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    PAPER COATED WITH A FUNCTIONAL POLYOLEFIN FILM
    21.
    发明公开
    PAPER COATED WITH A FUNCTIONAL POLYOLEFIN FILM 审中-公开

    公开(公告)号：US20230151549A1

    公开(公告)日：2023-05-18

    申请号：US17917684

    申请日：2021-04-15

    Applicant: Dow Global Technologies LLC

    Inventor： Alan M. Piwowar ,  Ray E. Drumright ,  Christina N. Ellison ,  David L. Malotky ,  Jonathan F. Mason ,  Hari Katepalli ,  Luqing Qi ,  Houxiang Tang ,  Robert R. Bills

    IPC: D21H17/37 ,  D21H19/20 ,  D21H21/16 ,  D21H21/02

    CPC classification number: D21H17/37 ,  D21H19/20 ,  D21H21/16 ,  D21H21/02

    Abstract: The present invention relates to an article and a method for its preparation; the article comprises a cured polymeric film superposing paper or paperboard. The polymeric film is derived from a dispersion which comprises:



    a) a dispersant which is a copolymer with an acid value of 130 or less, comprising structural units of ethylene and a carboxylic acid monomer, wherein the copolymer has a melt flow index in the range of from 50 to 2000 g/10 min at 190° C./2.16 kg; wherein the weight-to-weight ratio of structural units of ethylene to carboxylic acid monomer is in the range of from 95:5 to 70:30; and wherein the dispersant has a concentration in the range of from 9 to 50 weight percent based on the weight of polymer solids in the dispersion;
    b) a base polymer comprising non-functionalized ethylene-co-alkene copolymers, wherein the weight-to-weight ratio of the structural units of ethylene to alkene is in the range of from 99.8:0.2 to 50:50; and
    c) a neutralizing agent which is a hard base and excludes an organic base having a boiling point of less than 250° C.; wherein the concentration of the neutralizing agent is sufficient to neutralize at least half of the carboxylic acid groups associated with the dispersion composition.




    The article of the present invention is useful as a barrier to a wide range of hydrophobic and hydrophilic materials.

    Aqueous based blend composition and method of producing the same
    22.
    发明授权
    Aqueous based blend composition and method of producing the same 有权

    公开(公告)号：US11485872B2

    公开(公告)日：2022-11-01

    申请号：US14404675

    申请日：2013-05-16

    Applicant: Dow Global Technologies LLC ,  Rohm and Haas Company

    Inventor： Denise Lindenmuth ,  Joceyln Gruver ,  Ann R. Hermes ,  Ray E. Drumright

    IPC: C09D133/08 ,  C08L23/02 ,  C09J123/10 ,  C08L23/10 ,  C08L33/10 ,  C08J3/05 ,  C09D123/12 ,  C08L23/08

    Abstract: The instant invention is an aqueous based blend composition and method of producing the same. The aqueous based blend composition comprises (a) an aqueous polyolefin dispersion comprising the melt blending product of one or more base polymers and one or more stabilizing agents in the presence of water and optionally one or more neutralizing agents, wherein the polyolefin dispersion has an average volume particle size diameter in the range of from 400 to 1500 nm; and a pH range from 8 to 11; and (b) an acrylic emulsion acrylic solids having an average weight particle size diameter in the range of from 75 to 450 nm; an acid level in the range of from 0.25 to 5 percent by weight of acid monomers based on the weight of the acrylic monomer, and a weight average molecular weight in the range of from 200,000 to 5,000,000 g/mole, and a glass transition temperature (Tg) in the range of from 7 to 100° C., wherein said acrylic emulsion has a pH in the range of from 7 to 11; wherein said aqueous based blend composition has a solid content in the range of from 15 to 70 percent by weight of solids, based on the weight of the aqueous based blend composition, and a pH in the range of from 7 to 11.

    Water borne polyolefin dispersion coatings, and methods of making
    24.
    发明授权
    Water borne polyolefin dispersion coatings, and methods of making 有权

    公开(公告)号：US10221327B2

    公开(公告)日：2019-03-05

    申请号：US15064902

    申请日：2016-03-09

    Applicant: Dow Global Technologies LLC

    Inventor： Ray E. Drumright ,  Bernhard Kainz ,  Richard A. Lundgard ,  Cynthia Stants ,  Houxiang Tang ,  Jeffrey Wilbur

    IPC: C09D5/00 ,  C09D123/12 ,  C08L23/08 ,  C08L23/14 ,  C09D123/08 ,  C09D123/10 ,  C09J123/08 ,  C09J123/10 ,  C08L51/06 ,  C09D7/48 ,  C09D7/65 ,  C08K5/134

    Abstract: The present invention provides aqueous polyolefin dispersion compositions for use in metal coatings, such as can coatings, comprising one or more polyolefin base polymer, one or more at least partially neutralized olefinic stabilizing agent having an acid number (AN) of from 80 to 250, preferably, a polyolefin stabilizing agent, such as an olefin-carboxylic acid copolymer or a blend of two such polymers, an optional coupling agent having an acid number (AN) of from 10 to 70 and a melt index of from 500 to 5,000,000 grams of polymer melt passing in 10 minutes through a heated syringe or cylinder at 190° C. with a plunger loaded with 2.16 kg, preferably, a polymer, and a hindered phenolic antioxidant containing an ester linkage dispersed in the polyolefin dispersion composition. The hindered phenolic antioxidant containing an ester linkage can be masterbatched with a polyolefin base polymer, polyolefin stabilizing agent or a coupling agent which is a polymer, melt mixed with the remaining polyolefin composition and then dispersed with aqueous media and a neutralizing agent to form the aqueous dispersion.

    WATER BORNE POLYOLEFIN DISPERSION COATINGS, AND METHODS OF MAKING
    25.
    发明申请
    WATER BORNE POLYOLEFIN DISPERSION COATINGS, AND METHODS OF MAKING 审中-公开
    水性聚苯乙烯分散涂料及其制备方法

    公开(公告)号：US20160280951A1

    公开(公告)日：2016-09-29

    申请号：US15064902

    申请日：2016-03-09

    Applicant: Dow Global Technologies LLC

    Inventor： Ray E. Drumright ,  Bernhard Kainz ,  Richard A. Lundgard ,  Cynthia Stants ,  Houxiang Tang ,  Jeffrey Wilbur

    IPC: C09D123/12 ,  C09D5/00 ,  C09D7/12 ,  C09D123/08

    CPC classification number: C09D123/12 ,  C08K5/1345 ,  C08L23/0815 ,  C08L23/142 ,  C08L51/06 ,  C08L2201/08 ,  C08L2201/54 ,  C08L2205/025 ,  C08L2205/03 ,  C09D5/00 ,  C09D7/48 ,  C09D7/65 ,  C09D123/0815 ,  C09D123/10 ,  C09J123/0815 ,  C09J123/10 ,  C08F210/16 ,  C08F210/14 ,  C08F210/06

    Abstract: The present invention provides aqueous polyolefin dispersion compositions for use in metal coatings, such as can coatings, comprising one or more polyolefin base polymer, one or more at least partially neutralized olefinic stabilizing agent having an acid number (AN) of from 80 to 250, preferably, a polyolefin stabilizing agent, such as an olefin-carboxylic acid copolymer or a blend of two such polymers, an optional coupling agent having an acid number (AN) of from 10 to 70 and a melt index of from 500 to 5,000,000 grams of polymer melt passing in 10 minutes through a heated syringe or cylinder at 190° C. with a plunger loaded with 2.16 kg, preferably, a polymer, and a hindered phenolic antioxidant containing an ester linkage dispersed in the polyolefin dispersion composition. The hindered phenolic antioxidant containing an ester linkage can be masterbatched with a polyolefin base polymer, polyolefin stabilizing agent or a coupling agent which is a polymer, melt mixed with the remaining polyolefin composition and then dispersed with aqueous media and a neutralizing agent to form the aqueous dispersion.

    Abstract translation: 本发明提供用于金属涂层（例如罐涂层）的含水聚烯烃分散体组合物，其包含一种或多种聚烯烃基聚合物，一种或多种至少部分中和的具有80-250的酸值（AN）的烯属稳定剂， 优选聚烯烃稳定剂，例如烯烃 - 羧酸共聚物或两种这样的聚合物的共混物，任选的偶联剂，其酸值（AN）为10至70，熔体指数为500至500万克 聚合物熔体在10分钟内通过加热的注射器或圆筒在190℃下用负载有2.16kg的柱塞，优选聚合物和含有分散在聚烯烃分散体组合物中的酯键的受阻酚抗氧化剂。 含有酯键的受阻酚抗氧化剂可以用聚烯烃基聚合物，聚烯烃稳定剂或作为聚合物的偶联剂与剩余的聚烯烃组合物熔融混合，然后用水介质和中和剂分散以形成水性 分散。

    EPOXY RESIN COMPOSITIONS, METHODS OF MAKING SAME, AND ARTICLES THEREOF
    27.
    发明申请
    EPOXY RESIN COMPOSITIONS, METHODS OF MAKING SAME, AND ARTICLES THEREOF 审中-公开
    环氧树脂组合物，其制备方法及其制品

    公开(公告)号：US20140179828A1

    公开(公告)日：2014-06-26

    申请号：US14132078

    申请日：2013-12-18

    Applicant: Dow Global Technologies LLC

    Inventor： Robert E. Hefner, JR. ,  Ray E. Drumright ,  Jinghang Wu

    IPC: C08G59/00 ,  C09D163/00

    CPC classification number: C09D163/00 ,  C08G59/24 ,  C08G59/50

    Abstract: Epoxy resins comprising a diglycidyl ether of Formula 1 as defined herein are described. The diglycidyl ether contains a cycloaliphatic ring of 3-5 carbon atoms. The epoxy resins are made by a method comprising the steps of: (a) forming a reaction mixture comprising a diol of Formula 3 as defined herein, an epihalohydrin, a phase transfer catalyst, and optionally an organic solvent; (b) contacting a basic acting substance and water with the reaction mixture of step (a); (c) washing the mixture of step (b) with an aqueous solvent to substantially remove salts; and (d) isolating the epoxy resin. Curable and cured compositions comprising the epoxy resins are also disclosed. The epoxy resins have increased glass transition temperatures and reduced viscosity compared to epoxy resins derived from cyclohexanedimethanol.

    Abstract translation: 描述了包含本文所定义的式1的二缩水甘油醚的环氧树脂。 二缩水甘油醚包含3-5个碳原子的脂环族环。 环氧树脂通过包括以下步骤的方法制备：（a）形成包含如本文所定义的式3的二醇，表卤代醇，相转移催化剂和任选的有机溶剂的反应混合物; （b）将碱性作用物质和水与步骤（a）的反应混合物接触; （c）用水性溶剂洗涤步骤（b）的混合物以基本上除去盐; 和（d）分离环氧树脂。 还公开了包含环氧树脂的可固化和固化的组合物。 与衍生自环己烷二甲醇的环氧树脂相比，环氧树脂具有增加的玻璃化转变温度和降低的粘度。

    COATED CONTAINER DEVICE, METHOD OF MAKING THE SAME
    29.
    发明申请
    COATED CONTAINER DEVICE, METHOD OF MAKING THE SAME 有权

    公开(公告)号：US20220227536A1

    公开(公告)日：2022-07-21

    申请号：US17713182

    申请日：2022-04-04

    Applicant: Dow Global Technologies LLC

    Inventor： Bernhard Kainz ,  Richard A. Lundgard ,  David L. Malotky ,  Jodi M. Mecca ,  Charles F. Diehl ,  Ray E. Drumright

    IPC: B65D25/14

    Abstract: The instant invention provides a coated container device, and method of making the same. The coated container device according to the instant invention comprises: (1) a metal substrate; and (2) one or more crosslinked coating layers associated with the metal substrate, wherein the one or more crosslinked coating layers are derived from the application of one or more aqueous dispersions to at least one surface of the metal substrate, and wherein the one or more aqueous dispersion comprise: (a) one or more a base polymer; (b) one or more a stabilizing agent; (c) optionally one or more neutralizing agents, (d) one or more crosslinking agents; and (e) water.

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