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公开(公告)号：US5278116A
公开(公告)日：1994-01-11
申请号：US878113
申请日：1992-05-04
申请人： Charles T. Kresge , Wieslaw J. Roth
发明人： Charles T. Kresge , Wieslaw J. Roth
CPC分类号： B01J29/049
摘要： There is provided a method for preparing a pillared layered material, designated MCM-36, with a characteristic X-ray diffraction pattern. Upon calcination of the swollen, non-pillared form of this material, the layers collapse and condense upon one another in a somewhat disordered fashion to form a non-swellable material. However, when the swollen layered material is intercalated with polymeric oxide pillars, the layer separation is maintained, even after calcination. Cerium-containing aluminum phosphate gel particles are used to pillar the layered material.
摘要翻译： 提供了一种具有特征X射线衍射图谱的制备称为MCM-36的柱状分层材料的方法。 在煅烧该材料的膨胀的非柱形形式时，这些层以有点无序的方式彼此崩溃并冷凝，形成不溶胀的材料。 然而，当膨胀的层状材料插入聚合物氧化物柱时，即使在煅烧之后也保持层分离。 使用含铈磷酸铝凝胶颗粒来支撑层状材料。
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公开(公告)号：US5278115A
公开(公告)日：1994-01-11
申请号：US887811
申请日：1992-05-04
申请人： Charles T. Kresge , Wieslaw J. Roth
发明人： Charles T. Kresge , Wieslaw J. Roth
CPC分类号： B01J29/049
摘要： There is provided a method for preparing a pillared layered material, designated MCM-36, with a characteristic X-ray diffraction pattern. Upon calcination of the swollen, non-pillared form of this material, the layers collapse and condense upon one another in a somewhat disordered fashion to form a non-swellable material. However, when the swollen layered material is intercalated with polymeric oxide pillars, the layer separation is maintained, even after calcination. A combination of tetraethylorthosilicate and zirconium alkoxide is used as a pillaring agent for treating the swollen material.
摘要翻译： 提供了一种具有特征X射线衍射图谱的制备称为MCM-36的柱状分层材料的方法。 在煅烧该材料的膨胀的非柱形形式时，这些层以有点无序的方式彼此崩溃并冷凝，形成不溶胀的材料。 然而，当膨胀的层状材料插入聚合物氧化物柱时，即使在煅烧之后也保持层分离。 使用原硅酸四乙酯和烷氧基锆的组合作为用于处理膨胀材料的支柱剂。
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公开(公告)号：US5266541A
公开(公告)日：1993-11-30
申请号：US811383
申请日：1991-12-20
申请人： Charles T. Kresge , Wieslaw J. Roth
发明人： Charles T. Kresge , Wieslaw J. Roth
CPC分类号： B01J29/70 , B01J29/049 , C01B33/38
摘要： There is provided a crystalline oxide material with a characteristic X-ray diffraction pattern. This material is a layered material, designated MCM-39. This layered material may be swollen, and the swollen material may be pillared.
摘要翻译： 提供具有特征X射线衍射图案的结晶氧化物材料。 该材料是分层材料，命名为MCM-39。 这种层状材料可能膨胀，并且膨胀的材料可能被支撑。
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公开(公告)号：US5258569A
公开(公告)日：1993-11-02
申请号：US929550
申请日：1992-08-13
IPC分类号： C07C2/58
CPC分类号： B01J29/049 , C07C2/58 , C07C2521/04 , C07C2529/70
摘要： The alkylation of isoparaffin with olefin to provide alkylate is carried out in the presence of, as catalyst, MCM-36.
摘要翻译： 异烯烃与烯烃的烷基化以提供烷基化物在作为催化剂MCM-36的存在下进行。
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公开(公告)号：US5211934A
公开(公告)日：1993-05-18
申请号：US834452
申请日：1992-02-12
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16
CPC分类号： B01J29/82 , B01D53/8628 , B01J20/16 , B01J29/0308 , B01J29/04 , B01J29/041 , B01J29/40 , B01J29/70 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： There is provided a method for synthesizing a new synthetic composition of ultra-large pore crystalline material which can be used as a sorbent or catalyst component for conversion of organic and inorganic compounds. The crystalline material product of this method exhibits unusually large sorption capacity demonstrated by its benzene adsorption capacity of greater than about 15 grams benzene/100 grams at 50 torr and 25.degree. C. This material may have a hexagonal electron diffraction pattern that can be indexed with a d.sub.100 value greater than about 18 Angstom Units and a hexagonal arrangement of uniformly sized pores with a maximum perpendicular cross section of at least about 13 Angstrom Units. The reaction mixture for preparing this material contains a hydrolyzable source of alumina such as aluminum (isopropoxide).sub.2 acetoacetic ester chelate, and a hydrolyzable source of silica, such as tetraethylorthosilicate.
摘要翻译： 提供了一种用于合成可用作有机和无机化合物转化的吸附剂或催化剂组分的超大孔结晶材料的新合成组合物的方法。 该方法的结晶材料产品表现出异常大的吸附能力，其在50托和25℃下苯吸附能力大于约15克苯/ 100克。该材料可具有六角形电子衍射图，其可以用 大于约18埃单位的d100值和具有至少约13埃单位的最大垂直横截面的均匀尺寸孔的六边形排列。 用于制备该材料的反应混合物含有可水解的氧化铝源，例如铝（异丙醇）二乙酰乙酸酯螯合物，以及可水解的二氧化硅源，例如原硅酸四乙酯。
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公开(公告)号：US5108725A
公开(公告)日：1992-04-28
申请号：US625238
申请日：1990-12-10
申请人： Jeffrey S. Beck , Cynthia T. Chu , Ivy D. Johnson , Charles T. Kresge , Michael E. Leonowicz , Wieslaw J. Roth , James C. Vartuli
发明人： Jeffrey S. Beck , Cynthia T. Chu , Ivy D. Johnson , Charles T. Kresge , Michael E. Leonowicz , Wieslaw J. Roth , James C. Vartuli
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16
CPC分类号： B01J29/0308 , B01D53/8628 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/12 , B01J20/18 , B01J29/04 , B01J29/041 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42 , Y10S423/30
摘要： This invention relates to a method for synthesizing a new synthetic composition of ultra-large pore crystalline material which can be used as a sorbent or catalyst component for conversion of organic and inorganic compounds. The crystalline material product of this method exhibits unusually large sorption capacity demonstrated by its benzene adsorption capacity of greater than about 15 grams benzene/100 grams at 50 torr and 25.degree. C., a hexagonal electron diffraction pattern that can be indexed with a d.sub.100 value greater than about 18 Angstrom Units and a hexagonal arrangement of uniformly sized pores with a maximum perpendicular cross section of at least about 13 Angstrom units.
摘要翻译： 本发明涉及一种用于合成可用作有机和无机化合物转化的吸附剂或催化剂组分的超大孔结晶材料的新合成组合物的方法。 该方法的结晶材料产品显示出异常大的吸附能力，其吸附能力在50托和25℃时苯吸附量大于约15克苯/ 100克，可以用d100值指数的六方电子衍射图 大于约18埃单位和具有至少约13埃单位的最大垂直截面的均匀尺寸孔的六边形排列。
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公开(公告)号：US4477590A
公开(公告)日：1984-10-16
申请号：US525778
申请日：1983-08-24
CPC分类号： B01J23/6565 , C10G35/09
摘要： There is provided, in accordance with the present invention, a catalyst composition made up of a mixture of two components, one component comprising a minor proportion of platinum and rhenium on a support and the second component comprising a minor proportion of iridium and rhenium on a separate support. A process for reforming a charge stock, such as naphtha, utilizing such catalyst is also provided.
摘要翻译： 根据本发明，提供了由两种组分的混合物组成的催化剂组合物，一种在载体上包含少量铂和铼的组分，第二组分包含少量的铱和铼 单独支持。 还提供了利用这种催化剂重整电荷原料如石脑油的方法。
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公开(公告)号：US6054052A
公开(公告)日：2000-04-25
申请号：US572823
申请日：1995-12-14
CPC分类号： B01J20/186 , B01D15/00 , B01D15/34 , Y02W10/37
摘要： Incorporation of zirconium, nickel and/or copper into M41S results in selective sorption of bulky organic molecules. Zirconium, nickel and/or copper may be incorporated into M41S by exchange or impregnation.
摘要翻译： 将锆，镍和/或铜掺入M41S导致大量有机分子的选择性吸附。 锆，镍和/或铜可以通过交换或浸渍加入到M41S中。
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公开(公告)号：US5366945A
公开(公告)日：1994-11-22
申请号：US995091
申请日：1992-12-22
IPC分类号： B01J27/188 , B01J29/03 , B01J29/04 , C07C2/62 , B01J21/02 , B01J27/185 , B01J29/06
CPC分类号： B01J29/0341 , B01J27/188 , B01J29/041 , B01J29/043 , C07C2/62 , B01J29/0308 , C07C2527/188 , Y02P20/588
摘要： There is provided a catalyst comprising a heteropoly acid, such as phosphotungstic acid, supported on a mesoporous crystalline material, such as M41S. A particular form of this M41S support is designated as MCM-41. There is also provided a method for preparing this catalyst by impregnating the heteropoly acid on the support. There is also provided a process for using this catalyst to catalyze acid catalyzed reactions, such as the isomerization of paraffins and the alkylation of aromatics.
摘要翻译： 提供了一种催化剂，其包含负载在介孔结晶材料如M41S上的杂多酸如磷钨酸。 该M41S支持的特定形式被指定为MCM-41。 还提供了通过将杂多酸浸渍在载体上来制备该催化剂的方法。 还提供了一种使用该催化剂催化酸催化反应的方法，例如链烷烃的异构化和芳族化合物的烷基化。
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公开(公告)号：US5300277A
公开(公告)日：1994-04-05
申请号：US964235
申请日：1992-10-21
申请人： Charles T. Kresge , Wielsaw J. Roth
发明人： Charles T. Kresge , Wielsaw J. Roth
IPC分类号： B01D53/86 , B01J20/02 , B01J20/06 , B01J29/03 , B01J29/035 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , C01B33/20 , C01B33/26
CPC分类号： B01J29/83 , B01D53/8628 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/12 , B01J20/18 , B01J20/223 , B01J29/0308 , B01J29/035 , B01J29/04 , B01J29/041 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： This invention relates to an improvement in the method for synthesis of a new synthetic composition of porous crystalline material. The new crystalline material exhibits a large sorption capacity demonstrated by its benzene adsorption capacity of greater than about 10 grams benzene/100 grams at 50 torr and 25.degree. C. and a particular, unique X-ray diffraction pattern.
摘要翻译： 本发明涉及合成多孔结晶材料的新合成组合物的方法的改进。 新的结晶材料表现出大的吸附能力，其吸附能力在50乇和25摄氏度下大于约10克苯/ 100克，具有独特的X射线衍射图。
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