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    Catalyst for olefin polymer production and process for olefin polymer production employing the catalyst
    181.
    发明授权
    Catalyst for olefin polymer production and process for olefin polymer production employing the catalyst 失效
    用于烯烃聚合物生产的催化剂和使用催化剂的烯烃聚合物生产方法

    公开(公告)号：US06372681B1

    公开(公告)日：2002-04-16

    申请号：US09281062

    申请日：1999-03-09

    Applicant: Satoru Yamada ,  Akihiro Yano

    Inventor： Satoru Yamada ,  Akihiro Yano

    IPC: B01J3100

    CPC classification number: C08F10/00 ,  C08F4/61922 ,  C08F110/02 ,  C08F210/16 ,  C08F4/61912 ,  C08F210/14 ,  C08F2500/03

    Abstract: A novel catalyst for olefin polymerization is provided which comprises [A] a metallocene compound containing a transition metal selected from Groups 3, 4, 5, and 6 of Periodic Table, [B] a reaction product of topotactic reduction by electron transfer, and [C] an organoaluminum compound. The catalyst may contain additionally [D] an organoalkaline earth metal compound or an organozinc compound. This catalyst has high catalytic activity for olefin polymerization without employing an expensive catalyst component.

    Abstract translation: 提供了一种用于烯烃聚合的新型催化剂，其包含[A]含有选自元素周期表第3,4,5和6族的过渡金属的金属茂化合物，[B]通过电子转移的拓扑定向还原反应的产物和[ C]有机铝化合物。 该催化剂可另外含有[D]有机碱土金属化合物或有机锌化合物。 该催化剂在不使用昂贵的催化剂组分的情况下对烯烃聚合具有高催化活性。

    Ethylene polymerization catalyst and catalyst system
    185.
    发明授权
    Ethylene polymerization catalyst and catalyst system 失效
    乙烯聚合催化剂和催化剂体系

    公开(公告)号：US06323148B1

    公开(公告)日：2001-11-27

    申请号：US09441801

    申请日：1999-11-17

    Applicant: Mark K. Reinking

    Inventor： Mark K. Reinking

    IPC: B01J3100

    CPC classification number: B01J31/122 ,  B01J31/0274 ,  B01J31/38 ,  B01J37/0018 ,  C08F210/16 ,  C08F4/6565 ,  C08F4/025 ,  C08F210/08 ,  C08F2500/12 ,  C08F2500/21 ,  C08F2500/26 ,  C08F210/14

    Abstract: An ethylene polymerization catalyst and catalyst system which provides an ethylene copolymer which is characterized by desirable ER shift values. The high level ER shift of these polymers produce films having high impact strength. The catalyst is prepared by treating a support material with an agent selected from the group consisting of a compound having the structural formula BX53, where X5 is fluorine, chlorine, bromine, iodine or OR5, where R5 is C1-C6 alkyl; a compound having the structural formula X62 where X6 is fluorine, bromine or iodine; a compound having the structural formula NR6, where R6 is C1-C6 alkyl or OR7, where R7 is C1-C8 alkyl; and a compound having the structural formula Ti(OR8)4, where R8 is C1-C6 alkyl or phenyl to reduced surface hydroxyl group concentration of the support material. The thus treated support material is thereupon contacted with a dialkylmagnesium compound or complex, an alcohol compound or a silane compound and a transition metal compound, in that order. Alternatively, the sequence of contact of the transition metal compound and the silane compound may be reversed, as may be the sequence of addition of the dialkylmagnesium compound or complex and the silane compound.

    Abstract translation: 提供乙烯共聚物的乙烯聚合催化剂和催化剂体系，其特征在于所需的ER转移值。 这些聚合物的高水平ER变化产生具有高冲击强度的膜。 通过用选自具有结构式BX53的化合物，其中X5是氟，氯，溴，碘或OR5的化合物处理载体材料来制备催化剂，其中R5是C1-C6烷基; 具有结构式X62的化合物，其中X 6是氟，溴或碘; 具有结构式NR 6的化合物，其中R 6是C 1 -C 6烷基或OR 7，其中R 7是C 1 -C 8烷基; 和具有结构式Ti（OR 8）4的化合物，其中R 8是C 1 -C 6烷基或苯基，以降低载体材料的表面羟基浓度。 随后将如此处理的载体材料依次与二烷基镁化合物或络合物，醇化合物或硅烷化合物和过渡金属化合物接触。 或者，过渡金属化合物和硅烷化合物的接触顺序可以相反，可以是二烷基镁化合物或络合物和硅烷化合物的添加顺序。

    Catalyst for decomposing organohalogen compound
    187.
    发明授权
    Catalyst for decomposing organohalogen compound 失效
    用于分解有机卤素化合物的催化剂

    公开(公告)号：US06271168B1

    公开(公告)日：2001-08-07

    申请号：US09667304

    申请日：2000-09-25

    Applicant: Tomoyuki Imai ,  Satoshi Hatakeyama ,  Toshiki Matsui ,  Yasuhiko Fujii ,  Tomoko Okita

    Inventor： Tomoyuki Imai ,  Satoshi Hatakeyama ,  Toshiki Matsui ,  Yasuhiko Fujii ,  Tomoko Okita

    IPC: B01J3100

    CPC classification number: B01J37/04 ,  B01D53/8662 ,  B01D2255/20738 ,  B01J23/745 ,  B01J27/049 ,  B01J27/1853 ,  B01J31/0254 ,  B01J35/1009 ,  B01J35/1014 ,  B01J35/1019 ,  B01J37/06

    Abstract: A composite catalyst for decomposing an organohalogen compound of the present invention, comprises composite particles comprising: iron compound particles having an average particle size of 0.01 to 2.0 &mgr;m, a phosphorus content of not more than 0.02% by weight based on the weight of the particles, a sulfur content of not more than 0.3% by weight based on the weight of the particles, and a sodium content of not more than 0.3% by weight based on the weight of the particles; and an amine compound, said composite catalyst having a catalytic activity capable of decomposing not less than 50% by weight of monochlorobenzene when 50 mg of a mixture comprising iron oxide particles obtained by heat-treating said iron compound particles at a temperature of 300° C. for 60 minutes in air, and the amine compound, is instantaneously contacted with 5.0×10−7 mol of monochlorobenzene at a temperature of 300° C. at a space velocity of 150,000 h−1 in an inert gas atmosphere using a pulse catalytic reactor.

    Abstract translation: 用于分解本发明的有机卤素化合物的复合催化剂包括复合颗粒，其包含：平均粒度为0.01至2.0μm的铁化合物颗粒，基于颗粒重量的磷含量不超过0.02重量％ ，基于颗粒重量，不超过0.3重量％的硫含量，并且基于颗粒重量，钠含量不超过0.3重量％; 所述复合催化剂具有催化活性，当通过在300℃的温度下热处理所述铁化合物颗粒而获得的50mg包含氧化铁颗粒的混合物时，能够分解不低于50重量％的一氯苯。 在惰性气体气氛下，使用脉冲催化反应器，使空气中的胺化合物在300℃，150,000h -1的空速下与5.0×10-7mol的一氯苯瞬间接触。

    Boratabenzene cocatalyst with metallocene catalyst
    188.
    发明授权
    Boratabenzene cocatalyst with metallocene catalyst 失效
    硼酸钡助催化剂与金属茂催化剂

    公开(公告)号：US06255246B1

    公开(公告)日：2001-07-03

    申请号：US09487399

    申请日：2000-01-18

    Applicant: David D. Devore ,  Francis J. Timmers ,  David R. Neithamer

    Inventor： David D. Devore ,  Francis J. Timmers ,  David R. Neithamer

    IPC: B01J3100

    CPC classification number: C08F10/00 ,  C08F4/61908 ,  C08F4/61916 ,  C08F4/6192 ,  C08F4/65908

    Abstract: Boratabenzene cocatalysts, especially novel pentafluorophenyl boratabenzenes, are useful cocatalysts or activators with metallocenes. They are less expensive than prior art activators, are soluble and offer more irreversible reactions. Compositions comprise at least one metallocene catalyst and at least one dihydroboratabenzene or anion thereof. Processes include polymerizations with metallocenes in the presence of a boratabenzene cocatalyst.

    Abstract translation: 硼化物助催化剂，特别是新的五氟苯基硼苯偶氮，是有用的助催化剂或具有金属茂的活化剂。 它们比现有技术的活化剂便宜，是可溶的并且提供更多的不可逆反应。 组合物包含至少一种金属茂催化剂和至少一种二氢硼烷基或其阴离子。 方法包括在硼烷偶合助催化剂存在下与金属茂的聚合。

    Process for producing a vanadium phosphorus oxide catalyst
    190.
    发明授权
    Process for producing a vanadium phosphorus oxide catalyst 失效
    钒磷氧化物催化剂的制备方法

    公开(公告)号：US06228798B1

    公开(公告)日：2001-05-08

    申请号：US09308573

    申请日：1999-05-21

    Applicant: Sadesh H Sookraj

    Inventor： Sadesh H Sookraj

    IPC: B01J3100

    CPC classification number: B01J23/002 ,  B01J27/198 ,  B01J2523/00 ,  C07C51/215 ,  C07C51/25 ,  C07C57/145 ,  B01J2523/22 ,  B01J2523/3712 ,  B01J2523/51 ,  B01J2523/55 ,  B01J2523/72 ,  B01J2523/54 ,  B01J2523/48 ,  B01J2523/845 ,  B01J2523/67 ,  B01J2523/68

    Abstract: A method of making a vanadium phosphorus oxide (VPO) catalyst by precipitating from a 45-65 g/l solution of V4+ ions and V5+ ions a vanadium- and phosphorus-containing precipitate comprising a complex of formula VOHPO4. The precipitate is calcined under an inert atmosphere to produce a VPO catalyst whole active phase is formula (VO)2P2O9. Said solution comprises cations of at least two of Bi, Zr, Cr, Ce, Co, Mn, Mg and Mo such that the precipitate comprises 1-25% by mass of said dopant metal cations in total, the balance being said complex. Each dopant metal forms 0.1-20% by mass of the precipitate.

    Abstract translation: 一种通过从45-65g / l的V4 +离子和V5 +离子溶液中沉淀含钒和磷的沉淀物制备钒磷氧化物（VPO）催化剂的方法，该方法包括式VOHPO4的络合物。 将沉淀物在惰性气氛下煅烧以产生VPO催化剂，整个活性相为式（VO）2 P 2 O 9。 所述溶液包含Bi，Zr，Cr，Ce，Co，Mn，Mg和Mo中的至少两种的阳离子，使得沉淀物总共包含1-25质量％的所述掺杂金属阳离子，余量为所述络合物。 每种掺杂剂金属形成0.1-20质量％的沉淀物。

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