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    Multiple feeder reactor for the production of nano-particles of metal
    65.
    发明授权
    Multiple feeder reactor for the production of nano-particles of metal 有权
    用于生产金属纳米颗粒的多重进料反应器

    公开(公告)号：US08986602B2

    公开(公告)日：2015-03-24

    申请号：US13220392

    申请日：2011-08-29

    申请人： Robert Mercuri ,  Michael Kasper ,  Emilie Bekaert ,  Peter Axmann

    发明人： Robert Mercuri ,  Michael Kasper ,  Emilie Bekaert ,  Peter Axmann

    IPC分类号： B01J19/26 ,  C22B5/20 ,  B22F9/30 ,  B01J4/00 ,  B22F1/00 ,  B82Y30/00 ,  C22C19/03 ,  C22C21/00

    CPC分类号： B22F9/305 ,  B01J4/002 ,  B01J19/26 ,  B01J2219/00006 ,  B01J2219/00119 ,  B22F1/0018 ,  B22F2999/00 ,  B82Y30/00 ,  C22B5/20 ,  C22C19/03 ,  C22C21/00 ,  B22F2203/00

    摘要： The reactor is used for producing nano-particles of metal from volatile moieties in flow through mode. The reactor comprises at least a first feeder and a second feeder on one end of the vessel. The first feeder feeds the moiety in the form of an educt fluid into the reactor. This fluid is a mixture of metal moieties and a bearer fluid, entering the reactor in a vaporized state, in which the bearer fluid is used as a carrier gas. The second feeder is used as a radiator means to heat up the educt fluid within the reactor. By providing the heating fluid through the second feeder control over some environmental conditions like ambient temperature within the reactor is achieved and dissociation of the metal moieties under such controlled conditions leads to quantitative production of selected nano-particle morphologies.

    摘要翻译： 该反应器用于在流动模式下从挥发性部分制备金属的纳米颗粒。 反应器包括至少第一进料器和在容器的一端上的第二进料器。 第一个进料器将部分以喷射流体的形式进料到反应器中。 该流体是金属部分和承载流体的混合物，其以汽化状态进入反应器，其中承载流体用作载气。 第二进料器用作加热反应器内的流出液的散热器装置。 通过在某些环境条件下提供加热流体，例如反应器内的环境温度，并且在这种受控条件下金属部分的解离导致选定的纳米颗粒形态的定量生产。

    PURIFICATION OF PGM SPECIES FROM MIXTURES THEREOF
    66.
    发明申请
    PURIFICATION OF PGM SPECIES FROM MIXTURES THEREOF 有权
    从其混合物中纯化PGM物种

    公开(公告)号：US20100043598A1

    公开(公告)日：2010-02-25

    申请号：US12373438

    申请日：2007-06-28

    申请人： Dmitri Terekhov ,  Nanthakumar Victor-Emmanuel ,  Olujide Olurin ,  Kamran M. Khozan

    发明人： Dmitri Terekhov ,  Nanthakumar Victor-Emmanuel ,  Olujide Olurin ,  Kamran M. Khozan

    IPC分类号： C22B5/20 ,  C22B11/02

    CPC分类号： C22B5/20 ,  C22B11/02 ,  C22B11/021 ,  C22B11/06 ,  Y02P10/214

    摘要： A process for the production of a purified PGM selected from the group consisting of platinum and rhodium from an impure PGM source, the process comprising (a) obtaining an anhydrous PGM halide from the impure PGM source; (b) treating the PGM halide with carbon monoxide at an effective temperature; pressure and time to form the PGM carbonyl halide; and (c) (i) wherein the PGM is platinum, heating the platinum carbonyl halide at an effective platinum decomposition temperature to produce the purified platinum; (ii) wherein the PGM is rhodium, heating the rhodium halide at an effective rhodium decomposition temperature to produce the purified rhodium; and (iii) wherein the platinum carbonyl carbonyl halide and the rhodium carbonyl halide are in a gaseous mixture, effecting step (i) at a temperature lower than the rhodium effective decomposition temperature prior to effecting step (ii). The process is of particular value in the recovery and recycle of PGM materials from vehicle exhaust catalytic converters.

    摘要翻译： 一种从不纯的PGM源生产选自铂和铑的纯化PGM的方法，该方法包括（a）从不纯的PGM源获得无水PGM卤化物; （b）在有效温度下用一氧化碳处理PGM卤化物; 压力和时间形成PGM羰基卤化物; 和（c）（i）其中PGM是铂，以有效的铂分解温度加热铂羰基卤化物以产生纯化的铂; （ⅱ）其中PGM是铑，在有效的铑分解温度下加热卤化铑以产生纯化的铑; 和（iii）其中所述铂羰基羰基卤化物和所述卤化铑为气态混合物，在进行步骤（ii）之前，在低于所述铑有效分解温度的温度下进行步骤（i）。 该方法对于从车辆尾气催化转化器中回收和回收PGM材料具有特殊的价值。

    Method of winning copper, nickel, and other metals
    70.
    发明授权
    Method of winning copper, nickel, and other metals 失效
    铜，镍等金属的获得方法

    公开(公告)号：US3967958A

    公开(公告)日：1976-07-06

    申请号：US391619

    申请日：1973-08-27

    申请人： Thomas H. Coffield ,  Kestutis A. Keblys

    发明人： Thomas H. Coffield ,  Kestutis A. Keblys

    IPC分类号： C22B5/20 ,  C22B15/00 ,  C22B23/06 ,  C22B15/10 ,  C22B23/04

    CPC分类号： C22B5/20 ,  C22B15/0093 ,  C22B23/065 ,  Y02P10/236 ,  Y10S423/04

    摘要： The invention is a process for winning nickel by treating an aqueous ammonium salt solution of nickel salts with a carbon monoxide-containing gas under reducing conditions to produce nickel carbonyl and subsequently recovering nickel therefrom. Optionally, the production of nickel carbonyl can be catalyzed, for example, by cyanide. Also, an essentially water-immiscible solvent for nickel carbonyl can optionally be employed. The aqueous ammoniacal solution is typically an aqueous ammoniacal ammonium chloride, carbonate, sulfate, hydroxide, or mixture thereof. The valuable metals associated with nickel, e.g., copper, cobalt, iron, and precious metals, are also separated and recovered by this process. The general nature of the process allows a wide variety of primary and secondary sources of nickel to be utilized by combining this process with a number of known ore-treatment steps.

    摘要翻译： 本发明是通过在还原条件下用含一氧化碳的气体处理镍盐的铵盐溶液以产生镍羰基并随后从其中回收镍来获得镍的方法。 任选地，羰基镍的生产可以例如由氰化物催化。 此外，可以任选地使用与羰基镍基本上水不混溶的溶剂。 氨水溶液通常为含水氨基氯化铵，碳酸盐，硫酸盐，氢氧化物或其混合物。 与镍（例如铜，钴，铁和贵金属）相关的贵重金属也通过该方法分离和回收。 该方法的一般性质允许通过将该方法与许多已知的矿石处理步骤组合来使用多种一次和二次镍源。