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    PROCESS FOR PRODUCING FINE PARTICLES OF SOLID SOLUTION
    44.
    发明申请
    PROCESS FOR PRODUCING FINE PARTICLES OF SOLID SOLUTION 失效
    生产精细溶液颗粒的方法

    公开(公告)号：US20100022387A1

    公开(公告)日：2010-01-28

    申请号：US12506415

    申请日：2009-07-21

    Applicant: Yoshihisa Beppu ,  Kazuo Sunahara

    Inventor： Yoshihisa Beppu ,  Kazuo Sunahara

    IPC: B01J23/10

    CPC classification number: C01G25/006 ,  B01J23/002 ,  B01J35/023 ,  B01J35/1014 ,  B01J37/08 ,  B01J2523/00 ,  B82Y30/00 ,  C01P2002/50 ,  C01P2004/10 ,  C01P2004/20 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/12 ,  C03C3/155 ,  C03C10/00 ,  C03C23/008 ,  H01M4/9016 ,  B01J2523/24 ,  B01J2523/25 ,  B01J2523/305 ,  B01J2523/3706 ,  B01J2523/3712 ,  B01J2523/48 ,  B01J2523/3787 ,  B01J2523/3725 ,  B01J2523/3718 ,  B01J2523/375 ,  B01J2523/36

    Abstract: Provided is a process for readily producing fine particles of a solid solution having a small particle size, comprising a solid solution of zirconia, ceria and a rare earth oxide in a desired composition, and being highly crystalline.The process for producing the fine particles of the solid solution comprises the following steps in the order named: obtaining a melt comprising, in terms of mol % on an oxide basis, from 5 to 50% ZrO2, CeO2 and RE2O3 (where RE is at least one member selected from rare earth elements other than Ce) in total, from 10 to 50% RO (where R is at least one member selected from the group consisting of Mg, Ca, Sr, Ba and Zn), and from 30 to 75% B2O3; quenching the melt to obtain an amorphous material; heating the amorphous material to obtain precipitates containing crystals of a solid solution with ZrO2, CeO2 and RE2O3; and separating the crystals of the solid solution from the precipitates to obtain fine particles of the solid solution.

    Abstract translation: 本发明提供容易制造具有小粒径的固溶体的细颗粒的方法，其包含氧化锆，二氧化铈和稀土氧化物的固溶体，并具有高结晶性。 制造固溶体微粒的方法包括以下顺序的步骤：获得包含以氧化物为基准的摩尔％为5至50％的ZrO 2，CeO 2和RE 2 O 3（其中RE为 至少一种选自Ce以外的稀土元素的组分），10至50％的RO（其中R是选自Mg，Ca，Sr，Ba和Zn中的至少一种），并且从30至 75％B2O3; 淬火熔体以获得无定形材料; 加热无定形材料，得到含有ZrO 2，CeO 2和RE 2 O 3的固溶体晶体的析出物; 并将固溶体的晶体与析出物分离，得到固溶微细颗粒。

    Method for Making Silicon-Containing Products
    45.
    发明申请
    Method for Making Silicon-Containing Products 有权
    含硅产品的制造方法

    公开(公告)号：US20090324478A1

    公开(公告)日：2009-12-31

    申请号：US12556754

    申请日：2009-09-10

    Applicant: Norman D. Hinman ,  Charles S. Wyman

    Inventor： Norman D. Hinman ,  Charles S. Wyman

    IPC: C01B31/36

    CPC classification number: C01B21/0685 ,  C01B32/956 ,  C01P2004/10 ,  Y10S502/506 ,  Y10S502/507

    Abstract: A method for producing carbon-silica products from silica-containing plant matter such as rice hulls or straw by leaching with sulfuric acid to remove non-silica minerals and metal while adjusting the mole ratio of fixed carbon to silica in the resultant product. The carbon and silica are intimately mixed on a micron or submicron scale and are characterized by high purity and reactivity, small particle size, high porosity, and contain volatile carbon that can be used as a source of energy for the production of silicon-containing products from the carbon-silica products. High purity silicon-containing products made from the carbon-silica products of the invention are also disclosed.

    Abstract translation: 一种通过用硫酸浸出从含二氧化硅的植物物质例如稻壳或秸秆中生产碳硅石产品的方法，以在调节所得产物中固定碳与二氧化硅的摩尔比的同时除去非二氧化硅矿物和金属。 碳和二氧化硅在微米或亚微米尺度上紧密混合，其特征在于高纯度和反应性，小颗粒尺寸，高孔隙率，并含有可用作生产含硅产品的能量来源的挥发性碳 来自碳硅石产品。 还公开了由本发明的碳 - 硅石产品制成的高纯度含硅产品。

    High purity silicon-containing products
    46.
    发明授权
    High purity silicon-containing products 有权
    高纯度含硅产品

    公开(公告)号：US07638108B2

    公开(公告)日：2009-12-29

    申请号：US11248368

    申请日：2005-10-12

    Applicant: Norman D. Hinman ,  Charles E. Wyman

    Inventor： Norman D. Hinman ,  Charles E. Wyman

    IPC: C01B31/36

    CPC classification number: C01B33/021 ,  C01B21/0685 ,  C01B32/956 ,  C01B33/00 ,  C01B33/1071 ,  C01P2004/10

    Abstract: Silicon-containing products, such as silicon, silicon carbide and silicon nitride, containing less than 0.01 weight percent total mineral impurities and selectively determined carbon-to-silicon ratios. The products are derived from plant matter, such as rice hulls and rice straw, containing at least three weight percent silica. Methods are provided for making such high purity silicon-containing products by leaching silica-containing plant matter with aqueous sulfuric acid under controlled temperatures, pressures and reaction times to remove minerals and metals while adjusting the mole ratio of fixed carbon to silica, and then thermally treating under controlled conditions to produce the desired product.

    Abstract translation: 含硅产品，例如硅，碳化硅和氮化硅，含有小于0.01重量％的矿物杂质总数，并选择性地确定碳 - 硅的比例。 产品来自植物物质，如稻壳和稻草，含有至少三重量百分比的二氧化硅。 提供了通过在控制温度，压力和反应时间内将含二氧化硅的植物物质与硫酸水溶液浸出以除去矿物质和金属同时调节固定碳与二氧化硅的摩尔比，然后进行热处理的方法来制备这种高纯度含硅产物 在受控条件下处理以产生所需产物。

    TITANIUM OXIDE-BASED SOL-GEL POLYMER
    47.
    发明申请
    TITANIUM OXIDE-BASED SOL-GEL POLYMER 有权
    氧化钛基溶胶凝胶聚合物

    公开(公告)号：US20090173383A1

    公开(公告)日：2009-07-09

    申请号：US12406760

    申请日：2009-03-18

    Applicant: Luc Brohan ,  Hari Sutrisno ,  Yves Piffard ,  Maria Teresa Caldes-Rouillon ,  Olivier Joubert ,  Eric Puzenat ,  Annabelle Rouet

    Inventor： Luc Brohan ,  Hari Sutrisno ,  Yves Piffard ,  Maria Teresa Caldes-Rouillon ,  Olivier Joubert ,  Eric Puzenat ,  Annabelle Rouet

    IPC: H01L31/0216 ,  H01B1/02

    CPC classification number: B82Y30/00 ,  C01G23/0536 ,  C01P2002/76 ,  C01P2004/10 ,  C01P2004/64 ,  C01P2006/60

    Abstract: The invention relates to a titanium oxide-based polymer composition. The inventive composition comprises a TiOx(OH)y(H2O)z(x+y−+z=3) titanium oxide-based polymer in the form of a gel or sol. Said polymer, which has a one-dimensional (1D) structure, is made from concentrically-wound fibers having a periodicity which is deduced from the spacing between said fibers, of between 3.5 Å and 4 Å. Each fiber comprises TiO6octahedrons and each TiO6octahedron shares two opposite edges with two adjacent octahedrons (2.times.292 Å) in order to form infinite chains which develop along the axis of a fiber. According to the invention, two adjacent chains form double lines as a result of the shared edges (2.times.3.27 Å). The inventive polymer is suitable for use as a photosensitive element in a photovoltaic cell, such as a sunscreen for a window.

    Abstract translation: 本发明涉及一种基于氧化钛的聚合物组合物。 本发明的组合物包含凝胶或溶胶形式的TiO x（OH）y（H 2 O）z（x + y + z = 3）氧化钛基聚合物。 具有一维（1D）结构的所述聚合物由具有介于3.5和4之间的从所述纤维之间的间隔推断的周期性的同心缠绕的纤维制成。 每个纤维包括TiO 6八面体，并且每个TiO 6八面体共享两个相对的边缘和两个相邻的八面体（2.282），以形成沿着纤维轴发展的无限链。 根据本发明，作为共享边缘的结果，两个相邻的链形成双线（2/3.27埃）。 本发明的聚合物适合用作光伏电池中的光敏元件，例如用于窗户的防晒剂。

    Apparatus for Producing Nano-Particles of Molybdenum Oxide
    48.
    发明申请
    Apparatus for Producing Nano-Particles of Molybdenum Oxide 有权
    用于生产氧化钼纳米颗粒的装置

    公开(公告)号：US20090169437A1

    公开(公告)日：2009-07-02

    申请号：US12275929

    申请日：2008-11-21

    Applicant: Joel A. Taube ,  Mohamed H. Khan ,  James A. Cole

    Inventor： Joel A. Taube ,  Mohamed H. Khan ,  James A. Cole

    IPC: G05D23/00 ,  F28D21/00

    CPC classification number: B82Y30/00 ,  B01D7/00 ,  C01G39/02 ,  C01P2004/04 ,  C01P2004/10 ,  C01P2004/64 ,  C01P2006/12 ,  Y10S977/775 ,  Y10S977/776 ,  Y10S977/811

    Abstract: Apparatus for producing nano-particles includes a furnace defining a vapor region therein. A precipitation conduit having an inlet end and an outlet end is positioned with respect to the furnace so that the inlet end is open to the vapor region. A quench fluid supply apparatus supplies quench fluid in a gas state and quench fluid in a liquid state. A quench fluid port positioned within the precipitation conduit is fluidically connected to the quench fluid supply apparatus so that an inlet to the quench fluid port receives quench fluid in the gas state and quench fluid in the liquid state. The quench fluid port provides a quench fluid stream to the precipitation conduit to precipitate nano-particles within the precipitation conduit. A product collection apparatus connected to the outlet end of the precipitation conduit collects nano-particles produced within the precipitation conduit.

    Abstract translation: 用于生产纳米颗粒的装置包括在其中限定蒸汽区域的炉。 具有入口端和出口端的沉淀管相对于炉定位，使得入口端对蒸气区开放。 骤冷流体供给装置以气体状态供给骤冷流体并骤冷液态液体。 位于沉淀管道内的骤冷流体端口流体连接到骤冷流体供应装置，使得骤冷流体端口的入口容纳处于气体状态的骤冷流体并骤冷液态液体。 骤冷流体端口向沉淀管道提供骤冷流体流以沉淀沉淀管道内的纳米颗粒。 连接到沉淀管道的出口端的产品收集装置收集在沉淀管道内产生的纳米颗粒。

    Process for producing barium sulfate, barium sulfate and use thereof
    49.
    发明授权
    Process for producing barium sulfate, barium sulfate and use thereof 失效
    硫酸钡，硫酸钡的制造方法及其用途

    公开(公告)号：US07501110B2

    公开(公告)日：2009-03-10

    申请号：US11077775

    申请日：2005-03-11

    Applicant: Djamschid Amirzadeh-Asl ,  Jürgen Bäuml ,  Udo Selter

    Inventor： Djamschid Amirzadeh-Asl ,  Jürgen Bäuml ,  Udo Selter

    IPC: C01F5/42

    CPC classification number: C01F11/462 ,  C01P2004/10 ,  C01P2004/20 ,  C01P2004/54 ,  C01P2004/61 ,  C01P2004/62

    Abstract: This patent describes the use of barium sulfate as filler for thermosetting and thermoplastic plastics, elastomers, sealants, adhesives, fillers, varnishes, paints, paper, glass and as substrate for colored pigment formulations as well as for single-layer or multilayer coatings consisting of metal oxides, metal oxide mixtures and/or metal compounds, as a nucleus of crystallization for lead sulfate in the negative electrode paste of lead accumulators and as an X-ray contrast medium, the barium sulfate being produced by a continuous process wherein a barium salt solution and a sulfate solution are simultaneously and continuously brought together in equimolar quantities in a precipitating suspension at a temperature of 30 to 90° C., with constant stirring, the precipitating suspension is withdrawn continuously in a steady volume and the barium sulfate precipitate is filtered, washed and optionally dried, wherein the barium salt solution has a concentration of 0.1 to 0.8 Ba2+ mol/l and the sulfuric acid has a concentration of 0.1 to 2.0 SO42− mol/l, and the flow rate and stirring speed are controlled, at a constant precipitation volume, in such a way that a pH value of 1 to 5 is obtained in the precipitating suspension, and the lamellar barium sulfate particles produced as result of the precipitation are 0.1 to 50 μm wide, 0.1 to 50 μm long and 0.1 to 2 μm thick and the needle-shaped particles produced as result of the precipitation are 1 to 50 μm long and 0.1 to 2 μm thick, the ratio of length or width to the thickness being 3:1 to 500:1.

    Abstract translation: 该专利描述了硫酸钡作为热固性和热塑性塑料，弹性体，密封剂，粘合剂，填料，清漆，油漆，纸，玻璃以及用作有色颜料配方的底物以及用于单层或多层涂层 金属氧化物，金属氧化物混合物和/或金属化合物，作为铅蓄电池的负极糊料中的硫酸铅的结晶核，作为X射线造影剂，所述硫酸钡是通过连续方法生产的，其中钡盐 溶液和硫酸盐溶液以等摩尔量在沉淀悬浮液中在30至90℃的温度下同时并连续地连续，在恒定搅拌下，将沉淀的悬浮液以稳定的体积连续取出，并将硫酸钡沉淀物过滤 洗涤并任选地干燥，其中钡盐溶液的浓度为0.1至0.8Ba 2 + mol / l和th e硫酸的浓度为0.1〜2.0 SO42- mol / l，流速和搅拌速度以恒定的沉淀体积控制，使得在沉淀悬浮液中获得1〜5的pH值 ，沉淀结果产生的层状硫酸钡粒子为0.1〜50μm，宽度为0.1〜50μm，厚度为0.1〜2μm，由于沉淀而生成的针状粒子长度为1〜50μm， 0.1至2μm厚，长度或宽度与厚度之比为3:1至500:1。

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