Herve Borowiak ,  Gerard Lang

    IPC: D06P3/14 ,  A61K20060101 ,  A61K8/00 ,  A61K8/41 ,  A61Q5/10 ,  C07C20060101 ,  C07C215/78 ,  C07C215/80 ,  C07C217/84 ,  C09B53/02 ,  D06P1/32 ,  D06P3/04 ,  D06P3/08

    CPC classification number: A61K8/411 ,  A61Q5/10

    Abstract: New meta-phenylenediamines, process for preparation thereof, intermediate compounds and use of these metaphenylenediamines as couplers for the oxidation dyeing of keratinous fibres and especially human hair.The invention relates to the compounds of the formula: ##STR1## in which R.sub.1 and R.sub.2 denote, independently of one another, a hydrogen atom, a C.sub.1 -C.sub.4 alkyl radical or a C.sub.2 -C.sub.3 mono- or polyhydroxyalkyl radical,Z and Z' denote, independently of one another, a C.sub.1 -C.sub.4 alkyl or C.sub.2 -C.sub.4 hydroxyalkyl radical, with the proviso that, when R.sub.1 and R.sub.2 simultaneously denote a hydrogen atom, Z and Z' do not simultaneously denote a methyl radical, and to their addition salts with an acid, to a process for preparation thereof and also to their use, by way of couplers, in an aqueous vehicle, in combination with at least one oxidation dye percursor of the para type, for the dyeing of human hair.The invention also relates to the intermediate compounds of the formula: ##STR2## in which R' denotes a hydrogen atom, a C.sub.1 -C.sub.4 alkyl radical, a C.sub.2 or C.sub.3 mono- or polyhydroxyalkyl radical, or an acetyl or .beta.-chloethoxycarbonyl radical, and z and z' denote, independently of one another, a C.sub.1 -C.sub.4 alkyl radical.

    Abstract translation: 新的间苯二胺，其制备方法，中间体化合物以及这些间苯二胺作为角质纤维，特别是人类头发氧化染色的成色剂的用途。 本发明涉及下式的化合物：其中R 1和R 2彼此独立地表示氢原子，C 1 -C 4烷基或C 2 -C 3单 - 或多羟基烷基，Z 和Z'彼此独立地表示C1-C4烷基或C2-C4羟烷基，条件是当R1和R2同时表示氢原子时，Z和Z'不同时表示甲基，并且 与它们与酸的加成盐，涉及其制备方法，以及它们通过成色剂在水性载体中与至少一种对位型氧化染料组合物的组合用于人发染色 。 本发明还涉及下式的中间体化合物：其中R'表示氢原子，C 1 -C 4烷基，C 2或C 3单烷基或多羟基烷基，或乙酰基或β- 氯乙氧基羰基，z和z'彼此独立地表示C1-C4烷基。

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