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    Polyether polyols based on o-tolylenediamine, a process for their production, and their use for polyurethane and polyisocyanurate plastics
    53.
    发明授权
    Polyether polyols based on o-tolylenediamine, a process for their production, and their use for polyurethane and polyisocyanurate plastics 失效
    基于邻甲苯二胺的聚醚多元醇，其生产方法及其用于聚氨酯和聚异氰脲酸酯塑料的用途

    公开(公告)号：US5030758A

    公开(公告)日：1991-07-09

    申请号：US277165

    申请日：1988-11-29

    Applicant: Manfred Dietrich ,  Reinhard Kaufung

    Inventor： Manfred Dietrich ,  Reinhard Kaufung

    IPC: C08G18/48 ,  C08G18/50 ,  C08G65/26

    CPC classification number: C08G18/5033 ,  C08G18/4837 ,  C08G18/4845 ,  C08G65/2627 ,  C08G2101/0025 ,  C08G2105/02

    Abstract: This invention relates to o-tolylenediamine-based polyether polyols having an OH number of about 400 to 630, in which about 5 to 20% of the isocyanate-reactive groups of the polyether polyols are secondary amino groups and which contain less than about 0.2% by weight free o-tolylenediamine. The polyether polyols of the invention are formed by sequential reaction of o-tolylenediamine first with about 2 to 5 mol of ethylene oxide and then with about 1 to 5 mol of propylene oxide per mol of o-tolylenediamine. This invention also relates to the process for the production of polyether polyols using said sequential reaction at a temperature of about 90.degree. to 125.degree. C. and in the presence of an amine catalyst. This invention further relates to a method for the production of polyisocyanate-based plastics, preferably polyurethane foams, comprising reacting organic polyisocyanates with polyether polyols of the invention and compounds containing at least two isocyanate-reactive hydrogen atoms and having a molecular weight range of about 200 to 1,500, and optionally also with chain-extending agents or crosslinking agents and auxiliaries or additives.

    Abstract translation: 本发明涉及OH值为约400至630的邻甲苯二胺类聚醚多元醇，其中约5至20％的聚醚多元醇的异氰酸酯反应性基团是仲氨基并且含有小于约0.2％ 游离的邻甲苯二胺。 本发明的聚醚多元醇首先通过邻甲苯胺与约2-5mol环氧乙烷的顺序反应形成，然后与每摩尔邻甲苯二胺约1至5mol环氧丙烷形成。 本发明还涉及使用所述顺序反应在约90-125℃的温度下和在胺催化剂存在下生产聚醚多元醇的方法。 本发明还涉及一种生产基于多异氰酸酯的塑料，优选聚氨酯泡沫的方法，其包括使有机多异氰酸酯与本发明的聚醚多元醇和含有至少两个异氰酸酯反应性氢原子并且分子量范围为约200 至1,500，以及任选地还含有增链剂或交联剂和助剂或添加剂。

    Process for strengthening geological formations
    54.
    发明授权
    Process for strengthening geological formations 失效
    加强地质构造的过程

    公开(公告)号：US4904125A

    公开(公告)日：1990-02-27

    申请号：US348849

    申请日：1989-05-08

    Applicant: Manfred Schmidt ,  Manfred Kapps ,  Max Mann ,  Peter Vehlewald ,  Manfred Dietrich ,  Frank Meyer ,  Wolfgang Cornely ,  Hans E. Mehesch

    Inventor： Manfred Schmidt ,  Manfred Kapps ,  Max Mann ,  Peter Vehlewald ,  Manfred Dietrich ,  Frank Meyer ,  Wolfgang Cornely ,  Hans E. Mehesch

    IPC: E02D3/12 ,  C08G18/32 ,  C08G18/34 ,  C09K17/30 ,  E21D9/00 ,  E21D9/04

    CPC classification number: C09K17/30 ,  E21D9/002

    Abstract: The present invention is directed to a process for the strengthening of geological formations in underground workings and mines by the introduction of reaction mixtures which react to form polyurethanes into the formations which are to be strengthened, the reaction mixtures being based on(a) a polyisocyanate component,(b) a polyol component and(c) an ester,the ester having a hydroxyl number of about 10 to 630 and an acid number of at most 10 and obtained from (i) an acid component having a carboxyl functionality of at least 1.5 and containing a polymerized fatty acid having at least 12 carbon atoms or mixtures thereof with unpolymerized saturated or unsaturated fatty acids having at least 12 carbon atoms and (ii) a polyol component containing at least one polyhydric alcohol, the ester being present in a positive amount of up to 5% by weight, based on the weight of component (b).

    Abstract translation: 本发明涉及一种通过引入反应混合物来加强地下工作和矿井中的地质构造的方法，所述反应混合物反应以形成聚氨酯至待加强的地层中，所述反应混合物基于（a）多异氰酸酯 组分，（b）多元醇组分和（c）酯，所述酯的羟值为约10至630，酸值至多为10，并且由（i）至少具有羧基官能度的酸组分 并且含有具有至少12个碳原子的聚合脂肪酸或其与具有至少12个碳原子的未聚合的饱和或不饱和脂肪酸的混合物，和（ii）含有至少一种多元醇的多元醇组分，所述酯存在于阳性 数量高达5％（重量），基于组分（b）的重量。

    Single-phase, storage-stable polyol compositions containing salts and the use thereof in the production of polyurethanes
    58.
    发明授权
    Single-phase, storage-stable polyol compositions containing salts and the use thereof in the production of polyurethanes 失效
    含有盐的单相，储存稳定的多元醇组合物及其在生产聚氨酯中的用途

    公开(公告)号：US4436841A

    公开(公告)日：1984-03-13

    申请号：US497640

    申请日：1983-05-24

    Applicant: Werner Rasshofer ,  Wolfgang Reichmann ,  Adolf Richartz ,  Manfred Dietrich

    Inventor： Werner Rasshofer ,  Wolfgang Reichmann ,  Adolf Richartz ,  Manfred Dietrich

    IPC: C08G18/66 ,  C08K5/053 ,  C09K3/00 ,  C08G18/14 ,  C08G18/65

    CPC classification number: C08G18/6674 ,  C08K5/053 ,  C08G2120/00 ,  C08G2130/00 ,  Y10S521/914

    Abstract: A single-phase, storage-stable, emulsifier-free polyol mixture comprising 100 parts of a relatively high molecular weight polyoxyalkylene polyol of OH number from 20 to 120, which has at least 5% and less than 80% by weight, of terminal oxyethylene blocks; from 1 to 100 parts of a low molecular weight diol mixture which is a reaction product of ethylene glycol, butane diol-1,4, or a mixture of ethylene glycol and butane diol-1,4, with from 0.05 to 0.50 mols of alkyl oxiranes; from 0.1 to 5 parts of solubilizing additives comprising one or more salts, the cations of which are from Groups I, II and III of the Periodic Table, ammonium or mono- to tetra-alkyl ammonium ions, and the anions of which are produced by removing at least one proton from an acid having a K.sub.s value of at least 10.sup.-7 ; and, optionally, other compounds having isocyanate-reactive hydrogen atoms and other auxiliaries and additives for polyurethane production. Also polyurethanes produced using these polyol mixtures.

    Abstract translation: 一种单相，储存稳定，不含乳化剂的多元醇混合物，其包含100份具有20-120的OH数量的相对高分子量的聚氧化烯多元醇，其具有至少5重量％且小于80重量％的末端氧化乙烯 块 1至100份低分子量二醇混合物，其是乙二醇，丁二醇-1,4-或乙二醇和丁二醇-1,4-的混合物与0.05至0.50摩尔烷基的反应产物 环氧乙烷 0.1至5份包含一种或多种盐的增溶添加剂，其阳离子来自周期表第I，II和III族，铵或一至四烷基铵离子，其阴离子由 从Ks值至少为10-7的酸中除去至少一个质子; 和任选的具有异氰酸酯反应性氢原子的其它化合物和用于聚氨酯生产的其它助剂和添加剂。 还使用这些多元醇混合物制备聚氨酯。

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