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    Cycloalkanone composition
    41.
    发明申请
    Cycloalkanone composition 有权
    环烷酮组合物

    公开(公告)号：US20050227909A1

    公开(公告)日：2005-10-13

    申请号：US11076912

    申请日：2005-03-11

    Applicant: Koji Mine

    Inventor： Koji Mine

    IPC: C07C45/74 ,  C07B61/00 ,  C07C45/66 ,  C07C45/67 ,  C07C45/72 ,  C07C49/493 ,  C07C49/497 ,  C07C49/747 ,  C07C67/347 ,  A61K7/46 ,  C07C49/293 ,  C07C69/74

    CPC classification number: C07C49/493 ,  C07C45/66 ,  C07C45/67 ,  C07C45/72 ,  C07C49/497 ,  C07C49/747 ,  C07C49/647 ,  C07C49/597

    Abstract: The present invention relates to a cycloalkanone composition which contains cycloalkanone (1) in an amount of 70 wt % or more based on the composition, wherein the content of a dimer of a cycloalkanone represented by formula (2) is 0.055 or less in terms of weight ratio to the cycloalkanone (1), a process for producing the same, a process for producing a composition containing alkyl acetate (5) by using the cycloalkanone composition, and an alkyl acetate composition obtained by the process wherein n is an integer of 1 or 2, R1 and R2 each represent H, a C1 to C8 alkyl group etc., and R3 represents a C1 to C3 alkyl group.

    Abstract translation: 本发明涉及基于组合物含有70重量％以上的环烷酮（1）的环烷酮酮组合物，其中式（2）所示的环烷酮的二聚物的含量为0.055以下 与环烷酮（1）的重量比，其制备方法，通过使用环烷酮组合物制备含有烷基乙酸酯（5）的组合物的方法和通过其中n为整数1的方法获得的乙酸烷基酯组合物 或2，R 1和R 2各自表示H，C 1至C 8烷基等，R 3表示C 1至C 3 烷基。

    Gem-disubstituted cyclohexadienones and their production
    44.
    发明授权
    Gem-disubstituted cyclohexadienones and their production 失效
    双取代的环己二烯酮及其生产

    公开(公告)号：US4871877A

    公开(公告)日：1989-10-03

    申请号：US196680

    申请日：1988-05-20

    Applicant: G. Patrick Stahly

    Inventor： G. Patrick Stahly

    IPC: C07C39/24 ,  C07C39/38 ,  C07C45/62 ,  C07C45/67 ,  C07C45/68 ,  C07C49/497 ,  C07C49/713 ,  C07C49/747 ,  C07F7/18

    CPC classification number: C07F7/188 ,  C07C39/24 ,  C07C39/38 ,  C07C45/62 ,  C07C45/673 ,  C07C45/68 ,  C07C49/497 ,  C07C49/713 ,  C07C49/747 ,  C07F7/1856

    Abstract: Quinones may be perfluoroalkylated by means of perfluoroalkyltrihydrocarbyl silane using certain active alkali metal salt catalysts and a proton source. The reaction--which is conducted, preferably in a suitable liquid phase reaction medium, most preferably a dipolar aprotic solvent--results in the formation of gem-disubstituted cyclohexadienones in which the gem substitutes are a perfluoroalkyl group and a hydroxyl group. These gem-disubstituted compounds in turn can be readily converted to perfluoroalkyl substituted aromatics, thus circumventing the traditional need for photochlorination followed by halogen exchange using hydrogen fluoride as a means of preparing perfluoroalkyl aromatic compounds.

    Abstract translation: 使用某些活性碱金属盐催化剂和质子源，醌酮可以通过全氟烷基三烃基硅烷全氟烷基化。 进行的反应优选在合适的液相反应介质中，最优选偶极非质子溶剂，导致形成宝石二取代的环己二烯酮，其中宝石代用品是全氟烷基和羟基。 甲基二取代的化合物又可以容易地转化为全氟烷基取代的芳族化合物，从而避免了光氯化的传统需要，随后使用氟化氢进行卤素交换作为制备全氟烷基芳族化合物的手段。

    Production of gem-disubstituted cyclohexadienones
    45.
    发明授权
    Production of gem-disubstituted cyclohexadienones 失效
    偕二取代的环己二烯酮的生产

    公开(公告)号：US4845258A

    公开(公告)日：1989-07-04

    申请号：US177153

    申请日：1988-04-04

    Applicant: G. Patrick Stahly

    Inventor： G. Patrick Stahly

    IPC: C07C37/62 ,  C07C39/24 ,  C07C45/62 ,  C07C45/67 ,  C07C49/497 ,  C07C49/713 ,  C07C49/747 ,  C07F7/08 ,  C07F7/18

    CPC classification number: C07F7/1856 ,  C07C37/50 ,  C07C45/62 ,  C07C45/673 ,  C07C49/497 ,  C07C49/713 ,  C07C49/747 ,  C07F7/0818 ,  C07C2103/24 ,  C07C2103/26

    Abstract: Quinones may be perfluoroalkylated by means of perfluoroalkyltrihydrocarbyl silane using quaternary ammonium bifluorides, quaternary phosphonium bifluorides or alkali metal bifluorides as catalysts. The reaction--which is conducted under essentially anhydrous conditions, preferably in a suitable liquid phase reaction medium, most preferably a dipolar aprotic solvent--results in the formation of gem-disubstituted cyclohexadienones in which the gem substituents are a perfluoroalkyl group and a trihydrocarbylsiloxy group. These gem-disubstituted compounds in turn can be readily converted to perfluoroalkyl substituted aromatics, thus circumventing the traditional need for photochlorination followed by halogen exchange using hydrogen fluoride as a means of preparing perfluoroalkyl aromatic compounds.

    Abstract translation: 醌类可以通过全氟烷基三烃基硅烷全氟烷基化，使用二氟化二氟鎓，二氟化鏻二氟化物或碱金属二氟化物作为催化剂。 在基本上无水条件下进行的反应，优选在合适的液相反应介质中，最优选偶极非质子溶剂进行，导致形成偕二取代的环己二烯酮，其中偕取代基是全氟烷基和三烃基甲硅烷氧基。 甲基二取代的化合物又可以容易地转化为全氟烷基取代的芳族化合物，从而避免了光氯化的传统需要，随后使用氟化氢进行卤素交换作为制备全氟烷基芳族化合物的手段。

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