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    AZIRIDINATED TRIGLYCERIDES AND POLYMERS FORMED THEREFROM
    61.
    发明申请
    AZIRIDINATED TRIGLYCERIDES AND POLYMERS FORMED THEREFROM 审中-公开
    辅助的三聚体和形成的聚合物

    公开(公告)号：US20160289218A1

    公开(公告)日：2016-10-06

    申请号：US15085345

    申请日：2016-03-30

    申请人： Iowa State University Research Foundation, Inc.

    发明人： Ruqi Chen ,  Jason Shih-Hao Chen ,  Chaoqun Zhang ,  Michael Richard Kessler

    IPC分类号： C07D405/12 ,  C08G63/685 ,  C08G63/78

    CPC分类号： C07D405/12 ,  C08G63/6852 ,  C08G73/02

    摘要： Various embodiments disclosed relate to aziridinated triglycerides and polymers formed therefrom. In various embodiments, the present invention provides an aziridinated triglyceride having the structure described herein. In various embodiments, the present invention provides a method of making the aziridinated triglyceride, a method of crosslinking the aziridinated triglyceride to form a polymer, the polymer formed from the aziridinated triglyceride, a triglyceride with at least one pendent unsaturated group that can be used to form the aziridinated triglyceride, and a method of making the triglyceride having at least one pendent unsaturated group.

    摘要翻译： 所公开的各种实施方案涉及氮丙啶化的甘油三酸酯和由其形成的聚合物。 在各种实施方案中，本发明提供具有本文所述结构的氮丙啶化甘油三酸酯。 在各种实施方案中，本发明提供了制备氮丙啶化甘油三酸酯的方法，使氮丙啶化甘油三酯交联以形成聚合物的方法，由氮丙啶化甘油三酯形成的聚合物，具有至少一个侧链不饱和基团的甘油三酯，其可用于 形成氮丙啶化甘油三酸酯，以及使甘油三酯具有至少一个侧链不饱和基团的方法。

    Method for continuous production of biodegradable aliphatic/aromatic polyester copolymer
    63.
    发明授权
    Method for continuous production of biodegradable aliphatic/aromatic polyester copolymer 有权
    连续生产生物降解脂肪/芳族聚酯共聚物的方法

    公开(公告)号：US09416224B2

    公开(公告)日：2016-08-16

    申请号：US14651800

    申请日：2013-07-18

    申请人： LOTTE FINE CHEMICAL CO., LTD. ,  S-ENPOL CO., LTD.

    发明人： Gyung Don Kang ,  Ki Chull Yun ,  Sang Yob Kim ,  Kil Seuk Byun ,  Jung Ryum ,  Boo Seong Kim ,  Sei Hoon Kim ,  Sung Bae Park

    IPC分类号： C08G63/85 ,  C08G63/181 ,  C08G63/78 ,  C08G63/183 ,  C08G63/02

    CPC分类号： C08G63/85 ,  C08G63/181 ,  C08G63/183 ,  C08G63/78

    摘要： A continuous preparation method of a biodegradable aliphatic/aromatic polyester copolymer includes: performing a first esterification reaction of an aliphatic dihydroxy compound with an aliphatic dicarboxylic acid at a temperature of 185° C. or less; continuously performing a second esterification reaction of a reaction product from the first esterification reaction; continuously performing a first polycondensation reaction of a reaction product from the second esterification reaction to obtain a prepolymer; continuously performing a second polycondensation reaction of the prepolymer to obtain a second polycondensation reaction product having an intrinsic viscosity from about 0.9 dl/g to about 1.0 dl/g; and continuously performing a third polycondensation reaction of the second polycondensation reaction product to prepare the biodegradable aliphatic/aromatic polyester copolymer, wherein the performing of the first esterification reaction or the continuously performing of the second esterification reaction includes adding an aromatic carboxylic acid. The biodegradable aliphatic/aromatic polyester copolymer prepared by control of the intrinsic viscosity of the second polycondensation reaction product may be improved in processibility, film formability, tensile/tearing strength, and blending ability with another polymer resin. Use of a less amount of the aliphatic dihydroxy compound as a starting material may reduce manufacturing costs.

    摘要翻译： 生物降解性脂肪族/芳香族聚酯共聚物的连续制备方法包括：在185℃以下的温度下进行脂族二羟基化合物与脂肪族二羧酸的第一次酯化反应; 连续进行来自第一酯化反应的反应产物的第二次酯化反应; 连续进行来自第二酯化反应的反应产物的第一次缩聚反应，得到预聚物; 连续进行预聚物的第二缩聚反应，得到特性粘度为约0.9dl / g至约1.0dl / g的第二缩聚反应产物; 并连续进行第二缩聚反应产物的第三缩聚反应，制备生物降解性脂肪族/芳香族聚酯共聚物，其中进行第一酯化反应或连续进行第二酯化反应包括加入芳族羧酸。 通过控制第二缩聚反应产物的特性粘度而制备的可生物降解的脂族/芳族聚酯共聚物可以提高加工性，成膜性，拉伸/撕裂强度和与另一种聚合物树脂的共混能力。 使用少量的脂肪族二羟基化合物作为原料可能降低制造成本。

    Toner comprised of a sustainable polyester resin
    64.
    发明授权
    Toner comprised of a sustainable polyester resin 有权
    碳粉由可持续的聚酯树脂组成

    公开(公告)号：US09360782B2

    公开(公告)日：2016-06-07

    申请号：US14059840

    申请日：2013-10-22

    申请人： Xerox Corporation

    发明人： Ke Zhou ,  Guerino G Sacripante ,  Edward G Zwartz ,  Cuong Vong ,  Richard PN Veregin

    IPC分类号： G03G9/087 ,  C08G63/64 ,  C08G63/553 ,  C08G63/78

    CPC分类号： G03G9/08755 ,  C08G63/553 ,  C08G63/64 ,  C08G63/78 ,  G03G9/0806 ,  G03G9/08791

    摘要： The disclosure describes a one reactor process for making a bio-based polyester resin and the polyester polymer thereof The bio-based polymer is the product of a condensation reaction of (a) a rosin diol, (b) neopentyl glycol, (c) succinic acid, (d) an aromatic dicarboxylic acid and (e) dipropylene glycol or tripropvlene glycol, wherein the rosin diol is a reaction product between a rosin acid and a cyclic alkylene glycol and comprises only one rosin moiety. The resultant polyester resin retains thermal properties as compared to a similar resin but made using previous multi-step processes conducted in separate vessels.

    摘要翻译： 本发明描述了一种制备生物基聚酯树脂的反应器方法及其聚酯聚合物。生物基聚合物是（a）松香二醇，（b）新戊二醇，（c）琥珀酸酯的缩合反应的产物 酸，（d）芳族二羧酸和（e）二丙二醇或三丙二醇，其中松香二醇是松香酸和环状亚烷基二醇之间的反应产物，并且仅包含一个松香部分。 所得聚酯树脂与类似的树脂相比保持热性能，但是使用在分开的容器中进行的先前的多步法制备。

    Method for producing polymer and device for producing polymer
    65.
    发明授权
    Method for producing polymer and device for producing polymer 有权
    生产聚合物的方法和用于生产聚合物的装置

    公开(公告)号：US09346915B2

    公开(公告)日：2016-05-24

    申请号：US14372621

    申请日：2013-01-25

    申请人： Taichi Nemoto ,  Chiaki Tanaka

    发明人： Taichi Nemoto ,  Chiaki Tanaka

    IPC分类号： C08G63/78 ,  C08G63/08 ,  B01J19/24

    CPC分类号： C08G63/78 ,  B01J19/242 ,  B01J19/243 ,  B01J19/248 ,  B01J2219/00135 ,  B01J2219/2401 ,  C08G63/08 ,  C08G63/785 ,  Y02P20/544

    摘要： A method for producing a polymer, including: (i) continuously supplying and bringing at least a first monomer, which is ring-opening polymerizable, and a compressive fluid into contact with each other, to thereby allow the first monomer to carry out ring-opening polymerization to continuously generate an intermediate; and (ii) bringing the intermediate and a second monomer, which is identical to or different from the first monomer in kind, into contact with each other, to thereby allow the intermediate and the second monomer to carry out polymerization.

    摘要翻译： 一种聚合物的制造方法，其特征在于，包括：（i）连续供给至少使可开环聚合的第一单体和压缩流体彼此接触，从而使第一单体进行环 - 开始聚合以连续生成中间体; 和（ii）将与第一种类相同或不同的中间体和第二单体彼此接触，从而允许中间体和第二单体进行聚合。

    Continuous Solid-State Polymerization Device and Method
    66.
    发明申请
    Continuous Solid-State Polymerization Device and Method 有权
    连续固态聚合装置及方法

    公开(公告)号：US20160136611A1

    公开(公告)日：2016-05-19

    申请号：US14902076

    申请日：2013-11-21

    申请人： SAMSUNG SDI CO., LTD.

    发明人： Sang Kyun IM ,  Ki Yon LEE ,  Shin Hyo BAE ,  Young Jun KIM ,  Kyoung Kyun PARK ,  Young Sub JIN ,  Sang Hyun JEON

    IPC分类号： B01J19/28 ,  C08G64/20 ,  C08G63/78 ,  C08G63/80 ,  B01J19/00 ,  C08G69/06

    CPC分类号： B01J19/28 ,  B01J19/0073 ,  B01J2219/00094 ,  B01J2219/00159 ,  B01J2219/00162 ,  B01J2219/0204 ,  B01J2219/0245 ,  C08G63/785 ,  C08G63/80 ,  C08G64/205 ,  C08G69/06 ,  C08G69/30 ,  Y02P20/149

    摘要： A continuous solid-state polymerization device according to the present invention comprises: a feeder for injecting a prepolymer continuously; a transverse reactor connected to the feeder via a first connector to receive the prepolymer from the feeder and to perform solid-state polymerization, the reactor itself rotating; and a chamber connected to the transverse reactor via a second connector to receive a polymer, which has been discharged from the transverse reactor, and solid-state polymerization of which has been completed, and to discharge the polymer, wherein the transverse reactor has a demolding coating film formed on the inner wall thereof, and the feeder, the transverse reactor and the chamber are in a vacuum state. The continuous solid-state polymerization device can prevent formation of an interval, in which the prepolymer stagnates, and can perform solid-state polymerization continuously in a vacuum state without using inert gas.

    摘要翻译： 根据本发明的连续固态聚合装置包括：用于连续注入预聚物的进料器; 通过第一连接器连接到进料器的横向反应器以从进料器接收预聚物并进行固态聚合，反应器本身旋转; 以及通过第二连接器连接到横向反应器的室，以接收已经从横向反应器排出的聚合物，并且固体聚合已经完成，并且排出聚合物，其中横向反应器具有脱模 在其内壁上形成的涂膜，并且进料器，横向反应器和室处于真空状态。 连续固态聚合装置可以防止间歇形成，其中预聚物停滞，并且可以在真空状态下连续进行固态聚合而不使用惰性气体。

    Method for manufacturing biodegradable copolymer by split-injecting aromatic dicarboxylic acid compound
    69.
    发明授权
    Method for manufacturing biodegradable copolymer by split-injecting aromatic dicarboxylic acid compound 有权
    通过分散注入芳族二羧酸化合物制造可生物降解的共聚物的方法

    公开(公告)号：US09187595B2

    公开(公告)日：2015-11-17

    申请号：US14402516

    申请日：2013-05-13

    申请人： SAMSUNG FINE CHEMICALS CO., LTD

    发明人： Jong Pil Chun ,  Ye Jin Kim ,  Ki Chull Yun ,  Min Kyoung Kim

    IPC分类号： C08G63/16 ,  C08G63/183 ,  C08G63/12 ,  C08G63/78 ,  C08G63/52

    CPC分类号： C08G63/183 ,  C08G63/12 ,  C08G63/181 ,  C08G63/78

    摘要： There is provided a method of preparation for a biodegradable co-polyester, the method including: forming an oligomer through a primary esterification reaction between a hydroxy group of an aliphatic dihydroxy compound and a carboxylic group of an aliphatic dicarboxylic acid compound; performing a secondary esterification reaction between the formed oligomer and an aromatic dicarboxylic acid compound; and performing a polycondensation reaction in a vacuum, in which sequentially divided addition of the aromatic dicarboxylic acid compound is performed and the weight ratio of the aromatic dicarboxylic acid compound with respect to the oligomer for each time of the sequentially divided addition is from 2:8 to 5:5. The method efficiently increases a solubility of aromatic dicarboxylic acid, thereby increasing a reaction rate and reducing a side reaction.

    摘要翻译： 提供了一种可生物降解的共聚酯的制备方法，其包括：通过脂肪族二羟基化合物的羟基与脂肪族二羧酸化合物的羧基之间的一次酯化反应形成低聚物; 在形成的低聚物和芳族二羧酸化合物之间进行二次酯化反应; 在真空中进行缩聚反应，其中进行依次分配的芳族二羧酸化合物的添加，并且芳香族二羧酸化合物相对于低聚物的重量比分别为2:8 至5：5。 该方法有效地提高芳族二羧酸的溶解度，从而提高反应速度并减少副反应。