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    NANO-ENCAPSULATING POLYMERS WITH HIGH BARRIER PROPERTIES
    12.
    发明申请
    NANO-ENCAPSULATING POLYMERS WITH HIGH BARRIER PROPERTIES 有权
    具有高阻挡性能的纳米聚合物聚合物

    公开(公告)号：US20150333261A1

    公开(公告)日：2015-11-19

    申请号：US14651841

    申请日：2013-09-12

    Applicant: EMPIRE TECHNOLOGY DEVELOPMENT LLC

    Inventor： Georgius Abidal ADAM

    IPC: H01L51/00 ,  C09D179/04

    CPC classification number: H01L51/0035 ,  C08G65/22 ,  C08G65/263 ,  C08G73/0644 ,  C08G2650/06 ,  C08K5/34928 ,  C09D179/04 ,  H01L51/0043 ,  H01L51/5253 ,  H01L51/56 ,  H01L2924/0002 ,  H01L2924/00

    Abstract: Polymeric barriers for organic light emitting diodes are formed in-situ by encapsulation or polymerization. Encapsulation with melamine-cyanurate is performed using sublimation reaction technique. An encapsulation technique involves curing a layer of resin made by mixing a polyaza aryl compound, such as melamine, melam, or melem, with a cyanuryl triglycidyl ether. Another encapsulation technique involves curing a layer of resin made by mixing the polyaza aryl aromatic compound in 2,4,6-tricyanatophenyl glycidyl ether or tetracyanatobenzene applied to an organic light emitting diode. Photo catalytic curing of the coating may be achieved in the presence of catalysts such as titanium IV oxide acetylacetonate.

    Abstract translation: 通过包封或聚合原位形成有机发光二极管的聚合物屏障。 使用升华反应技术进行三聚氰胺 - 氰尿酸盐的封装。 包封技术包括固化通过将多芳基芳基化合物（例如三聚氰胺，二聚氰胺或多米酚）与氰尿酰基三缩水甘油醚混合而制得的树脂层。 另一种封装技术包括固化通过将多芳基芳基化合物混合在施加到有机发光二极管的2,4,6-三氰基苯基缩水甘油醚或四氰基苯中而制得的树脂层。 涂层的光催化固化可以在催化剂如乙酰丙酮钛IV的存在下实现。

    Nonaqueous compositions and additives therefor
    15.
    发明授权
    Nonaqueous compositions and additives therefor 有权
    非水组合物及其添加剂

    公开(公告)号：US06540942B2

    公开(公告)日：2003-04-01

    申请号：US09977824

    申请日：2001-10-15

    Applicant: Miguel A. Dones ,  Ramesh L. Narayan

    Inventor： Miguel A. Dones ,  Ramesh L. Narayan

    IPC: C08F246

    CPC classification number: C08L71/02 ,  C08G59/04 ,  C08G65/337 ,  C08G2650/06 ,  C08G2650/16 ,  C08K5/00 ,  C08L63/00 ,  C08L2205/05 ,  C09D7/63 ,  C08L2666/04 ,  C08L71/00

    Abstract: Nonaqueous compositions comprising at least one product of the reaction between A) a linking agent of formula I R4(Y)3  (I) Wherein each Y group is a halogen atom or one Y group is a halogen atom and two Y groups represent an epoxy oxygen atom, which is attached to two adjacent carbon atoms in the R4 group to form an epoxy group, and R4 is an alkanetriyl group containing from 3 to 10 carbon atoms; and B) a compound of formula II R3(EO)n(PO)m(BO)pX  (II) Wherein R3 is substituted or unsubstituted, saturated or unsaturated, organic oxy or thio group having from 1 to 36 carbon atoms or a primary or secondary amino group having from 1 to 36 carbon atoms; n is a number of from 0 to 50; m is a number of from 0 to 50; p is a number of from 0 to 50; and X is hydrogen, or X can be a mercapto group, an amino group, or a C1-C6 alkylamino group in place of a terminal —OH group, provided that when X is mercapto, amino or a C1-C6 alkylamino, the sum of n, m, and p must be at least 1; and the mole ratio of I:II is from about 0.1:1 to about 5:1.

    Abstract translation: 包含A）每个Y基团之间的式（I）的交联剂的至少一种产物的非水性组合物是卤素原子或一个Y基团是卤素原子，两个Y基团表示环氧氧原子，其与两个相邻碳原子连接 R4基团中的原子形成环氧基，R4是含有3〜10个碳原子的烷撑三基; 和B）式II化合物其中R 3是取代或未取代的饱和或不饱和的具有1至36个碳原子的有机氧基或硫基或具有1至36个碳原子的伯或仲氨基; n为0〜50的数; m是从0到50的数字; p是从0到50的数字; 并且X是氢，或X可以是巯基，氨基或C1-C6烷基氨基代替末端-OH基团，条件是当X是巯基，氨基或C1-C6烷基氨基时，总和 n，m和p必须至少为1; 且I：II的摩尔比为约0.1:1至约5:1。

    Process for preparing ether-capped poly(oxyalkylated) alcohol surfactants
    16.
    发明授权
    Process for preparing ether-capped poly(oxyalkylated) alcohol surfactants 失效
    制备醚封端的聚（烷氧基化）醇表面活性剂的方法

    公开(公告)号：US06495727B1

    公开(公告)日：2002-12-17

    申请号：US09831117

    申请日：2001-05-04

    Applicant: Glenn Thomas Jordan, IV ,  Larry Eugene Miller ,  Donald Eugene Levengood ,  Mark Robert Sivik ,  Bernard William Kluesener ,  Terry Franklin Formyduval ,  Deborah Jean Back

    Inventor： Glenn Thomas Jordan, IV ,  Larry Eugene Miller ,  Donald Eugene Levengood ,  Mark Robert Sivik ,  Bernard William Kluesener ,  Terry Franklin Formyduval ,  Deborah Jean Back

    IPC: C07C4311

    CPC classification number: B01F17/0028 ,  C08G65/22 ,  C08G65/2609 ,  C08G2650/06 ,  C08G2650/34 ,  C11D1/721

    Abstract: A process for preparing an ether-capped poly(oxyalkylated) alcohol surfactant having the formula R1O[CH2CH(R3)O]xCH2CH(OH)CH2OR2 wherein R1 and R2 are linear or branched, saturated or unsaturated, aliphatic or aromatic hydrocarbon radicals having from 1 to about 30 carbon atoms; R3 is H, or a linear aliphatic hydrocarbon radical having from 1 to about 4 carbon atoms; x is an integer having an average value from 1 to about 30, wherein when x is about 2 or greater R3 may be the same or different; further wherein when x is about 15 or greater and R3 is H and methyl, at least four of R3 are methyl, further wherein when x is about 15 or greater and R3 includes H and from 1 to 3 methyl groups, then at least one R3 is ethyl, propyl or butyl, further wherein R2 can optionally be alkoxylated, wherein said alkoxy is selected from ethoxy, propoxy, butoxy and mixtures thereof; said process comprising the steps of: (b) providing a glycidyl ether having the formula:  wherein R2 is defined as above; (c) providing an ethoxylated alcohol having the formula:  wherein R1, R3 and x are defined as above; (f) reacting said glycidyl ether with said ethoxylated alcohol to form said surfactant in the presence of a basic catalyst; (g) said surfactant is sparged with an inert gas, preferably N2, Ar and mixtures thereof, optionally under vacuum, preferably a vacuum in the range of 5 to 500 mmHg; and said surfactant is bleached with an about 0.05% to about 5.0%, preferably about 0.1% to about 1.0%, by weight solution of a bleach at a temperature from about 25° C. to about 95° C.

    Abstract translation: 制备具有式R 1和R 2的醚的聚（烷氧基化）醇表面活性剂的方法是具有1至约30个碳原子的直链或支链，饱和或不饱和的脂族或芳族烃基; R3是H或具有1至约4个碳原子的直链脂族烃基; x是平均值为1至约30的整数，其中当x为约2或更大时，R 3可以相同或不同; 其中当x为约15或更大且R 3为H和甲基时，R 3中的至少4个为甲基，此外，当X为约15或更大且R 3包括H和1至3个甲基时，则至少一个R 3 乙基，丙基或丁基，其中R 2可任选地被烷氧基化，其中所述烷氧基选自乙氧基，丙氧基，丁氧基及其混合物; 所述方法包括以下步骤：（b）提供具有下式的缩水甘油醚：其中R2如上定义;（c）提供具有下式的乙氧基化醇：其中R1，R3和x如上定义;（f） 使所述缩水甘油醚与所述乙氧基化醇反应以在碱性催化剂存在下形成所述表面活性剂;（g）任选地在真空下，优选在该范围内的真空下，用惰性气体，优选N 2，Ar及其混合物喷射所述表面活性剂 为5〜500mmHg; 漂白剂在约25℃至约95℃的温度下漂白约0.05％至约5.0％，优选约0.1％至约1.0％的漂白剂。

    Branched polymeric surfactant reaction products, methods for their preparation, and uses therefor
    17.
    发明申请
    Branched polymeric surfactant reaction products, methods for their preparation, and uses therefor 有权
    支化聚合物表面活性剂反应产物，其制备方法及用途

    公开(公告)号：US20010027227A1

    公开(公告)日：2001-10-04

    申请号：US09783855

    申请日：2001-02-15

    Inventor： Kenneth Breindel ,  Ronald W. Broadbent ,  Michael S. Wiggins ,  Marcie Natale

    IPC: C08J003/03 ,  C08L063/00 ,  C08L071/00 ,  C08L079/00 ,  C08G073/00 ,  C08G065/00 ,  C08G059/00 ,  C09D163/00 ,  C09D171/00 ,  C09D179/00

    CPC classification number: C08G65/337 ,  B01D19/0427 ,  C08G65/33306 ,  C08G2650/06 ,  C08G2650/50 ,  C08L71/02 ,  C08L71/03 ,  C08L79/02 ,  C09D5/024 ,  C09D7/65

    Abstract: Polymeric compounds useful as low foaming surfactants and defoaming and stabilizing agents for aqueous-and nonaqueous-based compositions, and to processes for the preparation of the polymeric compounds, wherein the polymeric compounds are the reaction products of reactants comprising A) at least one linking compound of formula I R1(X)3nullnull(I) wherein each X group is a halogen atom or one X group is a halogen atom and two X groups represent an epoxy oxygen atom, which is attached to two adjacent carbon atoms in the R1 group to form an epoxy group, and R1 is an alkanetriyl group containing from 3 to 10 carbon atoms; and B) compounds of formula 11 R2(OA)nXnullnull(II) wherein R2 is an organic group containing from 4 to 36 carbon atoms, n is a number of from 0 to 200, X is nullOH, nullNHRnull, or nullSH and each OA group is independently an ethyleneoxy, 1,2-propyleneoxy, or 1,2-butyleneoxy group.

    Abstract translation: 用作低泡表面活性剂的聚合化合物和用于水基和非水基组合物的消泡和稳定剂以及制备聚合物的方法，其中聚合物是反应物的反应产物，其包含A）至少一种连接化合物 其中每个X基团是卤素原子或一个X基团是卤素原子，其中每个X基团是卤原子，或者一个X基团是卤素原子 并且两个X基团表示环氧氧原子，其与R1基团中的两个相邻碳原子连接以形成环氧基，并且R 1是含有3至10个碳原子的烷三基; 和B）式11化合物（其中R2是含有4至36个碳的有机基团），其中R2是含有4至36个碳的有机基团 原子，n为0〜200的数，X为-OH，-NHR'或-SH，各OA基独立为亚乙氧基，1,2-亚丙氧基或1,2-亚丁氧基。

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