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公开(公告)号：US06194716B1
公开(公告)日：2001-02-27
申请号：US09143399
申请日：1998-08-28
Applicant: Yasuaki Takada , Takayuki Nabeshima , Minoru Sakairi , Yuichiro Hashimoto
Inventor： Yasuaki Takada , Takayuki Nabeshima , Minoru Sakairi , Yuichiro Hashimoto
IPC: B01D5944
CPC classification number: H01J49/424 , H01J49/0009 , H01J49/428
Abstract: A method for performing a mass calibration under an application of a desired ion peak position of mass spectrum attained by a mass scanning of ions of substance having a known value of m/z and the known value of m/z is added with a step for ejecting an amount of unnecessary ions not contributing to the aforesaid mass calibration accumulated in the aforesaid ion trap type mass analysis region prior to the aforesaid mass scanning operation. An accumulation of a large amount of unnecessary ions in the ion trap type mass analysis region is restricted, a disturbance of electric field in the ion trap mass analysis region generated under an influence of a spatial charge caused by accumulation of the unnecessary ions can be prevented and the aforesaid mass calibration can be performed in an easy and accurate manner.
Abstract translation: 在通过具有已知m / z值的物质的离子的质量扫描和已知的m / z值获得的质谱所需离子峰位置的施加下进行质量校准的方法添加了用于 在上述质量扫描操作之前，排出在上述离子阱型质量分析区域中累积的对上述质量校准无贡献的不需要的离子的量。 离子阱型质量分析区域中的大量不需要的离子的积聚受到限制，可以防止在由不需要的离子的积聚引起的空间电荷的影响下产生的离子阱质量分析区域中的电场的扰动 并且可以容易且准确地进行上述质量校准。
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公开(公告)号：US09040905B2
公开(公告)日：2015-05-26
申请号：US13884755
申请日：2011-11-08
Applicant: Hisashi Nagano , Yasutaka Suzuki , Hideo Kashima , Yuichiro Hashimoto , Masuyuki Sugiyama , Masakazu Sugaya , Yasunori Doi , Koichi Terada
Inventor： Hisashi Nagano , Yasutaka Suzuki , Hideo Kashima , Yuichiro Hashimoto , Masuyuki Sugiyama , Masakazu Sugaya , Yasunori Doi , Koichi Terada
CPC classification number: H01J49/0422 , G01N1/2211 , G01N1/2214 , G01N33/0057 , G01N2001/028 , H01J49/00 , H01J49/0036 , H01J49/04 , H01J49/0459 , H01J49/0468 , Y02A50/25
Abstract: Provided is a technique of analyzing particles in real time while collecting and condensing the particles continuously. Gas and/or particles as a detection target substance that are attached to an authentication target 2 are removed by air flow from a blowing region 5. The removed sample is sucked and is condensed and sampled at a sampling region 10, and ions of the sample are generated at an ion source 21 and are then subjected to mass analysis at a mass analysis region 23. Determination of the obtained mass spectrum is made as to the presence or not of a mass spectrum derived from the detection target substance, and a monitor 27 displays a result thereof. Thereby, the detection target substance attached to the authentication target 2 can be detected continuously in real time, promptly and with a less error rate.
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公开(公告)号：US08973606B2
公开(公告)日：2015-03-10
申请号：US13327678
申请日：2011-12-15
Applicant: Yuichiro Hashimoto , Junichi Miyaji
Inventor： Yuichiro Hashimoto , Junichi Miyaji
Abstract: The present invention is one that prevents standard gas from remaining in a standard gas line to prevent a concentration of standard gas from being reduced due to adsorption, modification, or the like, and has: a diluent gas line provided with a diluent gas flow rate controlling mechanism; a standard gas line provided with a standard gas flow rate controlling mechanism; an output gas line joined by the diluent gas line and standard gas line and outputs the standard gas having a predetermined concentration; an exhaust gas line connected to an upstream side of the standard gas flow rate controlling mechanism in the standard gas line and provided with an on/off valve and a flow rate control part; and a control part that, depending on a flow rate of the standard gas flowing through the standard gas line or the type of the standard gas, switches on/off the on/off valve.
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公开(公告)号：US08710430B2
公开(公告)日：2014-04-29
申请号：US13527619
申请日：2012-06-20
Applicant: Masuyuki Sugiyama , Yuichiro Hashimoto , Shun Kumano , Yohei Kawaguchi , Hidetoshi Morokuma
Inventor： Masuyuki Sugiyama , Yuichiro Hashimoto , Shun Kumano , Yohei Kawaguchi , Hidetoshi Morokuma
CPC classification number: H01J49/4265 , H01J49/0009 , H01J49/0036
Abstract: A mass spectrometry method that corrects the effects from space charge and that achieves both sensitivity and a dynamic range. The mass axis of the mass spectrum is corrected based on the counts of ions accumulated within the ion trap at the point in time each ion was extracted.
Abstract translation: 一种校正空间电荷效应并实现灵敏度和动态范围的质谱法。 基于在每个离子被提取的时间点内积聚在离子阱内的离子的计数校正质谱的质量轴。
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公开(公告)号：US20130334416A1
公开(公告)日：2013-12-19
申请号：US14001711
申请日：2012-01-27
Applicant: Hiroyuki Satake , Hideki Hasegawa , Masuyuki Sugiyama , Yuichiro Hashimoto
Inventor： Hiroyuki Satake , Hideki Hasegawa , Masuyuki Sugiyama , Yuichiro Hashimoto
IPC: H01J49/10
CPC classification number: H01J49/10 , H01J49/0431 , H01J49/165
Abstract: The quantitative accuracy of analysis is improved without reducing the dynamic range for measurement of concentrations by performing stable ionization through electrospray or the like which repeats sampling and ionization using a movable probe electrode.A voltage is applied from a high-voltage power source 4 to a sample transport electrode 7 having a plurality of probe electrodes 1 and a driving section 3 drives the sample transport electrode 7 to rotate. The plurality of probe electrodes 1, to which a sample solution 5 is adhered, are sequentially transported to an inlet 21 of a mass spectrometer 20, thus electrospray ionization is continuously performed.
Abstract translation: 通过使用可移动探针电极重复取样和电离的电喷雾等进行稳定的电离，可以提高分析的定量精度，而不降低浓度测定的动态范围。 从高电压电源4向具有多个探针电极1的检体输送电极7施加电压，驱动部3驱动检体输送电极7旋转。 将附着有样品溶液5的多个探针电极1依次输送到质谱仪20的入口21，从而连续进行电喷雾离子化。
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Patent Agency Ranking
公开(公告)号：US20130240726A1
公开(公告)日：2013-09-19
申请号：US13877717
申请日：2011-10-03
Applicant: Hideki Hasegawa , Masuyuki Sugiyama , Hiroyuki Satake , Yuichiro Hashimoto
Inventor： Hideki Hasegawa , Masuyuki Sugiyama , Hiroyuki Satake , Yuichiro Hashimoto
IPC: H01J49/06
CPC classification number: H01J49/063 , H01J49/005 , H01J49/068 , H01J49/4255
Abstract: This mass spectrometer is provided with an ion guide (37) having a multipole rod electrode (1), a power source unit (5) for applying voltage to the multipole rod electrode, and a control unit for controlling the power source unit, said mass spectrometer being characterised by the multipole rod electrode having a rod electrode divided into a plurality of segmented rods (2A-1, 2A-2, 2B-1, 2B-2, 2C-1, 2C-2, 2D-1, 2D-2) at mutually different positions in the axial direction. Thus enabled is low-cost, high-throughput analysis.
Abstract translation: 该质谱仪设置有具有多极杆电极（1）的离子引导件（37），用于向多极杆电极施加电压的电源单元（5），以及用于控制电源单元的控制单元，所述质量 光谱仪的特征在于多极杆电极具有分为多个分段杆（2A-1,2A-2,2B-1,2B-2,2C-1,2C-2，2D-1，2D- 2）在轴向上相互不同的位置。 因此启用了低成本，高通量分析。
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公开(公告)号：US08368013B2
公开(公告)日：2013-02-05
申请号：US13084930
申请日：2011-04-12
Applicant: Masako Ishimaru , Yuichiro Hashimoto , Hideki Hasegawa , Masuyoshi Yamada , Masuyuki Sugiyama , Hidetoshi Morokuma
Inventor： Masako Ishimaru , Yuichiro Hashimoto , Hideki Hasegawa , Masuyoshi Yamada , Masuyuki Sugiyama , Hidetoshi Morokuma
CPC classification number: H01J49/145
Abstract: An analyzer performs dielectric barrier discharge and ionization of a sample by a reaction between the sample and excited molecules or ions generated by the dielectric barrier discharge at a pressure lower than an atmospheric pressure.
Abstract translation: 分析仪通过在低于大气压的压力下通过介电阻挡放电产生的样品和激发的分子或离子之间的反应来进行介电阻挡放电和样品的离子化。
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公开(公告)号：US20120326022A1
公开(公告)日：2012-12-27
申请号：US13527627
申请日：2012-06-20
Applicant: Shun KUMANO , Masuyuki Sugiyama , Yuichiro Hashimoto , Hideki Hasegawa , Masuyoshi Yamada , Hidetoshi Morokuma , Shuhei Hashiba
Inventor： Shun KUMANO , Masuyuki Sugiyama , Yuichiro Hashimoto , Hideki Hasegawa , Masuyoshi Yamada , Hidetoshi Morokuma , Shuhei Hashiba
IPC: H01J49/04
CPC classification number: H01J49/0409 , H01J49/0495
Abstract: A mass spectrometer including a sample attaching member of attaching a sample, an ionizing chamber including an introductory port of the sample attaching member and an ionization source of generating a sample ion, a vacuumed chamber having a mass analyzer of analyzing the sample ion, and an opening/closing mechanism provided between the ionizing chamber and the vacuumed chamber, in which the opening/closing mechanism is controlled from a closed state to an open state after introducing the sample attaching member into the ionizing chamber to thereby enable to perform ionization with inconsiderable fragmentation at a high sensitivity with a high throughput
Abstract translation: 一种质谱仪，包括附着样品的样品附着构件，包括样品附着构件的入口的电离室和产生样品离子的离子源，具有分析样品离子的质量分析器的真空室，以及 设置在离子化室和真空室之间的开/关机构，其中将样品附着构件引入电离室之后，将开/关机构从关闭状态控制到打开状态，从而能够以不可分割的碎片进行电离 灵敏度高，吞吐量高
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公开(公告)号：US20120152364A1
公开(公告)日：2012-06-21
申请号：US13327678
申请日：2011-12-15
Applicant: Yuichiro Hashimoto , Junichi Miyaji
Inventor： Yuichiro Hashimoto , Junichi Miyaji
IPC: F15D1/00
CPC classification number: G05D11/132 , G01N33/0006 , Y10T137/0318 , Y10T137/7759 , Y10T137/7761 , Y10T137/87249 , Y10T137/8729 , Y10T137/87314 , Y10T137/87676
Abstract: The present invention is one that prevents standard gas from remaining in a standard gas line to prevent a concentration of standard gas from being reduced due to adsorption, modification, or the like, and has: a diluent gas line provided with a diluent gas flow rate controlling mechanism; a standard gas line provided with a standard gas flow rate controlling mechanism; an output gas line joined by the diluent gas line and standard gas line and outputs the standard gas having a predetermined concentration; an exhaust gas line connected to an upstream side of the standard gas flow rate controlling mechanism in the standard gas line and provided with an on/off valve and a flow rate control part; and a control part that, depending on a flow rate of the standard gas flowing through the standard gas line or the type of the standard gas, switches on/off the on/off valve.
Abstract translation: 本发明是防止标准气体残留在标准气体管线中，以防止标准气体由于吸附，改性等而降低的浓度，并具有：具有稀释气体流量的稀释气体管线 控制机制; 设有标准气体流量控制机构的标准气体管线; 通过稀释气体管线和标准气体管路连接的输出气体管线，输出具有预定浓度的标准气体; 与标准气体流量控制机构的标准气体流量控制机构的上游侧连接并配置有开关阀和流量控制部的排气管路， 以及控制部，其根据流过标准气体管路的标准气体的流量或标准气体的类型来开/关开闭阀。
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公开(公告)号：US20120112059A1
公开(公告)日：2012-05-10
申请号：US13383371
申请日：2010-07-09
Applicant: Masuyuki Sugiyama , Yuichiro Hashimoto , Hisashi Nagano , Hideki Hasegawa , Yasuaki Takada , Masuyoshi Yamada
Inventor： Masuyuki Sugiyama , Yuichiro Hashimoto , Hisashi Nagano , Hideki Hasegawa , Yasuaki Takada , Masuyoshi Yamada
IPC: H01J49/26
CPC classification number: H01J49/004
Abstract: An object is to measure both cations and anions with high duty cycle. In a mass spectrometer comprising an ion source (1), an ion guide part (31), and an ion trap (32), while ions are being mass-selectively ejected from the ion trap, ions having a polarity reverse to that of the ions trapped in the ion trap are introduced into the ion guide part.
Abstract translation: 一个目标是测量阳离子和阴离子高占空比。 在离子源（1），离子引导部（31）和离子阱（32）的质谱仪中，离子从离子阱中质量选择性地喷出时，具有与 捕获在离子阱中的离子被引入离子引导部。
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