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    Azide crosslinked and physically crosslinked polymers for membrane separation
    32.
    发明授权
    Azide crosslinked and physically crosslinked polymers for membrane separation 有权
    用于膜分离的叠氮化物交联和物理交联的聚合物

    公开(公告)号：US09174175B2

    公开(公告)日：2015-11-03

    申请号：US14345343

    申请日：2012-09-20

    Applicant: DOW GLOBAL TECHNOLOGIES LLC

    Inventor： Scott T. Matteucci ,  Clark H. Cummins ,  William J. Kruper ,  Harry Craig Silvis

    IPC: B01D71/58 ,  B01D53/22 ,  C08K5/28 ,  C08K5/43 ,  C08L77/12 ,  C08L79/08

    CPC classification number: B01D71/58 ,  B01D53/22 ,  B01D2053/221 ,  B01D2257/504 ,  C08K5/28 ,  C08K5/43 ,  C08L77/12 ,  C08L79/08

    Abstract: The present invention appreciates that compounds comprising ester linkages and nitrogen-containing moieties that are at least divalent (e.g., urea, urethane, amide, etc.) can be crosslinked with azides to form membranes that are resistant to CO2 plasticization, that are selective for acid gases relative to nonpolar gases such as hydrocarbons, and that have high acid gas flux characteristics. The resultant membranes have stable structure and stable separation properties at higher temperatures and pressures. The membranes are compatible with many industrial processes in which polar gases are separated from nopolar gases. In an exemplary mode of practice, the membranes can be used to separate acid gases from the hydrocarbon gases in natural or non-acid gas components of flue gas mixtures (e.g., N2, O2, etc.).

    Abstract translation: 本发明认识到，含有至少二价的酯键和含氮部分的化合物（例如尿素，氨基甲酸酯，酰胺等）可以与叠氮化物交联以形成耐二氧化碳增塑的膜，其对于 酸性气体相对于非极性气体如烃类，具有较高的酸性气体通量特性。 所得膜在较高的温度和压力下具有稳定的结构和稳定的分离性能。 该膜与许多工业过程兼容，其中极性气体与非极性气体分离。 在示例性实践模式中，膜可以用于将烟气混合物（例如，N 2，O 2等）的天然或非酸性气体组分中的烃气体分离出酸性气体。

    RADIATION CURED MEMBRANES DERIVED FROM POLYMERS THAT ARE CO-REACTIVE WITH AZIDE CROSSLINKING AGENT(S)
    34.
    发明申请
    RADIATION CURED MEMBRANES DERIVED FROM POLYMERS THAT ARE CO-REACTIVE WITH AZIDE CROSSLINKING AGENT(S) 有权
    从与AZIDE交联剂反应的聚合物衍生的辐射固化的膜（S）

    公开(公告)号：US20150218330A1

    公开(公告)日：2015-08-06

    申请号：US14422008

    申请日：2013-09-18

    Applicant: Dow Global Technologies LLC

    Inventor： Scott T. Matteucci ,  Junqiang Liu ,  Ahmad Madkour ,  William J. Harris

    IPC: C08J7/12 ,  B01D53/22 ,  B01D71/64 ,  C08J3/24 ,  B01D67/00

    CPC classification number: C08J7/123 ,  B01D53/228 ,  B01D67/0006 ,  B01D67/0013 ,  B01D71/58 ,  B01D71/64 ,  B01D2323/08 ,  B01D2323/30 ,  B01D2323/34 ,  B01D2323/345 ,  C08J3/24 ,  C08J2375/04 ,  C08J2375/06

    Abstract: The present invention appreciates that compounds comprising nitrogen-containing moieties that are at least divalent (e.g., urea, urethane, amide, etc.) can be reacted with azides using at least radiation energy to initiate the reaction between at least a portion of the compounds and the azides to form membranes that have surprisingly high selectivities for acid gases relative to nonpolar gases such as hydrocarbons. The membranes are also resistant to CO2 plasticization and have high acid gas flux characteristics. The resultant membranes can be extremely thin (e.g., 10 micrometers or less), which promotes high permeability for the acid gas and can translate into high productivity on a scaled-up, industrial level.

    Abstract translation: 本发明意识到包含至少二价的含氮部分的化合物（例如尿素，氨基甲酸酯，酰胺等）可以与叠氮化物反应，至少使用辐射能来引发至少一部分化合物之间的反应 和叠氮化物以形成相对于非极性气体如烃类具有令人惊奇的高选择性的酸性气体的膜。 膜也耐二氧化碳增塑，具有较高的酸性气体通量特性。 所得到的膜可以非常薄（例如10微米或更小），其促进酸性气体的高渗透性，并且可以在放大的工业水平上转化为高生产率。

    HIGH POROSITY MESOPOROUS SILICEOUS STRUCTURES
    36.
    发明申请
    HIGH POROSITY MESOPOROUS SILICEOUS STRUCTURES 有权
    高密度多孔硅质结构

    公开(公告)号：US20140295165A1

    公开(公告)日：2014-10-02

    申请号：US14352423

    申请日：2012-11-19

    Applicant: Dow Global Technologies LLC

    Inventor： Beata A. Kilos ,  Cathy L. Tway ,  Scott T. Matteucci ,  Christopher J. Tucker ,  Anne M. Kelly-Rowley

    IPC: C01B33/12

    CPC classification number: C01B33/128 ,  C01B33/12 ,  C01B37/02 ,  Y10T428/249921

    Abstract: A process comprising: A) contacting one or more of sources of silicon oxide, selected from water sol-uble.silica sources arid alkali metal silicates, with an aqueous reaction medium, comprising one or more nonionic surfactants and thereby forming mesoporous structures comprising crosslinked silicon oxide units, wherein said cross-linked silicon oxide units have pores of about 1 to about 100 nanometers and wherein the aqueous reaction medium exhibits a pH of about 0 to about 4.0; B) exposing the aqueous reaction medium containing the mesoporous structures to elevated temperatures for a time sufficient to achieve the desired structure and pore size. Preferred water soluble silica sources comprise silicic acid, or po!ysilicic acids, The aqueous reaction, medium is prepared by combining one or more nonionic surfactants and water, theteby forming an aqueous, reaction medium. comprising micelles. Preferably, the aqueous reaction medium further comprises, a. micelle swelling agent capable of swelling micelles formed by the surfactant in the aqueous reaction medium. In one embodiment the process forms structures with struts comprised of crosslinked silicon oxides which connect at least some of the pore forming structures.

    Abstract translation: 一种方法，包括：A）将一种或多种选自水溶性二氧化硅源和碱金属硅酸盐的氧化硅源与含有一种或多种非离子表面活性剂的含水反应介质接触，从而形成包含交联硅 氧化物单元，其中所述交联的氧化硅单元具有约1至约100纳米的孔，并且其中所述水性反应介质的pH为约0至约4.0; B）将含有介孔结构的含水反应介质暴露于升高的温度足以实现所需结构和孔径的时间。 优选的水溶性二氧化硅源包括硅酸或聚硅酸。通过形成水性反应介质，通过组合一种或多种非离子表面活性剂和水来制备含水反应介质。 包括胶束。 优选地，水性反应介质还包含a。 能够在水性反应介质中溶胀由表面活性剂形成的胶束的胶束溶解剂。 在一个实施方案中，该方法形成具有连接至少一些成孔结构的交联氧化硅的支柱的结构。

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