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    Process to polymerize AB-PBO monomer phosphate salts
    22.
    发明授权
    Process to polymerize AB-PBO monomer phosphate salts 失效
    聚合AB-PBO单体磷酸盐的方法

    公开(公告)号：US5210171A

    公开(公告)日：1993-05-11

    申请号：US546597

    申请日：1990-06-29

    申请人： William J. Harris ,  Zenon Lysenko ,  Carl W. Hurtig

    发明人： William J. Harris ,  Zenon Lysenko ,  Carl W. Hurtig

    IPC分类号： C07C227/06 ,  C08G73/22

    CPC分类号： C08G73/22 ,  C07C227/06

    摘要： AB-polybenzoxazole monomer, such as 3-amino-4-hydroxybenzoic acid, can be synthesized in high yields from a hydroxy-benzoic acid or related compound in a three-step process of (1) nitration, (2) hydrolysis of the ester, and (3) reduction of the nitro moiety. The monomer is conveniently recovered as a phosphate salt in high purity by precipitating and recrystallizing from a phosphoric acid solution. The monomer may be polymerized in high concentrations in polyphosphoric acid containing high levels of P.sub.2 O.sub.5 to yield a high molecular weight polymer without dehydrohalogenation.

    摘要翻译： 可以在（1）硝化的三步法中，从羟基 - 苯甲酸或相关化合物以高产率合成AB-聚苯并恶唑单体，例如3-氨基-4-羟基苯甲酸，（2）酯的水解 ，和（3）还原硝基部分。 通过从磷酸溶液中沉淀和重结晶，可以方便地将单体作为高纯度的磷酸盐回收。 单体可以在含有高含量的P 2 O 5的多磷酸中以高浓度聚合，得到高分子量聚合物，而无需脱卤化氢。

    Electrocatalytic method for producing dihydroxybenzophenones
    23.
    发明授权
    Electrocatalytic method for producing dihydroxybenzophenones 失效
    用于制备二羟基二苯甲酮的电催化方法

    公开(公告)号：US4624758A

    公开(公告)日：1986-11-25

    申请号：US816502

    申请日：1986-01-06

    申请人： Zenon Lysenko ,  Eric E. Bancroft

    发明人： Zenon Lysenko ,  Eric E. Bancroft

    IPC分类号： C25B3/02 ,  C07B29/06 ,  C07C49/64

    CPC分类号： C25B3/02

    摘要： A method for producing dihydroxybenzophenones by the electrocatalytic oxidation of bis(4-hydroxyphenyl) methanes, or the quinone methide intermediate, with 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ). Spent oxidant, in the form of DDQH.sub.2, may be recycled and electrochemically regenerated to active DDQ oxidant.

    摘要翻译： 通过双（4-羟基苯基）甲烷或醌甲基化物中间体与2,3-二氯-5,6-二氰基-1,4-苯醌（DDQ）的电催化氧化制备二羟基二苯甲酮的方法。 以DDQH2形式的废氧化剂可以循环使用并电化学再生成活性DDQ氧化剂。

    MOISTURE RESISTANT PHOTOVOLTAIC DEVICES WITH ELASTOMERIC, POLYSILOXANE PROTECTION LAYER
    24.
    发明申请
    MOISTURE RESISTANT PHOTOVOLTAIC DEVICES WITH ELASTOMERIC, POLYSILOXANE PROTECTION LAYER 审中-公开
    具有弹性体，多晶硅保护层的防潮光伏器件

    公开(公告)号：US20110162705A1

    公开(公告)日：2011-07-07

    申请号：US12974643

    申请日：2010-12-21

    申请人： Paul J. Popa ,  Michelle L. Boven ,  Zenon Lysenko ,  Michael E. Mills ,  Leonardo C. Lopez

    发明人： Paul J. Popa ,  Michelle L. Boven ,  Zenon Lysenko ,  Michael E. Mills ,  Leonardo C. Lopez

    IPC分类号： H01L31/0216

    CPC分类号： H01L31/0749 ,  H01L31/048 ,  Y02E10/541

    摘要： Improved protection systems for CIGS-based microelectronic devices of the type incorporating electric conductor(s) such as an electronic collection grid. In one aspect, the present invention relates to a photovoltaic device having a light incident surface and a backside surface. The device includes a chalcogenide-containing photovoltaic layer comprising at least one of copper, indium and/or gallium. A transparent conductive layer is interposed between the photovoltaic layer and the light incident surface, wherein the transparent conductive layer is electrically coupled to the photovoltaic layer. An electronic collection grid is electrically coupled to the transparent conductive layer and overlying at least a portion of the transparent conductive layer. An elastomeric structure having a light incident surface, said structure overlying at least portions of the electronic collection grid and the transparent conductive layer in a manner such that the light incident surface of the elastomeric structure is spaced apart from a major portion of the conductor, and wherein the elastomeric structure comprises an elastomeric siloxane polymer having a WVTR of at least 0.1 g/m2-day. An optional protective barrier overlies the elastomeric structure. The protection systems of the invention incorporate elastomers with water vapor transmission rates that are atypically high in the context of CIGS-based devices.

    摘要翻译： 改进了包含电导体（例如电子收集网格）类型的基于CIGS的微电子器件的保护系统。 一方面，本发明涉及具有光入射面和背面的光电器件。 该装置包括含硫族化物的光伏层，其包含铜，铟和/或镓中的至少一种。 透明导电层介于光伏层和光入射表面之间，其中透明导电层电耦合到光伏层。 电子收集栅格电耦合到透明导电层并且覆盖透明导电层的至少一部分。 具有光入射表面的弹性体结构，所述结构以使得弹性体结构的光入射表面与导体的主要部分间隔开的方式覆盖电子收集栅格和透明导电层的至少一部分，以及 其中所述弹性体结构包含具有至少0.1g / m 2·天的WVTR的弹性体硅氧烷聚合物。 可选的保护屏障覆盖弹性体结构。 本发明的保护系统结合了在基于CIGS的设备的背景下具有非常高的水蒸汽透过率的弹性体。

    Integrate chemical processes for industrial utilization of seed oils
    25.
    发明授权
    Integrate chemical processes for industrial utilization of seed oils 有权
    整合化学工业用于种子油的工业利用

    公开(公告)号：US07576227B2

    公开(公告)日：2009-08-18

    申请号：US10508805

    申请日：2003-04-17

    申请人： Zenon Lysenko ,  Bob R. Maughon ,  Josef Bicerano ,  Christopher P. Christenson ,  Clark H. Cummins ,  Marvin L. Dettlof ,  Jerry E. White

    发明人： Zenon Lysenko ,  Bob R. Maughon ,  Josef Bicerano ,  Christopher P. Christenson ,  Clark H. Cummins ,  Marvin L. Dettlof ,  Jerry E. White

    IPC分类号： C07C57/00 ,  C07C53/00

    CPC分类号： C07D303/42 ,  C07C67/31 ,  C07C67/333 ,  C07C67/347 ,  C07C67/56 ,  C07C69/533 ,  C07C227/08 ,  C07C227/18 ,  C07C229/08 ,  Y02P20/125 ,  C07C69/716 ,  C07C69/675

    摘要： Integrated processes of preparing industrial chemicals starting from seed oil feedstock compositions containing one or more unsaturated fatty acids or unsaturated fatty acid esters, which are essentially free of metathesis catalyst poisons, particularly hydroperoxides; metathesis of the feedstock composition with a lower olefin, such as ethylene, to form a reduced chain olefin, preferably, a reduced chain α-olefin, and a reduced chain unsaturated acid or ester, preferably, a reduced chain α,ω-unsaturated acid or ester. The reduced chain unsaturated acid or ester may be (trans)esterified to form a polyester polyolefin, which may be epoxidized to form a polyester polyepoxide. The reduced chain unsaturated acid or ester may be hydroformylated with reduction to produce an α,ω-hydroxy acid or α,ω-hydroxy ester, which may be (trans)esterified with a polyol to form an α,ωpolyester polyol. Alternatively, the reduced chain unsaturated acid or ester may be hydroformylated with reductive amination to produce an α,ω-amino acid or α,ω-amino ester, which may be (trans)esterified to form an α,ωpolyester polyamine.

    摘要翻译： 从含有一种或多种不饱和脂肪酸或不饱和脂肪酸酯的种子油原料组合物制备工业化学品的综合方法，其基本上不含复分解催化剂毒物，特别是氢过氧化物; 原料组合物与低级烯烃如乙烯的复分解以形成还原链烯烃，优选还原链的α-烯烃和还原链不饱和酸或酯，优选还原链的α，ω-不饱和酸 或酯。 还原链不饱和酸或酯可以（反式）酯化以形成聚酯聚烯烃，其可以被环氧化以形成聚酯多环氧化物。 还原链不饱和酸或酯可以通过还原加氢甲酰化以产生α，ω-羟基酸或α，ω-羟基酯，其可以与多元醇反应形成α，ω-聚酯多元醇。 或者，还原链不饱和酸或酯可以通过还原胺化加氢甲酰化以产生α，ω-氨基酸或α，ω-氨基酯，其可以（反式）酯化形成α，ω-聚酯多胺。

    Process for the synthesis of unsaturated alcohols
    27.
    发明授权
    Process for the synthesis of unsaturated alcohols 有权
    合成不饱和醇的方法

    公开(公告)号：US07176336B2

    公开(公告)日：2007-02-13

    申请号：US10940403

    申请日：2004-09-14

    申请人： Bob R. Maughon ,  Kenneth A. Burdett ,  Zenon Lysenko

    发明人： Bob R. Maughon ,  Kenneth A. Burdett ,  Zenon Lysenko

    IPC分类号： C07C29/00 ,  C07C33/025 ,  C07C33/03

    CPC分类号： C07C29/095 ,  C07C67/293 ,  C07C67/333 ,  C07C67/475 ,  C07C69/007 ,  C07C69/533 ,  C07C69/593 ,  C07C69/145 ,  C07C33/03 ,  C07C33/035

    摘要： A process of preparing an unsaturated alcohol (olefin alcohol), such as, a homo-allylic mono-alcohol or homo-allylic polyol, involving protecting a hydroxy-substituted unsaturated fatty acid or fatty acid ester, such as methyl ricinoleate, derived from a seed oil, to form a hydroxy-protected unsaturated fatty acid or fatty acid ester; homo-metathesizing or cross-metathesizing the hydroxy-protected unsaturated fatty acid or fatty acid ester to produce a product mixture containing a hydroxy-protected unsaturated metathesis product; and deprotecting the hydroxy-protected unsaturated metathesis product under conditions sufficient to prepare the unsaturated alcohol. Preferably, methyl ricinoleate is converted by cross-metathesis or homo-metathesis into the homo-allylic mono-alcohol 1-decene-4-ol or the homo-allylic polyol 9-octadecene-7,12-diol, respectively.

    摘要翻译： 一种制备不饱和醇（烯烃）的方法，例如均聚单醇或均烯基多元醇，包括保护羟基取代的不饱和脂肪酸或脂肪酸酯如蓖麻油酸甲酯，其衍生自 种子油，形成羟基保护的不饱和脂肪酸或脂肪酸酯; 羟基保护的不饱和脂肪酸或脂肪酸酯的均匀化或交叉变性以产生含有羟基保护的非饱和复分解产物的产物混合物; 并在足以制备不饱和醇的条件下脱保护羟基保护的不饱和复分解产物。 优选地，蓖麻油酸甲酯通过交叉复分解或均一复分解转化成均相烯醇1-癸烯-4-醇或均烯基多元醇9-十八碳烯-7,12-二醇。

    Process for the preparation of diaminoresorcinol
    29.
    发明授权
    Process for the preparation of diaminoresorcinol 失效
    制备二氨基间苯二酚的方法

    公开(公告)号：US5399768A

    公开(公告)日：1995-03-21

    申请号：US173452

    申请日：1993-12-23

    申请人： Zenon Lysenko ,  Richard G. Pews

    发明人： Zenon Lysenko ,  Richard G. Pews

    IPC分类号： C07C213/02 ,  C07C209/18

    CPC分类号： C07C213/02

    摘要： The present invention relates to a method of preparing 4,6-diaminoresorcinol from 1,2-dichloro-3,5-dinitrobenzene comprising the steps of:(a) contacting 1,2-dichloro-3,5-dinitrobenzene with a hydroperoxide in the presence of anhydrous base to form 2,3-dichloro-4,6-dinitrophenol;(b) contacting 2,3-dichloro-4,6-dinitrophenol with a hydroxy-containing compound to form 2-chloro-4,6-dinitroresorcinol; and(c) converting 2-chloro-4,6-dinitroresorcinol to 4,6-diaminoresorcinol, which is isolated as a salt or other stabilized form thereof,

    摘要翻译： 本发明涉及从1,2-二氯-3,5-二硝基苯制备4,6-二氨基间苯二酚的方法，包括以下步骤：（a）使1,2-二氯-3,5-二硝基苯与氢过氧化物接触 无水碱的存在形成2,3-二氯-4,6-二硝基苯酚; （b）使2,3-二氯-4,6-二硝基苯酚与含羟基化合物接触以形成2-氯-4,6-二硝基间苯二酚; 和（c）将2-氯-4,6-二硝基间苯二酚转化为4,6-二氨基间苯二酚，其以盐或其它稳定形式分离，