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    Low temperature initiators for improving the rubber phase volume of HIPS formulations
    33.
    发明申请
    Low temperature initiators for improving the rubber phase volume of HIPS formulations 有权
    用于改善HIPS配方橡胶相体积的低温引发剂

    公开(公告)号：US20070100079A1

    公开(公告)日：2007-05-03

    申请号：US11262641

    申请日：2005-10-31

    Applicant: Jose Sosa ,  Shazia Ullah

    Inventor： Jose Sosa ,  Shazia Ullah

    IPC: C08F263/00

    CPC classification number: C08F279/02 ,  C08L51/04 ,  C08L2666/02

    Abstract: Peroxide initiators are disclosed that can be used at lower temperatures during HIPS production. Enhanced formation of graft polymers between polystyrene and polybutadiene (rubber) can be accomplished by using these lower temperature peroxide initiators that have a 1 hour half-life period at one or more temperatures from 95° C. to less than 111° C. during the pre-inversion stage. “Higher” temperature initiators are used during and/or after inversion. The use of such “low” temperature initiators improves polymerization rates and grafting values, while reducing the swell index and the amount of rubber used, thereby producing improved HIPS more rapidly and at a lower cost. Also disclosed are HIPS compositions and products produced by such “low” temperature initiators as well as a method of producing improved HIPS.

    Abstract translation: 公开了可以在HIPS生产期间在较低温度下使用的过氧化物引发剂。 在聚苯乙烯和聚丁二烯（橡胶）之间增强的接枝聚合物的形成可以通过使用这些低温过氧化物引发剂来实现，该引发剂在一个或多个温度从95℃到小于111℃的时间内具有1小时的半衰期 预转换阶段。 在反转期间和/或之后使用“较高”的温度引发剂。 使用这种“低”温度引发剂提高了聚合速率和接枝值，同时降低了溶胀指数和使用的橡胶的量，从而以更低的成本更快速地生产改进的HIPS。 还公开了由这种“低”温度引发剂生产的HIPS组合物和产物以及生产改进的HIPS的方法。

    Preparation of a compound containing cyclic and linear carbonate groups
    34.
    发明授权
    Preparation of a compound containing cyclic and linear carbonate groups 失效
    制备含有环状和直链碳酸酯基团的化合物

    公开(公告)号：US07112633B2

    公开(公告)日：2006-09-26

    申请号：US10486733

    申请日：2002-08-05

    Applicant: Vincent Stone

    Inventor： Vincent Stone

    IPC: C08F263/00 ,  C08F18/12 ,  C07D317/10 ,  C07D493/00

    CPC classification number: C07D317/36

    Abstract: The invention relates to a process for the preparation of compound(s) comprising at least one acrylate or methacrylate group, at least one linear carbonate group and at least one 5-membered cyclic carbonate group. The process comprises (A) a selective ring-opening step and (B) a (meth)acrylation step. The process is environment-friendly and compounds obtained are usable in radiation curable compositions, for example in radiation-curable inks.

    Abstract translation: 本发明涉及一种制备包含至少一种丙烯酸酯或甲基丙烯酸酯基团，至少一个直链碳酸酯基团和至少一个5-元环状碳酸酯基团的化合物的方法。 该方法包括（A）选择性开环步骤和（B）（甲基）丙烯酸酯化步骤。 该方法是环境友好的，并且所获得的化合物可用于可辐射固化组合物，例如在可辐射固化的油墨中。

    Method for producing a modified propylene polymer
    35.
    发明申请
    Method for producing a modified propylene polymer 失效
    改性丙烯聚合物的制造方法

    公开(公告)号：US20060148995A1

    公开(公告)日：2006-07-06

    申请号：US11270453

    申请日：2005-11-10

    Applicant: Hiroyoshi Nakajima ,  Shuichi Kimata ,  Susumu Kanzaki

    Inventor： Hiroyoshi Nakajima ,  Shuichi Kimata ,  Susumu Kanzaki

    IPC: C08F263/00

    CPC classification number: C08L51/06 ,  C08F110/06 ,  C08F255/00 ,  C08F255/02 ,  C08F297/083 ,  C08L23/10 ,  C08L23/12 ,  C08L53/00 ,  C08L2205/02 ,  C08L2666/24 ,  C08L2666/02 ,  C08F2500/17 ,  C08F2500/03

    Abstract: Disclosed is a method for producing a modified propylene polymer, the method comprising heating a mixture of 100 parts by weight of a propylene polymer (A) defined below and from 0.1 to 50 parts by weight of an ethylenically unsaturated bond-containing monomer (B) in the presence of from 0.01 to 20 parts by weight of an organic peroxide (C); propylene polymer (A) being a propylene polymer composed of from 0.5 to 90% by weight of a propylene polymer component (A1) having an intrinsic viscosity [η], as measured in tetralin at 135° C., of from 5 dl/g to 15 dl/g and from 10 to 99.5% by weight of a propylene polymer component (A2) having an intrinsic viscosity [η], as measured in tetralin at 135° C., of not less than 0.1 dl/g but less than 5 dl/g.

    Abstract translation: 公开了一种制备改性丙烯聚合物的方法，该方法包括加热100重量份下文定义的丙烯聚合物（A）和0.1-50重量份含烯属不饱和键的单体（B）的混合物， 在有机过氧化物（C）为0.01〜20重量份的情况下， 丙烯聚合物（A）是丙烯聚合物，其由0.5至90重量％的丙烯聚合物组分（A1）在135℃下在四氢化萘中测得的特性粘度η为5dl / g 至15dl / g和10至99.5wt％的丙烯聚合物组分（A2），其特性粘度η在135℃下在四氢化萘中测得为不小于0.1dl / g但小于 5 dl / g。

    Aqueous emulsion and use thereof
    36.
    发明申请
    Aqueous emulsion and use thereof 有权
    水乳液及其用途

    公开(公告)号：US20050197441A1

    公开(公告)日：2005-09-08

    申请号：US11081360

    申请日：2005-03-04

    Applicant: Mitsuo Shibutani ,  Kiyoharu Kitamura ,  Kinji Taki ,  Masaaki Yamada

    Inventor： Mitsuo Shibutani ,  Kiyoharu Kitamura ,  Kinji Taki ,  Masaaki Yamada

    IPC: C08F2/24 ,  C08F261/04 ,  C08F263/00 ,  C08L29/04 ,  C08L33/00 ,  C08L51/00 ,  C09J151/00 ,  C08K3/20

    CPC classification number: C08F263/00 ,  C08F261/04 ,  C08L29/04 ,  C08L33/00 ,  C08L51/003 ,  C08L2666/02 ,  C09J151/003 ,  C08L2666/04

    Abstract: The present invention provides an aqueous emulsion having excellent polymerization stability and standing stability and a redispersible powder. Specifically, the present invention relates to an aqueous emulsion of a polymer obtained by polymerizing an acrylic monomer in the presence of a polyvinyl alcohol containing an acetoacetic ester group; wherein the polyvinyl alcohol containing an acetoacetic ester group has block character [η] of 0.3 to 0.6, hydrolysis degree of at least 97% by mol and acetoacetic esterification degree of 0.01 to 1.5% by mol, and the value obtained by dividing the maximum value by the minimum value of the respective average acetoacetic esterification degree for each of the polyvinyl alcohol containing an acetoacetic ester group separated by particle size of 44 to 74, 74 to 105, 105 to 177, 177 to 297, 297 to 500 and 500 to 1680 μm is 1.0 to 3.0. Also, the present invention relates to a redispersible fiber obtained by drying the aqueous emulsion.

    Abstract translation: 本发明提供了具有优异的聚合稳定性和稳定性的水性乳液和可再分散的粉末。 具体地说，本发明涉及通过在含有乙酰乙酸酯基的聚乙烯醇存在下聚合丙烯酸类单体获得的聚合物的水性乳液; 其中含有乙酰乙酸酯基的聚乙烯醇的嵌段特性η为0.3〜0.6，水解度为97摩尔％以上，乙酰乙酸酯化度为0.01〜1.5摩尔％，通过除去最大值 通过分别由44〜74,74〜105,105〜177,177〜297,297〜500和500〜1680分隔的含有乙酰乙酸酯基的各聚乙烯醇的各自的平均乙酰乙酸酯化度的最小值 妈妈是1.0到3.0。 此外，本发明涉及通过干燥水性乳液获得的可再分散纤维。

    Process for producting optical resin materials with distributed refractive index
    37.
    发明授权
    Process for producting optical resin materials with distributed refractive index 失效
    具有折射率分布的光学树脂材料的制造方法

    公开(公告)号：US5763514A

    公开(公告)日：1998-06-09

    申请号：US475101

    申请日：1995-06-07

    Applicant: Yasuhiro Koike

    Inventor： Yasuhiro Koike

    IPC: C08F2/00 ,  C08F2/44 ,  C08K5/00 ,  C08L67/07 ,  G02B1/04 ,  G02B6/028 ,  C08F263/00

    CPC classification number: G02B6/02038 ,  C08F2/44 ,  C08K5/0008 ,  C08L67/07 ,  G02B1/04 ,  G02B1/045 ,  Y10S525/932

    Abstract: An optical resin, of which the refractive index continuously changes in a specific direction, is produced by filling a polymerization container with a mixed solution containing at least one type of polymerizable monomer or polymerizable monomer sol and at least one type of substance whose solubility parameter differs by 7 (cal/cm.sup.3).sup.1/2 or less and refractive index by 0.001 or more from those of a polymer produced by polymerization of the monomer, and by subjecting the mixture to polymerization reaction by applying heat or energy rays to the container from outside so that the polymerization reaction starts and progresses preferentially from a particular region of the mixture, thus forming a concentration gradient of the substance having different refractive index.The polymerization container may be made of a polymer which swells and dissolves into the mixed solution from an inner wall thereof. After completing the polymerization reaction, the optical resin is subjected to hot drawing to obtain an optical conductor. Further, post-treatment based on crosslinking reaction is applied to improve heat resistance.

    Abstract translation: 通过用含有至少一种可聚合单体或可聚合单体溶胶的混合溶液和至少一种溶解度参数不同的物质填充聚合容器来产生折射率在特定方向上连续变化的光学树脂 通过单体聚合制备的聚合物的折射率乘以7（cal / cm 3）+ E，fra 1/2 + EE或更低，折射率为0.001以上，并且通过施加热或能量使混合物进行聚合反应 从聚合反应开始并优先从混合物的特定区域进行聚合反应，从而形成具有不同折射率的物质的浓度梯度。 聚合容器可以由从其内壁溶胀并溶解到混合溶液中的聚合物制成。 聚合反应完成后，对光学树脂进行热拉伸，得到光导体。 此外，应用基于交联反应的后处理以改善耐热性。

    Process for the manufacture of polymeric materials with a high chemical and mechanical resistance and polymeric materials with a high chemical and mechanical resistance
    38.
    发明授权
    Process for the manufacture of polymeric materials with a high chemical and mechanical resistance and polymeric materials with a high chemical and mechanical resistance 失效

    公开(公告)号：US5736608A

    公开(公告)日：1998-04-07

    申请号：US564203

    申请日：1996-04-17

    Applicant: Marceli Cyrkiewicz ,  Erwin Herling ,  Jacek Kleszczewski

    Inventor： Marceli Cyrkiewicz ,  Erwin Herling ,  Jacek Kleszczewski

    IPC: C04B14/30 ,  C04B14/36 ,  C04B26/04 ,  C04B26/18 ,  C08F2/44 ,  C08F263/00 ,  C08F299/04 ,  C08K3/32 ,  C08K3/34 ,  C08L67/06 ,  C08K3/30

    CPC classification number: C08K3/32

    Abstract: A process for the manufacture of materials with a high chemical and mechanical resistance in which for each 100 parts by volume of vinylester resin treated with 0.85-1.47 parts by volume of an accelerant in the form of cobalt naphthenate, there are added at least in two batches 50-900 parts by volume of an inorganic filler constituting previously roasted at a temperature not lower than 470 K disintegrated to a particle size of at least 30 .mu.m phosphogypsum or a composition of phosphogypsum with glass-forming oxides or phosphogypsum with magnetite or phosphogypsum with microsphere, after which on continuous stirring there is added, if necessary, up to 60 parts by volume of styrene and/or up to 0.2 parts by volume of dimethylaniline, and then the whole is polymerized in the presence of know initiators such as organic peroxides. The materials with a high chemical and mechanical resistance constitute polymerized composition of synthetic resin and inorganic fillers, consisting of 7.5-88.1% by weight of vinylester resin, styrene and/or a low-molecular-weight unsaturated polyester resin in a quantity up to 34.1% by weight, and 14.3-86.6% by weight of phosphogypsum or 0.4-46.6% by weight of phosphogypsum and 6.4-44.8% by weight of glass-forming oxides or 4.6-53.5% by weight of microsphere or 5.5-42.1% by weight of magnetite. The process for the manufacture of these materials makes it possible to utilize industrial wastes resulted from production of phosphoric acid, while the material itself in all its varieties is characterized by a very good resistance to aggressive media, also at elevated temperatures, and suitable for processing by mechanical methods as well as for combining with other materials by using to that end an incompletely polymerized composition of the material.

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